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Transcript of SYNTHESIS - hps. tre%u015Bci/SYNTHESIS.pdf · PDF file1 Enantioselective Preparation of...

  • SYNTHESIS Vol. 41 - 2009


    No. 1

    1 Enantioselective Preparation of 2-Amino Acid Derivatives for -Peptide Synthesis / D. Seebach, A. K. Beck, S. Capone, G. Deniau, U. Groelj, E. Zass

    33 Discoveries from the Abyss: The Abyssomicins and Their Total Synthesis / K. C. Nicolaou, S. T. Harrison, J. S. Chen

    43 -Metallated O-2-Alkenyl Carbamates: Synthetic Equivalents of Chiral Homoenolates and Materials for Asymmetric Homoaldol Reaction / D. Hoppe

    56 Direct CarbonCarbon Bond Formation via Soft Enolization of Thioesters: An Operationally Simple Mannich Addition Reaction / J. M. Yost, M. R. Garnsey, M. C. Kohler, D. M. Coltart

    59 Synthesis of Norbornane-Bridged Diporphyrins via Palladium-Catalyzed [3+2] Annulation Strategy / M. Mizumura, H. Shinokubo, A. Osuka

    62 Synthesis and Olfactory Evaluation of (4aR*,8aR*)-1,1,8a-Trimethyldecahydronaphthalen-4a-ol: A cis-Decalol Intersection Structure of ()-Patchoulol and (5R*,6S*)-1,1,6-Trimethylspiro[4.5]decan-6-ol / A. Jahnke, C. Burschka, R. Tacke, P. Kraft

    69 Synthesis of Novel Halogenated 4(1H)-Quinolones by Thermolysis of Arylaminomethylene-1,3-dioxane-4,6-diones / S. Rotzoll, H. Reinke, C. Fischer, P. Langer

    79 Synthesis of Functionalized Oligophenylenes and Oligoarylenes Bearing Heteroaryl Groups / I. Wallmann, G. Schnakenburg, A. Ltzen

    85 Synthesis of Benzo[b]furans by PalladiumNHC Catalyzed Ring Closure of o-Bromobenzyl Ketones / J. Farag, A. Kotschy

    91 Intermolecular CH and SiH Insertion Reactions with Halodiazoacetates / H. T. Bonge, T. Hansen

    97 The Direct Synthesis of Unsymmetrical Vicinal Diamines from Terminal Alkynes: A Tandem Sequential Approach for the Synthesis of Imidazolidinones / A. V. Lee, M. Sajitz, L. L. Schafer

    105 Synthesis of 2'-Deoxyuridine and 2'-Deoxycytidine Nucleosides Bearing Bipyridine and Terpyridine Ligands at Position 5 / L. Kalachova, R. Pohl, M. Hocek

    113 Inverse-Electron-Demand DielsAlder Reactions of N-(Heteroarylsulfonyl)-1-aza-1,3-dienes Catalyzed by Chiral Lewis Acids / J. Esquivias, I. Alonso, R. Gmez Arrays, J. C. Carretero

    127 Coordination-Induced Intramolecular Double Cyclization: Synthesis of Boron-Bridged Dipyridylvinylenes and Dithiazolylvinylenes / Q. Zhao, H. Zhang, A. Wakamiya, S. Yamaguchi

    133 An Enantiospecific Approach to Triazolylalanine Derivatives / C. E. Jamookeeah, C. D. Beadle, J. P. A. Harrity

    138 Double Couplings of Dibromothiophenes Using Boronic Acids and Boronates / S. Varello, S. T. Handy

    143 Synthesis of Fmoc-Pro-Hyp(TBDPS)-Gly-OH and Its Application as a Versatile Building Block for the Preparation of Collagen Model Peptides / R. S. Erdmann, H. Wennemers

  • 148 Complementary Reactions of Allylic Carbamates Using Palladium(II): Formation of Oxazolidinones or Allylic Amides from a Common Precursor / S. D. R. Christie, A. D. Warrington, C. J. Lunniss

    155 Thermal Amination of 2,6-Dihalopyridines by Sterically Demanding Amines / A. Faust, O. Wolff, S. R. Waldvogel

    160 The Thermal Amidation of Carboxylic Acids Revisited / L. J. Gooen, D. M. Ohlmann, P. P. Lange

    XVII Instructions for Authors XXIII Forthcoming Articles

  • No. 2 165 Selected Synthetic Strategies to Spirocyclics / S. Kotha, A. C. Deb,

    K. Lahiri, E. Manivannan 194 Effective Catalytic Activity of the Hydrated Gold Catalyst NaAuCl42H2O To

    Construct Highly Fused Cyclopentenones / S. Karmakar, A. Kim, C. H. Oh

    199 Efficient Synthesis of an Allose-Containing Analogue of the Phytoalexin-Elicitor Glucohexaose and Its Dodecyl Glycoside / H. Ma, D. Qiu, X. Mei, J. Ning, Q. Zhao, Y. Li

