ASSOCIATED NAVAL ARCHITECTS, INC. 3400...

McCALLUMTESTING LABORATORIES, INC.

Geotechnical Engineering, Materials Testing & Environmental Services

SITE CHARACTERIZATION ADDENDUM PHASE

QUARTERLY MONITORING REPORT

ASSOCIATED NAVAL ARCHITECTS, INC.

3400 SHIPWRIGHT STREET

PORTSMOUTH, VIRGINIA

DEQ PC#05-5160

MTL PROJECT #05-1681 / 05-6695

1808 HAYWARD AVENUE, CHESAPEAKE, VA. 23320 Φ P. O. BOX 13337, CHESAPEAKE, VA. 23325-0337 PHONE (757) 420-2520 Φ FAX (757) 424-2874

McCALLUM TESTING LABORATORIES, INC. Geotechnical Engineering, Materials Testing & Environmental Services


May 23, 2006

Associated Naval Architects, Inc. 3400 Shipwright Street Portsmouth, Virginia 23703 Attention: Brandt Everhart Secretary and General Counsel Subject: Site Characterization Addendum Phase Quarterly Monitoring Report Associated Naval Architects, Inc. 3400 Shipwright Street Portsmouth, Virginia DEQ PC# 05-5160 MTL Project #05-1681 / 05-6695 Dear Mr. Everhart: McCallum Testing Laboratories, Inc. is pleased to present this Quarterly Monitoring Report of the subject property, performed in general conformance with the Department of Environmental Quality (DEQ) Petroleum Program Manual effective October 4, 2001. Should you have any questions regarding this report, please contact our office at your convenience. Sincerely, MCCALLUM TESTING LABORATORIES, INC. Marvin D. Smith Project Geologist Richard J. Seage, P.G. Manager, Environmental Services Copy: Lynne E. Smith - DEQ

McCALLUM TESTING LABORATORIES, INC. Geotechnical Engineering, Materials Testing & Environmental Services


SITE CHARACTERIZATION ADDENDUM PHASE QUARTERLY MONITORING REPORT

ASSOCIATED NAVAL ARCHITECTS, INC. 3400 SHIPWRIGHT STREET PORTSMOUTH, VIRGINIA

MTL Project # 05-1681/05-6695 DEQ PC# 05-5160

Prepared for

Brandt Everhart Associated Naval Architects, Inc.

3400 Shipwright Street Portsmouth, Virginia 23703

Submitted to

Lynne E. Smith Virginia Department of Environmental Quality

Tidewater Regional Office 5636 Southern Boulevard

Virginia Beach, Virginia 23462

Prepared by

McCallum Testing Laboratories, Inc.

1808 Hayward Avenue Chesapeake, Virginia 23320

SIGNATURE/CERTIFICATION SHEET I certify that I have prepared or supervised preparation of the attached report, that it has been prepared in accordance with industry standards and practices, and that the information contained herein is truthful and accurate to the best of my knowledge. Prepared by: Marvin D. Smith _______________________________ Project Geologist Richard Seage, P.G. _____________________________ Manager, Environmental Services VA Professional Certification: CPG #466 McCallum Testing Laboratories, Inc. 1808 Hayward Avenue Chesapeake, Virginia 23320 UST Owner/ Operator: Associated Naval Architects, Inc. 3400 Shipwright Street Portsmouth, Virginia 23703

TABLE OF CONTENTS

SIGNATURE/CERTIFICATION SHEET TABLE OF CONTENTS 1.0 PROJECT HISTORY 2.0 MONITORING RESULTS 3.0 QUARTERLY GROUNDWATER ANALYSES 4.0 FREE PRODUCT RECOVERY 4.1 AFVR Pilot Study 4.2 Free Product Recovery Record 5.0 CONCLUSIONS AND RECOMMENDATIONS 6.0 LIMITATIONS APPENDIX A - FIGURES

Figure 1 - Site Location Map Figure 2 - Site Drawing Figure 3 - AFVR Area of Influence

