Contributed Articles
Transcript of Contributed Articles
Contributed Articles
Potentiometric Study of Base Strengths in the Binary Solvent, Acetic Acid-Chloroform. O. W. Kolling and K. I. Laws 986
Investigation of Polytertiary Alkylamines Using Chemical Ionization Mass Spectrometry. Τ. Λ. Whitney, L. P. Klemann, and F. H. Field 1048
Automation of Nitrogen Analysis of Grain and Grain Products. D. E. Uhl, Ε. Β. Lancaster, and Charles Vojnovich 990
Conducting Glass Electrode in a Thin-Layer Electrochemical Cell with Application to the Analysis of Neptunium. R. C. Propst 994
Combined High Speed Liquid Chromatography and Bioassay for the Evaluation and Analysis of an Or-ganophosphorus Larvacide. R. A. Henry, J. A. Schmit, J. F. Dieckman, and F. J. Murphey 1053
Laser Pyrolysis Gas Chromatography—Application to Polymers. 0. F. Folmer, Jr. 1057
Electrochemical Reduction of α,^-Unsaturated Ketones. J. P. Zimmer, J. A. Richards, J. C. Turner, and D. H. Evans 1000
X-Ray Photoelectron Spectroscopy of Quaternary Phosphonium Compounds. W. E. Swartz, Jr., and D. M. Hercules 1066
Characterization and Analysis of Waxes by Gel Permeation Chromatography. D. E. Hillman 1007
Analysis of Chrome Ores and Chrome-Magnesite Refractory Samples by Atomic Absorption Spectrometry. R. P. Lucas and B. C. Ruprecht 1013
Rapid Laboratory Dialysis for Aminoacylation Assay of tRNA. Hao-Chia Chen, C. H. O'Neal, and L. C. Craig 1017
Neutron Activation Analysis of Sediments for Halogens Using Szilard-Chalmers Reactions. L. J. Walters, Jr., and J. W. Winchester 1020
Analytical Significance of Peaks and Peak Ratios in X-Ray Fluorescence Analysis Using a High Resolution Semiconductor Detector. Analysis of Uranium Solutions by X-Ray Spectrometry. Cesia Shenberg and Saadia Amiel 1025
Analysis of Krebs Cycle and Related Acids in Guinea Pig Tissue by Gas-Liquid Chromatography. Estner Mensen de Silva 1031
Resolution Enhancement of Chromatograph Peaks. D. W. Kirmse and A. W. Westerberg 1035
Gas Chromatographic Analysis of Phenol and Substituted Methyl Phenols Using Open Tubular Columns. Jân Hrivnâk and Jiri Macék 1039
Fluorometric Determination of Some Primary Aromatic Amines with 2,6-Diaminopyridine. L. J. Drom-browski and E. L. Pratt 1042
Barium Ion-Selective Electrode Based on a Neutral Carrier Complex. R. J. Levins 1045
Spectroelectrochemistry—Application of Optically Transparent Minigrid Electrodes under Semi-Infinite Diffusion Conditions. Miiica Petek, T. E. Neal, and R. W. Murray 1069
Mercury-Platinum Optically Transparent Electrode. W. R. Heineman and Theodore Kuwana 1075
Computerized Recording and Interpretation of Spark Source Mass Spectra. Robert Brown, Patrick Powers, and W. A. Wolstenholme 1079
Submolecular Group Analyses of High Resolution Mass Spectra of Peptides and Other Sequence Molecules. A. Kunderd, R. B. Spencer, and W. L. Budde 1086
Mechanistic Studies on the Valinomycin-Based Potassium Electrode. Ehud Eyal and G. A. Rechnitz 1090
Notes
Gas Chromatographic Resolution of Optically Active Alcohols as 3/3-Acetoxy-A5-Etienates. M. W. Anders and M. J. Cooper 1093
Effect of Temperature Control on the Stability and Sensitivity of a High Pressure Liquid Chromatography Ultraviolet Flow Cell Detector. Gary Brooker 1095
Interpretation and Correlation of Bulkiness Chirality and Separation Coefficients in the Resolution of Dia-stereoisomers by Gas-Liquid Partition Chromatography. Binyamin Feibush 1098
Spectrophotometry Determination of Cyanide, Sulfide, and Sulfite with Mercuric Chloranilate. R. E. Humphrey and Willie Hinze 1100
ANALYTICAL CHEMISTRY, VOL. 43, NO. 8, JULY 1971 • 3 A
Contributed Articles
Example of Flame Photometric Analysis for Methyl Parathion in Rat Whole Blood and Brain Tissue. Joe Gabica, Joe Wyllie, Michael Watson, and W. W. Benson 1102
Analysis of Composite Spectra from Mixtures Subjected to Micromolecular Distillation in a Mass Spectrometer. R. D. Grigsby, C. 0. Hansen, D. G. Manner-ing, W. G. Fox, and R. H. Cole 1135
Determination of Perbromates by Potentiometric Titration. J. R. Brand and M. L. Smith 1105 Correspondence
Molecular Weight Determination of Benzene Containing Compounds by Ultraviolet Spectrometry. F. R. Seymour 1107
Separation of Calcium-Strontium Investigated by the Use of Tracers. E. J. Baratta and F. E. Knowles, Jr. 1138
Determination of Nitric Acid in Oleum with a Nitrate Ion Selective Electrode. J. M. C. Ridden, R. R. Barefoot, and J. G. Roy 1109