    205 Synthesis of 1,4-Benzodiazepine-2,5-diones Using an Ionic Liquid as a Soluble Support / H. Xie, C. Lu, G. Yang, Z. Chen

    211 A Facile Synthesis of Thioalkyl- and Di(thioalkyl)-Substituted Bipyridines / D. Chen, R. De, D. L. Mohler

    217 Diastereoselective Synthesis of Dimethyl (4R*,4a'R*,7a'R*)-1-Aryl-6'-benzoyl-4a'-methyl-5-oxo-1,4',4a',5,5',6'-hexahydrospiro[pyrazole-4,7'-pyrrolo[3,4-c]pyridazine]-3',7a'(1'H)-dicarboxylates / U. Uri, U. Groelj, A. Meden, J. Svete, B. Stanovnik

    227 Synthesis of 3-Acylpyrroles, 3-(Alkoxycarbonyl)pyrroles, 1,5,6,7-Tetrahydro-4H-indol-4-ones and 3-Benzoylpyridines Based on StaudingerAza-Wittig Reactions of 1,3-Dicarbonyl Compounds with 2- and 3-Azido-1,1-dialkoxyalkanes / E. Bellur, M. A. Yawer, I. Hussain, A. Riahi, O. Fatunsin, C. Fischer, P. Langer

    243 Regioselective Synthesis of Functionalized Biaryls Based on the First [3+3] Cyclocondensations of 4-Aryl-1,3-bis(trimethylsilyloxy)buta-1,3-dienes / M. Adeel, M. A. Rashid, N. Rasool, R. Ahmad, A. Villinger, H. Reinke, C. Fischer, P. Langer

    251 Synthesis of Functionalized Bicyclic Precursors of Heptulosonic Acid Analogues / H. Filali, S. Ballereau, F. O. Chahdi, M. Baltas

    257 Efficient Regio- and Stereoselective Synthesis of 5-Alkyl(aryl)idene- and 5-[Iodoalkyl(aryl)idene]-1H-pyrrol-2(5H)-ones via Electrophilic Cyclization / K. Cherry, A. Duchne, J. Thibonnet, J.-L. Parrain, E. Anselmi, M. Abarbri

    271 Pd/Cu-Catalyzed Oxidative CH Alkenylation of Imidazo[1,2-]pyridines / J. Koubachi, S. Berteina-Raboin, A. Mouaddib, G. Guillaumet

    277 A Convenient Synthesis of Unsymmetrical Pinacols by Coupling of Structurally Similar Aromatic Aldehydes Mediated by Low-Valent Titanium / X.-F. Duan, J.-X. Feng, G.-F. Zi, Z.-B. Zhang

    283 A Method for the Selective Protection of Aromatic Amines in the Presence of Aliphatic Amines / V. Perron, S. Abbott, N. Moreau, D. Lee, C. Penney, B. Zacharie

    290 Synthesis and Antiviral Evaluation of ()-3'-Methylcarbovir, ()-3'-Methylabacavir, and Modified Purine Analogues / P. Brmond, G. Audran, H. Monti, E. De Clercq, C. Pannecouque

    297 Regioselective Synthesis of 2-(Aryloxythio)benzoates by the First [3+3] Cyclizations of 3-Aryloxythio-1-silyloxybuta-1,3-dienes with 3-Alkoxy-2-en-1-ones / I. Iqbal, M. Imran, A. Villinger, P. Langer

    306 Molybdenum(VI) Dichloride Dioxide Catalyzed Conversion of b-Hydroxycarbonyls into a-Bromo 1,3-Dicarbonyls by N-Bromosuccinimide / K. Jeyakumar, D. K. Chand

  • 311 A Short Route to the Synthesis of Pyrrolocoumarin and Pyrroloquinolone Derivatives by Sonogashira Cross-Coupling and Gold-Catalyzed Cycloisomerization of Acetylenic Amines / K. C. Majumdar, B. Chattopadhyay, S. Samanta

    318 Aspects of the Synthesis of an Exceptionally Preorganized Self-Immolative SpacerPhenolate Unit / M. Waibel, X.-B. Zhang, J. Hasserodt