APPENDIX B - CERTIFICATE OF ANALYSIS and CHAIN OF CUSTODY FORM APPENDIX C - VACUUM TRUCK MANIFESTS

1

SITE CHARACTERIZATION ADDENDUM QUARTERLY MONITORING REPORT

ASSOCIATED NAVAL ARCHITECTS, INC. PORTSMOUTH, VIRGINIA

Section 1.0 PROJECT HISTORY On March 29, 2005, during a site inspection by the Department of Environmental Quality (DEQ), minor amounts of free product were observed by the DEQ inspector, in a shallow open excavation in the area where Associated Naval Architects (ANA) was constructing a concrete pad for an aboveground air supply tank. The Site Location Map (Figure 1-Appendix A) shows the location of the site. An aboveground used oil tank was previously located in this area. The DEQ requested that Initial Abatement Measures and a Site Characterization be conducted to determine the nature and extent of the suspected release. On June 22, 2005, McCallum conducted a site characterization of ANA, which consisted of drilling six soil borings in the area identified in a previous Site Check report as the area of an AST used oil release. The Site Drawing (Figure 2-Appendix A) shows the locations of the borings. Selected soil samples from the borings were submitted to the laboratory for Total Petroleum Hydrocarbons (TPH) analysis using EPA Method 418.1. Laboratory analysis detected moderate to high TPH concentrations in the soil samples. The TPH results, measured in milligrams TPH per kilogram of soil (mg/kg), are presented in the table below.

SCR LABORATORY RESULTS (SOIL)

SAMPLE PID Response (ppm) TPH-418.1 (mg/kg)B-1 (4-5’) 99 409.9 B-2 (4-5’) 1 460.8 B-3 (4-5’) 0 BDL B-4 (2-4’) 11 7916.0 B-5 (4-5’) 2 205.7 B-6 (2-4’) 1 166.0

BDL – Below Detection Limit mg/kg – Equivalent to parts per million (ppm)

Based on laboratory results, petroleum contaminated soils covered an area approximately 1600 to 1800 square feet, around the area of the former used oil AST. To help determine the groundwater quality beneath the site, five (5) 2 inch diameter groundwater monitoring wells (MW-1 through MW-5) were installed. Figure 2 shows the locations of the monitoring wells. Groundwater was examined for free product in each monitoring well and was sampled for TPH analysis. No free product was detected in MW-1, MW-2, MW-3 or MW-5; however, a minor amount of free product (1/8 inch) was detected in MW-4.

2

Since the AST reportedly contained used oil, the groundwater samples were analyzed for Total Petroleum Hydrocarbons (TPH) using EPA Test Method 418.1. The results of the laboratory analyses are presented in the following table.

LABORATORY RESULTS (Groundwater)

Well TPH Concentration (mg/L) MW-1 8.1 MW-2 28.4 MW-3 BDL MW-5 12.9

BDL- Below detection limit mg/L – Equivalent to parts per million (ppm) Since the free product detected was considered a continuous source of both dissolved phase and residual phase contamination and due to the proximity of the impacted area to the Elizabeth River, the remediation of the free product was addressed. In-Situ Bioremediation was requested by the DEQ, as a cost effective method of remediation at this site. A product known as AgroRemed® was chosen, because of its ability to address all phases of petroleum contamination using a single application. Prior to the application of AgroRemed, groundwater samples were collected from each of the monitoring wells and submitted to the laboratory for analysis, to establish a baseline to compare and determine the effectiveness of the remediation process. On October 6, 2005, the five groundwater monitoring wells were sampled. Prior to sampling, each of the monitoring wells were examined for free product. The groundwater data for each monitoring well is presented in the table below.

GROUNDWATER DATA October 6, 2005

Well Elevation Top of Casing (ft.)

Depth to Groundwater (ft.)

Groundwater Elevation (ft.)

Free Product Thickness (in.)

MW-1 6.12 2.51 3.61 0.12 MW-2 6.39 2.26 4.13 0.0 MW-3 6.78 2.71 4.07 0.0 MW-4 6.75 2.25 4.52 0.24 MW-5 6.68 2.23 4.45 0.0

Elevations are relative to an arbitrary benchmark of +10.00 ft. Groundwater elevations in MW-1 and MW-4 are corrected for free product The groundwater samples were analyzed for GRO-TPH, DRO-TPH, BTEX, MTBE and Naphthalene at the direction of the DEQ. The baseline laboratory results are presented in the table below.

