Mathematics (Ι) B - University of Technology, Iraq€¦ · Mathematics (Ι) 10 Basic Principles of...

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Contents First Year Syllabus Title Page Technical English 9 Mathematics (Ι) 10 Basic Principles of Chem. Eng. ( I ) 11 Chemistry 12 Chemistry of Petroleum 13 Chemistry Laboratory 15 Engineering Drawing 17 Engineering Mechanics and Strength of Materials 18 Electrical Technology 19 Computer Programming (I) 20 Workshop 22 Second Year Syllabus Human Rights 23 Democracy 24 Mathematics (II) 25 Basic principles of Chem. Eng (II) 26 Fluid Flow 27 Fluid Flow Laboratory 29 Physical Chemistry 30 Physical Chemistry Laboratory 31 Computer Programming (II) 32 Material Science and Engineering 34 Material Science and Engineering Laboratory 35 Fuel's Technology 36 Properties of Petroleum Products 37 Fuel's Technology Laboratory 38 Statistics and Measurements 39 Third Year Syllabus Thermodynamics 40 Thermodynamics Laboratory 42 Applied Mathematics 43 Mass Transfer 44 Mass Transfer Laboratory 45 Reactor Design 46 Reactor Design 47 Heat Transfer 48 Heat Transfer Laboratory 49 Equipment Design 50 Equipment Design 51 Numerical Analysis 52 Bio Chemical Eng. 53 Particles and Nano Technology 54 Petrochemical industries 55 Chemicals from Petroleum 56 Combustion Engineering 57 Storage and Transport of Crude Oil and Petroleum Products 58 Fourth Year Syllabus Project 60 Unit Operation 61 Unit Operation Laboratory 62 Process Control 63 Process Control Laboratory 64 Chemical Process Industries 65 Chemical Process Industries Laboratory 66 Petroleum Refinery Eng. 67 Catalysis and Catalytic Eng. 68 Industrial Management 69 Environmental Eng. And Industrial Safety 70 Corrosion Engineering 71 Optimization 72 Petroleum Refinery Eng. 73 Petroleum Refinery Eng. Laboratory 74 Gas Technology 75 Catalysis in Petroleum Refineries 76 Environmental Pollution and Safety in Petroleum Refinery 77 Corrosion Engineering 78

Transcript of Mathematics (Ι) B - University of Technology, Iraq€¦ · Mathematics (Ι) 10 Basic Principles of...

Page 1: Mathematics (Ι) B - University of Technology, Iraq€¦ · Mathematics (Ι) 10 Basic Principles of Chem. Eng. (I) 11 . Chemistry . 12 : Chemistry of Petroleum 13 Chemistry Laboratory

Contents First Year Syllabus

Title Page Technical English 9 Mathematics (Ι) 1 0 Basic Principles of Chem. Eng. ( I ) 1 1 Chemistry 1 2 Chemistry of Petroleum 1 3 Chemistry Laboratory 1 5 Engineering Drawing 1 7 Engineering Mechanics and Strength of Materials 1 8 Electrical Technology 1 9 Computer Programming (I) 2 0 Workshop 2 2

Second Year Syllabus Human Rights 2 3 Democracy 2 4 Mathematics (II) 2 5 Basic principles of Chem. Eng (II) 2 6 Fluid Flow 2 7 Fluid Flow Laboratory 2 9 Physical Chemistry 3 0 Physical Chemistry Laboratory 3 1 Computer Programming (II) 3 2 Material Science and Engineering 3 4 Material Science and Engineering Laboratory 3 5 Fuel's Technology 3 6 Properties of Petroleum Products 3 7 Fuel's Technology Laboratory 3 8 Statistics and Measurements 3 9

Third Year Syllabus Thermodynamics 4 0 Thermodynamics Laboratory 4 2 Applied Mathematics 4 3 Mass Transfer 4 4 Mass Transfer Laboratory 4 5 Reactor Design 4 6 Reactor Design 4 7 Heat Transfer 4 8 Heat Transfer Laboratory 4 9 Equipment Design 5 0 Equipment Design 5 1 Numerical Analysis 5 2 Bio Chemical Eng. 5 3 Particles and Nano Technology 5 4 Petrochemical industries 5 5 Chemicals from Petroleum 5 6 Combustion Engineering 5 7 Storage and Transport of Crude Oil and Petroleum Products 5 8