    325 Design and Efficient Synthesis of Amino Acid Derived 2-Substituted Imidazoles by Palladium-Catalyzed Cross-Coupling Reactions / A. Marek, J. Kulhnek, F. Bure

    332 A Convenient Preparation of Di-p-chlorobenzyl Azodicarboxylate (DCAD) for Mitsunobu Couplings / B. R. Taft, E. C. Swift, B. H. Lipshutz

    335 Enantioselective Rhodium-Catalyzed Alkylative Desymmetrization of 3,5-Dimethylglutaric Anhydride / M. J. Cook, T. Rovis

    XIII Forthcoming Articles

  • No. 3 339 Intermolecular Addition Reactions of N-Acyliminium Ions (Part I) /

    A. Yazici, S. G. Pyne 369 Desulfurization of Thioamides into Amides with H2O2/ZrCl4 Reagent System

    / K. Bahrami, M. M. Khodaei, Y. Tirandaz 372 Total Synthesis of ()-1,3,4,5-Tetragalloylapiitol / R. M. Patel,

    N. P. Argade 375 A Convenient Synthesis of 4-Hydroxy-2-oxo-1,2-dihydro-1,8-

    naphthyridine-3-carboxamide Derivatives / K. Kobayashi, D. Iitsuka, S. Fukamachi, H. Konishi

    379 Intramolecular Ketalization of Functionalized 7-Norbornenols / L. A. Paquette, J. D. Pettigrew

    385 Ring Contraction of 1,2-Dihydronaphthalenes Promoted by Thallium(III) in Acetonitrile: A Diastereoselective Approach to Indanes / H. M. C. Ferraz, V. M. T. Carneiro, L. F. Silva, Jr.

    389 Regio-Controlled Nucleophilic Attack of 3-Thiaisatoic Anhydride by -Amino Acids: One-Pot Synthesis of 3-(2-Thienyl)imidazolidine-2,4-dione and 3,4-Substituted Thieno[2,3-e][1,4]diazepine-2,5-dione Analogues / Y. Brouillette, G. Sujol, J. Martinez, V. Lisowski

    395 The Unprecedented Cobalt-Catalysed Oxidative Glaser Coupling under Reductive Conditions / G. Hilt, C. Hengst, M. Arndt

    399 Nucleophilic Addition of 4-Hydroxycoumarin to BaylisHillman Acetate Adducts / C. Raji Reddy, N. Kiranmai, K. Johny, M. Pendke, P. Naresh

    403 Palladium-Mediated Heck Reaction to the Synthesis of 3-Substituted Indoles and Indolones / K. C. Majumdar, S. Chakravorty, P. K. Shyam, A. Taher

    409 Synthesis of Bicyclo[3.1.0]hexan-2-ones by Manganese(III) Oxidation in Ethanol / K. Asahi, H. Nishino

    424 High Regio- and Stereoselective Synthesis of (Z)- or (E)-N-Acryl Butenedioic Monoimide Derivatives by a Multicomponent Reaction / F. Sha, Y. Lin, X. Huang

    431 The First Synthesis of Allyl Isonitriles from BaylisHillman Adducts, and Their Application in the Synthesis of Substituted Imidazo[1,2-]pyridines and Tetraazadibenzoazulenes / M. Nayak, S. Kanojiya, S. Batra

    438 One-Pot Three-Step Synthesis of Pyrazinothienopyrimidines Using Tandem Aza-Wittig/Electrocyclic Ring Closure / G. Blanco, A. Fernndez-Mato, J. M. Quintela, C. Peinador

    445 Synthesis of Biaryls, Fluorenones, Cyclopenta[def]phenanthren-4-ones, and Benzophenones Based on Formal [3+3] Cyclocondensations of 1,3-Bis(silyloxy)buta-1,3-dienes with 3-(Silyloxy)-2-en-1-ones / S. Reim, M. Lau, M. Adeel, I. Hussain, M. A. Yawer, A. Riahi, Z. Ahmed, C. Fischer, H. Reinke, P. Langer

    464 Diastereoselective Synthesis of -Stabilized Phosphorus Ylides via a Four-Component Reaction / A. Alizadeh, N. Zohreh, L.-G. Zhu

    469 Stereoselective Synthesis of Alkynyl Vinyl Chalcogenides via HornerWittig Reaction / C. C. Silveira, F. Rinaldi, R. C. Guadagnin, A. L. Braga

    474 Stereoselective Preparation of C1C10 and C11O14 Fragments of N