3

LABORATORY RESULTS (GROUNDWATER) (mg/L)

October 6, 2005 Analyte MW-1 MW-2 MW-3 MW-4 MW-5

TPH-GRO 1.1 BDL BDL BDL 0.80

TPH-DRO 32.4 10.4 0.60 14.8 5.10

MTBE BDL BDL BDL BDL BDL

Benzene 0.0056 BDL BDL BDL BDL

Toluene 0.0078 BDL BDL 0.0054 BDL

Ethylbenzene 0.0121 BDL BDL 0.0393 BDL

Xylene BDL BDL BDL 0.0393 BDL

Naphthalene 0.2070 0.0170 BDL 0.1256 0.0392 BDL - Below Detection Limit mg/L- Equivalent to parts per million (ppm) The TPH concentration detected in boring B-4/MW-4 from the SCR (7,916 ppm) was used as the baseline reading for the petroleum contaminated soil. On October 18, 2005, McCallum conducted the AgroRemed application at ANA. A total of 20 gallons of AgroRemed were used in the 2,000 square foot coverage area. A total of fifteen gallons of AgroRemed were directly applied by sprayer on the ground surface. Four gallons were applied full strength, within a shallow trench around the former AST area, currently the air tank platform and one half gallon each was used in a spot application around monitoring wells MW-1 and MW-4. Section 2.0 MONITORING RESULTS The groundwater was examined for free product in each of the monitoring wells for six months following the application of the AgroRemed. The groundwater data is presented in the table below. Initial field observations of the free product

4

Associated Naval Architects Groundwater Data

Date Parameter MW-1 MW-2 MW-3 MW-4 MW-5 Groundwater

Depth (ft) 2.46 2.11 2.67 2.15 2.16

11/10/05 Groundwater Elevation (ft) 3.66* 4.28 4.11 4.63* 4.52

Free Product (in) 0.12 0.0 0.0 0.48 0.0

Groundwater Depth (ft) 2.15 1.98 2.30 1.99 N/A

12/30/05 Groundwater Elevation (ft) 3.97 4.41 4.48 4.76* N/A

Free Product (in) 0.0 0.0 0.0 0.12 N/A

Groundwater Depth (ft) 2.18 1.91 2.30 1.92 1.90

1/12/06 Groundwater Elevation (ft) 3.94 4.48 4.48 4.85* 4.78

Free Product (in) Emulsion 0.0 0.0 0.24 0.0

Groundwater Depth (ft) 2.63 2.40 2.83 2.23 N/A

Groundwater Elevation (ft) 3.49 3.99 3.95 4.61* N/A 2/21/06

Free Product (in) 0.0 0.0 0.0 1.2 N/A


Groundwater Elevation (ft) 3.35 3.79 3.78 4.04* 2.88 3/16/06

Free Product (in) 0.0 0.0 0.0 12.96 0.0


Groundwater Elevation (ft) 3.51 3.82 3.95 4.31* 4.13 4/19/06

Free Product (in) 0.0 0.0 0.0 6.0 0.0

* Groundwater elevations are corrected for free product N/A – Not Accessible Note: AgroRemed applied on 10-18-05 Section 3.0 QUARTERLY GROUNDWATER ANALYSES On January 12, 2006 and April 19, 2006 groundwater samples from the monitoring wells were collected and submitted to EnviroCompliance Laboratories for TPH, BTEX, MTBE and Naphthalene analyses. The laboratory results including the baseline results are presented in the table below. The laboratory’s Certificate of Analysis is included in Appendix B. Graphed comparisons of TPH and Naphthalene concentrations are also presented below.

