micromeritics® instrument corporatio

1
micromeritics® instrument corporation Briefs Determination of Trace Quantities of Aromatic Amines in Dyestuffs 171 Benzidine, a- and β-naphthylamine, 3,3'-dichloroben- zidine, and 4-dimethylaminoazobenzene are analyzed by extraction with chloroform followed by gas-liquid chroma- tography and thin-layer chromatography. Janos Schulze,* Charles Ganz, and Douglas Parkes, Dyestuffs and Chemicals Division, CIBA-GEIGY Corporation, Post Office Box 11422, Greensboro, N.C. 27409 Anal. Chem., 50 (1978) Determination of the Aqueous Solubility of Polynuclear Aromatic Hydrocarbons by a Coupled Column Liquid Chromatographic Technique 175 A novel technique based on pumping distilled water through thermostated "generator columns" provides a means for determining the aqueous solubility of polynu- clear aromatic hydrocarbons as a function of temperature. Willie E. May* and Stanley P. Wasik, Institute for Materials Re- search, National Bureau of Standards, Washington, D.C. 20234, and David H. Freeman, Chemistry Department, University of Maryland, College Park, Md. 20790 Anal. Chem., 50 (1978) Nondestructive High Temperature Gas Radiochromatography 179 A nondestructive gas radiochromatographic system for continuous operation at 300 °C is developed. Backgrounds are low (75 cpm) and detector decontamination can be done in situ. B. E. Gordon,* W. R. Erwin, M. Press, and R. M. Lemmon, Laboratory of Chemical Biodynamics, Lawrence Berkeley Labora- tory, University of California, Berkeley, Calif. 94720 Anal. Chem., 50 (1978) Aids for Analytical Chemists Isolation of Xenobiotic Chemicals from Tissue Samples by Gel Permeation Chromatography 182 Douglas W. Kuehl* and Edward N. Leonard, U.S. Environmen- tal Protection Agency, Environmental Research Laboratory-Du- luth, 6201 Condgon Boulevard, Duluth, Minn. 55804 Anal. Chem., 50 (1978) High Performance Liquid Chromatographic Determination of Unreacted Acrylamide in Emulsion or Aqueous Homopolymers or Emulsion Copolymers 185 F. J. Ludwig, Sr.,* and M. F. Besand, Research Laboratory, Petrolite Corporation, Tretolite Division, St. Louis, Mo. 63119 Anal. Chem., 50 (1978) Supplementary Information for "Reagent Chemicals", 5th Edition 188 Manuscript Requirements Spectrometry Nomenclature 189 190 Guide for Use of Terms in Reporting Data in ANALYTICAL CHEMISTRY 191 Analysis, Identification, Determination, and Assay SI Units 191 192 CIRCLE 142 ON READER SERVICE CARD 10 A · ANALYTICAL CHEMISTRY, VOL. 50, NO. 1, JANUARY 1978 Unattended H PLC Up to 192 injections Up to 64 samples Automatically . . . • Microprocessor operation controls injections per sample, injection time, rinse b e t w I H samples and automatic shutdown. • Positive flow design requiiB only 0.75 ml of sample, allows precise, reproducible sample volumes. • Adaptable to any HPLCrli pumping unit — can be externally controlled by computer integrator. . . . with the model 72^ automatic injector for HPLC 5680 goshen springsWB| Τ^^ΉΤ^^ U.S.A. · telephone: 404/44ïPH£^R!Tex: 70-7450

Transcript of micromeritics® instrument corporatio

micromeritics® instrument corporation

Briefs

Determination of Trace Quantities of Aromatic Amines in Dyestuffs 171 Benzidine, a- and β-naphthylamine , 3,3'-dichloroben-zidine, and 4-dimethylaminoazobenzene are analyzed by extract ion with chloroform followed by gas- l iquid chroma­tography and thin- layer chromatography. Janos Schulze,* Charles Ganz, and Douglas Parkes , Dyestuffs and Chemicals Division, CIBA-GEIGY Corporation, Post Office Box 11422, Greensboro, N.C. 27409 Anal. Chem., 50 (1978)

Determination of the Aqueous Solubility of Polynuclear Aromatic Hydrocarbons by a Coupled Column Liquid Chromatographic Technique 175 A novel technique based on pumping distilled water through the rmos ta t ed "genera tor co lumns" provides a means for de te rmining the aqueous solubility of polynu­clear aromat ic hydrocarbons as a function of t empera tu re . Willie E. May* and Stanley P. Wasik, Institute for Materials Re­search, National Bureau of Standards, Washington, D.C. 20234, and David H. Freeman, Chemistry Department, University of Maryland, College Park, Md. 20790 Anal. Chem., 50 (1978)

Nondestructive High Temperature Gas Radiochromatography 179 A nondest ruct ive gas radiochromatographic system for cont inuous operat ion at 300 °C is developed. Backgrounds are low (75 cpm) and detector decontamina t ion can be done in situ. B. E. Gordon,* W. R. Erwin, M. Press, and R. M. Lemmon, Laboratory of Chemical Biodynamics, Lawrence Berkeley Labora­tory, University of California, Berkeley, Calif. 94720

Anal. Chem., 50 (1978)

Aids for Analytical Chemists

Isolation of Xenobiotic Chemicals from Tissue Samples by Gel Permeation Chromatography 182

Douglas W. Kuehl* and Edward N. Leonard, U.S. Environmen­tal Protection Agency, Environmental Research Laboratory-Du-luth, 6201 Condgon Boulevard, Duluth, Minn. 55804

Anal. Chem., 50 (1978)

High Performance Liquid Chromatographic Determination of Unreacted Acrylamide in Emulsion or Aqueous Homopolymers or Emulsion Copolymers

185

F. J . Ludwig, Sr.,* and M. F. Besand, Research Laboratory, Petrolite Corporation, Tretolite Division, St. Louis, Mo. 63119

Anal. Chem., 50 (1978)

Supplementary Information for "Reagent Chemicals", 5th Edition 188

Manuscript Requirements

Spectrometry Nomenclature

189

190

Guide for Use of Terms in Reporting Data in ANALYTICAL CHEMISTRY 191

Analysis, Identification, Determination, and Assay

SI Units

191

192 CIRCLE 142 ON READER SERVICE CARD

10 A · ANALYTICAL CHEMISTRY, VOL. 50, NO. 1, JANUARY 1978

Unattended H PLC Up to 192 injections Up to 64 samples Automatically . . . • Microprocessor operat ion

controls injections per sample, injection time, rinse b e t w I H samples and automatic shutdown.

• Positive flow design requi iB only 0.75 ml of sample, al lows precise, reproducible sample volumes.

• Adaptable to any HPLCrli pumping unit — can be externally controlled by computer integrator.

. . . wi th the model 7 2 ^ automatic injector for HPLC

5680 goshen spr ingsWB| Τ^^ΉΤ^^ U.S.A. · telephone: 4 0 4 / 4 4 ï P H £ ^ R ! T e x : 70-7450