Fourth Year Syllabus Project 6 0 Unit Operation 6 1 Unit Operation Laboratory 6 2 Process Control 6 3 Process Control Laboratory 6 4 Chemical Process Industries 6 5 Chemical Process Industries Laboratory 6 6 Petroleum Refinery Eng. 6 7 Catalysis and Catalytic Eng. 6 8 Industrial Management 6 9 Environmental Eng. And Industrial Safety 7 0 Corrosion Engineering 7 1 Optimization 7 2 Petroleum Refinery Eng. 7 3 Petroleum Refinery Eng. Laboratory 7 4 Gas Technology 7 5 Catalysis in Petroleum Refineries 7 6 Environmental Pollution and Safety in Petroleum Refinery 7 7 Corrosion Engineering 7 8

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INTRODUCTION

Chemical engineering is the branch of engineering that applies scientific

and mathematical principles to design and develop processes by which

available chemicals can be converted into a variety of useful product such as

detergents, plastics, and pharmaceuticals. Chemical engineers are responsible

for designing these industrial processes that make our lives easier and more

productive. New compounds may be discovered by chemists , however,

without a chemical engineer engaging his/her skills to quantify, test, and

produce it, the new compound may never become a final product.

Chemical engineer also applies his background knowledge of chemistry

with his an understanding of chemical processing to tackle most any

chemical problem, from waste minimization, to environmental remediation,

or to purification of drinking water. Most major chemical companies hire

chemical engineers to fill their technical position in environmental

engineering.

In the chemical engineering department of Technology University, there are two branches, as specialization, starting from the first year. These are Chemical processing engineering. & Oil and gas refinery engineering

The B.sc programmed for the two branches involves mathematics,

including analysis and computer application, chemistry, mechanics,

electricity, chemical engineering principles and practice subjects including

fluid dynamics, heat transfer, unit operation, chemical reactor design,

thermodynamics, and chemical processes. In addition the program involves

English language which is essential for any engineering student to enable

him/her to benefit from thousand of textbooks and periodicals.

A considerable emphasis is laid, in this department, on practical training

and laboratory work, which helps students in getting better understanding of

the theoretical part of their curriculum.

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Moreover students required to spend eight weeks, training in industry

during summer vacations.

This booklet contains the academic program with its units and syllabus for

subjects which are taken by chemical engineering students during their four

years study.

Prof. Thamer Jasim Mohammed

Head of Chemical Engineering Department

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First Year

B.Sc.\ Chemical Processing Engineering

Serial Number

Subject Code Subject

Hours / Week Credits First Term Second Term

L-P-T L-P-T 1 CE.111 Technical English 2-0-0 2-0-0 4 2 CE.121 Mathematics (Ι) 2-0-1 2-0-1 4 3 CE.141 Basic Principles of Chem. Eng. (Ι) 2-0-1 2-0-1 4 4 CE.122 Chemistry 2-2-1 2-2-1 6 5 CE.131 Engineering Drawing 1-2-0 1-2-0 4

6 CE.132 Engineering Mechanics & Strength of Materials 2-0-1 2-0-1 4

7 CE.133 Electrical Technology 1-0-1 1-0-1 2 8 CE.123 Computer Programming (Ι) 1-2-1 1-2-1 4 9 CE.134 Workshop 0-6-0 0-6-0 4 Total 13-12-6 13-12-6 36 4BHours/week 31 31

First Year

B.Sc.\ Oil and Gas Refinery Engineering

Serial Number

Subject Code Subject

Hours / Week Credits First Term Second Term

L-P-T L-P-T 1 CE.111 Technical English 2-0-0 2-0-0 4 2 CE.121 Mathematics (Ι) 2-0-1 2-0-1 4 3 CE.141 Basic principles of Chem. Eng (I) 2-0-1 2-0-1 4 4 CE.142 Chemistry of Petroleum 2-2-1 2-2-1 6 5 CE.131 Engineering Drawing 1-2-0 1-2-0 4