5

Laboratory Results –Groundwater (mg/L)

MW-1 MW-2 MW-3 Analyte 10/6/05 1/12/06 4/19/06 10/6/05 1/12/06 4/19/06 10/6/05 1/12/06 4/19/06

TPH – GRO 1.1 BDL BDL BDL BDL BDL BDL 1.2 BDL

TPH – DRO 32.4 39.7 6.90 10.4 6.3 BDL 0.60 BDL BDL

MTBE BDL BDL BDL BDL BDL BDL BDL BDL BDL

BENZENE 0.0056 BDL BDL BDL BDL BDL BDL BDL BDL

TOLUENE 0.0078 BDL BDL BDL BDL BDL BDL BDL BDL

E-BENZENE 0.0121 BDL BDL BDL BDL BDL BDL BDL BDL

XYLENE BDL BDL BDL BDL BDL BDL BDL BDL BDL

NAPHTHALENE 0.2070 0.060 BDL 0.0170 0.030 0.0131 BDL BDL BDL BDL – Below detection limit mg/L - Equivalent to parts per million (ppm)

Laboratory Results –Groundwater (mg/L)

MW-4 MW-5 Analyte 10/6/05 1/12/06 4/19/06 10/6/05 1/12/06 4/19/06

TPH – GRO BDL 0.80 N/A 0.80 BDL 1.30

TPH – DRO 14.8 216.2 N/A 5.10 0.60 BDL

MTBE BDL BDL N/A BDL BDL BDL

BENZENE BDL BDL N/A BDL BDL BDL

TOLUENE 0.0054 0.0094 N/A BDL BDL BDL

E-BENZENE 0.0393 0.0432 N/A BDL BDL BDL

XYLENE 0.0393 BDL N/A BDL BDL BDL

NAPHTHALENE 0.1256 1.70 N/A 0.0392 BDL BDL BDL – Below detection limit mg/L - Equivalent to parts per million (ppm) N/A – No analyses run. Free product present

Graphed comparisons of TPH and Naphthalene concentrations are also presented below.

6

Groundwater Analyses Results MW-1

05

1015202530354045

10/6/05 1/12/06 4/19/06

Date

Conc

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mg/

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GRO DRO Naphthalene


0

2

4

6

8

10

12

10/6/05 1/12/06 4/19/06

Date

Conc

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mg/

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GRO DRO Naphthalene

7


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10/6/05 1/12/06 4/19/06

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100

150

200

250

10/6/05 1/12/06 4/19/06

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10/6/05 1/12/06 4/19/06

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Section 4.0 FREE PRODUCT RECOVERY Groundwater monitoring shows a significant increase in free product in MW-4 in March. McCallum previously recommended the use of Aggressive Fluid Vapor Recovery (AFVR) to recover free product that may have been trapped within pockets formed by fill material in the subsurface. Section 4.1 AFVR Pilot Study On March 16, 2006, McCallum monitored a pilot study of Aggressive Fluid-Vapor Recovery (AFVR) to determine its effectiveness as a method of free product recovery. The depth to groundwater and free product was measured in each monitoring well prior to recovery, to obtain baseline readings from which to measure the groundwater table drawdown and determine the radius of influence. The recovery point was from monitoring well MW-4. The vacuum in the truck stabilized at 20 inches of mercury during the operation. The depth to groundwater and product thicknesses in the surrounding wells were recorded at regular intervals as presented in the following table.

9

GROUNDWATER DATA March 16, 2006

0.5 Hour 2.5 Hours 5.5 Hours Well

Prior to

Start Measurement Change (in) Measurement Change

(in) Measurement Change (in)

Water Table Depth (ft.) 2.77 2.77 0 2.81 -0.48 2.84 -0.84 MW-1 Product

Thickness (in.) 0 0 0 0 0 0 0 Water Table Depth (ft.) 2.60 2.60 0 2.69 -1.08 2.81 -2.52 MW-2 Product

Thickness (in.) 0 0 0 0 0 0 0 Water Table Depth (ft.) 3.00 3.00 0 3.00 0 3.00 0 MW-3 Product

Thickness (in.) 0 0 0 0 0 0 0 Water Table Depth (ft.) 3.80 2.75 +12.6 2.78 +12.24 2.78 +12.24 MW-5 Product