Conductometric Determination of pK„ Values—Oxalic and Squaric Acids. R. /. Gelb 1110
Measurement of Atmospheric Nitrous Oxide Using a Molecular Sieve 5A Trap and Gas Chromatography. M. D. LaHue, H. D. Axelrod, and J. P. Lodge, Jr. 1113
Ferrate(VI) Analysis by Cyclic Voltammetry. A. S. Venkatadri, W. F. Wagner, and H. H. Bauer 1115
Aids for Analytical Chemists
Digital Data Acquisition from a Hilger-Watts H I 2 0 0 Infrared Spectrophotometer. J. S. Mattson and A. C. McBride III
Modification of a Direct Probe for the Controlled Introduction of Mass Spectrometer Samples. L. D. Smith-
1139
Versatile Injection System for Gas Chromatography. G. E. Pollock, Angelo Margozzi, Ralph Donaldson, and Fritz Woeller 1141
1142
Contraction of Some Solvents Used in Low-Temperature Spectrometric Measurements. Onno Korver and Jan Bosma 1119
Modification of a Fraction Collector for Large Volumes and Use of Siphons in Fraction Collecting. N. S. Radin 1143
Determination of Iodine and Fluorine in Selenium. Ulla Westerlund-Helmerson 1120
Determination of Polysorbates in Food Products by Reaction Gas Chromatography. Gary Lundqu/st and C. E. Meloan 1122
Stoichiometry in the Neutral lodometric Procedure for Ozone by Gas-Phase Titration with Nitric Oxide. J. A. Hodgeson, R. E. Baumgardner, B. E. Martin, and K. A. Rehme 1123
Some Observations on Stoichiometry of lodometric Analyses of Ozone at pH 7.0. S. L. Kopczynski and J. J. Bufalini 1126
Determination of Submicrogram Quantities of Mercury in Pulp and Paperboard by Flameless Atomic Absorption Spectrometry. D. C. Lee and C. W. Lauf-mann 1127
Programmed Temperature Gas Chromatography for Identification of Ester Plasticizers. Anoop Kn'shen 1130
Technique for Controlling Thio Compound Concentration in Electroless Plating Baths. N. Feldstein and J. A. Weiner 1133
© Copyright 1971
by the American chemical Society
MANUSCRIPT REQUIREMENTS published in December 1970 issue, page 1879, outlines scope and copy requirements to be observed in preparing manuscripts for consideration. Manuscript (4 copies) should be submitted to ANALYTICAL CHEMISTRY, 1155 Sixteenth St., N.W., Washington, D. C. 20036.
The American Chemical Society assumes no responsibility for the statements and opinions advanced by contributors to its publications. Views expressed in the editorials are those of the editors and do not necessarily represent the official position of the American Chemical Society.
1971 Subscription Rates
1 yr. 2 yr. 3 yr.
$5.00 Î 9.00 $12.00 7.00 12.00 16.00
15.00 27.50 40.00
Members, domestic and foreign Nonmembers, domestic and Canada Nonmembers, foreign except Canada
Postage: Canada and Pan-American Union, $2.50; foreign, $3.50. Single copies: current, $2.00 except Annual Reviews, $3.00 each. Rates for back issues and volumes are available from Special Issues Sales Dept., 1155 Sixteenth St., N.W., Washington, D. C. Claims for missing numbers will not be allowed if received more than 60 days from date of mailing plus time normally required for postal delivery of journal and claim. No claims allowed because of failure to notify the Subscription Service De' partment of a change of address or because copy is "missing from files." Those interested in joining the American Chemical Society should write to Admissions Department at the Washington Office.
Published monthly with Review issue added in April and a Laboratory Guide in July by the American Chemical Society, from 20th and Northampton Sts., Easton, Pa. 18042; Executive Offices, Editorial Headquarters, and Subscription Service Department, 1155 Sixteenth St., N.W., Washington, D. C. 20036; Advertising Office, 142 East Ave., Norwalk, Conn. 06851. ANALYTICAL CHEMISTRY and other ACS periodicals are available on microfilm. For information write to: MICROFILM, Special Issues Sales, American Chemical Society. 1155 Sixteenth St., N.W., Washington, D. C. 20036. Second class postage paid at Easton, Pa. CHANGE OF ADDRESS: Notify Subscription Service Department, American Chemical Society, 1155 Sixteenth St., N.W., Washington, D. C. 20036. Such notification should include both old and new addresses, with ZIP code numbers, and be accompanied by mailing label from a recent issue. Allow four weeks for change to become effective.
4 A • ANALYTICAL CHEMISTRY, VOL. 43, NO. 8, JULY 1971
ABC