Thickness (in.) 0 0 0 0 0 0 0 This data was used to generate a map of the AFVR drawdown (Figure 3). The map shows an irregular area of influence that is likely due to the irregular nature of the subsurface fill material. However, the radius of drawdown is apparently sufficient to affect the impacted area. Section 4.2 Free Product Recovery Two AFVR events have been performed to date. Approximate recovery totals are presented in the table below. AFVR FREE PRODUCT RECOVERY RECORD

Date Contaminated Water Recovered Free Product Recovered

3/16/06 836 120 4/20/06 527 9 Total 1363 129

Section 5.0 CONCLUSIONS / RECOMMENDATIONS The application of AgroRemed appears to have reduced the levels of dissolved phase contamination in the groundwater and increased dispersion of the free product, resulting in an increase in the amount of free product in MW-4. Recovery of the free product utilizing aggressive fluid vapor recovery (AFVR) appears to be effective; therefore, its continued use is recommended.

10

Section 6.0 LIMITATIONS It is important to note that the groundwater samples analyzed in this investigation are considered as isolated data points which may not be representative of subsurface conditions across the entire site. Therefore, the conclusions of this investigation may not be completely indicative of all subsurface conditions. The conclusions are based on the scope of work described herein and the best available data at this time. No other warranty is expressed or implied. This report does not warrant against future operations or present conditions not discovered by this investigation.

APPENDIX A

FIGURES

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McGALLUM TESTING LABORATORIES, ING.1808 Hayrard Avenue

Ghesapeake, Virginia 23325-0337Approved By: Richard J. Seage, p.G.

Associated Naval Architects3400 Shipwright Street

Portsmouth, Virginia DEQ PC#05-51 60

DrawingTitle:

Area of AFVR lnfluence

APPENDIX B

GERTI FIGATES OF ANALYSF

AND CHAIN OF CUSTODY FORM

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APPENDIX G

VACUUM TRUCK MANIFEST

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VA CLASS A LIC2701 0371144

Recovery Services, Inc.635 Maltby Avenue

P.O. Box 1458Norfolk, Virginia 23501

(757) 627-87s1

N9 3612224 HOUR EMERGENCY

RESPONSE1-800-723-69s1

JoB No D-16722-06JLl, t I

CUSTOMER'S ORDER NO. DAIE: 04 | 20 r A6

CUSTOMER'S NAME: I4cCALLLIM TESTING l,AtsS

MAILING ADDRESS: P. O. Box 1 3337 . Chesapeake . VA 23325

Adliiional Description For Material Listed Above:r l ' i , A

\ ttrJilf Kt---'o'{e:v < 'ALA VYtc n|lon', n tA<lispetroCtrem necovery Services, Inc. gX .ir,, 4635 Maltby Ave., Norfolk, VA 23504 * , , t i f i -

THE CUSTOI!{ER AGREES THAT IT SHALL NOT PROVIDE TO PETROCHEM RECOVERY SERVICES, INC. ANY"HMARDOUS WASTE" OR "HAZARDOUS SUBSTANCE" AS DEFINED IN THE CODE OF FEOERAL REGUIJATIONS.

ACCEPTANCE OF JOB -- The prices, spacifications and conditions are satislaclory and are hereby accepted. You are authorized to

do the work speciiied. payment to bs made as follorrs: Net 10 days upon completion of PetroChom Recovery Services, Inc. work order'

1 .57" Serv iceChargepermonthover30days logetherw i iha t to rney 's leesannunt ing loZSq, "o l the to ta l anpuntdue i l incur red .

Leaveshoo 01KS Arrive sire o8 15 Leave Site / RVJrArrive 6p

birxt

Driver's Signature: Truck #

Dale:

Payment Received. $.

Facility Acceptance:r1-../?

PORTLOCK PRINTING 543.5381

JOBLOCATION: ANA' S@

I M SHIPPING NAME & DESCRIPTION OUANTIIY UNIT

Combustible Uquid, n.o.s. r _.1- ,A( L { S E O o t L + W 4 7 C K )itAl993, PG lll

i - '1 r '

5-1(a 6q!.';

b)Flammable Llquid, n.o.s.( )3, uN 1993, PG lll

) Non-Regulated Wastewater

lro-ta{k Ebttpt

ASSOCIATED NAVAL ARCHITECTS, INC. 3400...

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