6 CE.132 Engineering Mechanics & Strength of Materials 2-0-1 2-0-1 4

7 CE.133 Electrical Technology 1-0-1 1-0-1 2 8 CE.122 Computer Program ming (Ι) 1-2-1 1-2-1 4 9 CE.134 Workshop 0-6-0 0-6-0 4 Total 13-12-6 13-12-6 36 Hours/Week 31 31

Note: The student is required to complete eight weeks summer training in industry UKey of subject code U(from lift): CE: Chemical Engineering First No.: Year of study Second No.: Specialization

1: Human subject 2: Basic subject

3: General subject 4: Specific subject

Third No.: Order of subject with specialization

UKey of Hours / Week U: L: Lecture , P:Practical , T: Tutorial

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Second Year B.Sc.\ Chemical Processing Engineering

Serial

Number Subject

Code Subject Hours / Week

Credits First Term Second Term L-P-T L-P-T

1 CE.211 Human Rights 1-0-1 0-0-0 1 2 CE.212 Democracy 0-0-0 1-0-1 1 3 CE.221 Mathematics (II) 2-0-1 2-0-1 4 4 CE.241 Basic principles of Chem. Eng (II) 2-0-1 2-0-1 4 5 CE.242 Fluid Flow 2-2-1 2-2-1 6 6 CE.231 Physical Chemistry 2-2-1 2-0-1 5 7 CE.222 Computer Programming (II) 1-2-1 1-2-1 4 8 CE.232 Material Science& Eng. 2-0-1 2-2-1 5 9 CE.243 Fuel’s Technology 1-2-1 1-0-1 3

10 CE.233 Statistics and measurements 1-0-1 1-2-1 3 Total 14-8-9 14-8-9 36 Hours/Week 31 31

Second Year B.Sc.\ Oil and Gas Refinery Engineering

Serial

Number Subject Code Subject

Hours / Week Credits First Term Second Term

L-P-T L-P-T 1 CE.211 Human Rights 1-0-1 0-0-0 1 2 CE.212 Democracy 0-0-0 1-0-1 1 3 CE.221 Mathematics (II) 2-0-1 2-0-1 4 4 CE.241 Basic principles of Chem. Eng (II) 2-0-1 2-0-1 4 5 CE.242 Fluid Flow 2-2-1 2-2-1 6 6 CE.231 Physical Chemistry 2-2-1 2-0-1 5 7 CE.222 Computer Programming (П) 1-2-1 1-2-1 4 8 CE.232 Material Science& Eng. 2-0-1 2-2-1 5 9 CE.244 Properties of Petroleum Products 1-2-1 1-0-1 3

10 CE.233 Statistics & measurements 1-0-1 1-2-1 3 Total 14-8-9 14-8-9 36 Hours/Week 31 31

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Third Year

B.Sc.\Chemical Processing Engineering

Serial Number

Subject Code Subject

Hours / Week Credits First Term Second Term

L-P-T L-P-T 1 CE.341 Thermodynamics 2-0-1 2-2-1 5 2 CE.331 Applied Mathematics 2-0-1 2-0-1 4 3 CE.342 Mass Transfer 2-3-1 2-0-1 5 4 CE.343 Reactor Design 2-0-1 2-0-1 4 5 CE.344 Heat Transfer 2-0-1 2-3-1 5 6 CE.345 Equipment Design 2-2-1 2-0-1 5 7 CE.332 Numerical Analysis 0-0-0 2-2-1 3 8 CE.346 Bio Chemical Eng. 2-0-1 0-0-0 2 9 CE.347 Particles& Nanotechnology 2-0-1 0-0-0 2

10 CE.349 Petrochemical Industries 0-0-0 2-0-1 2 Total 16-5-8 16-7-8 37 Hours/Week 29 31

Third Year

B.Sc.\ Oil and Gas Refinery Engineering

Serial Number

Subject Code Subject

Hours / Week Credits First Term Second Term

L-P-T L-P-T 1 CE.341 Thermodynamics 2-0-1 2-2-1 5 2 CE.331 Applied Mathematics 2-0-1 2-0-1 4 3 CE.342 Mass Transfer 2-3-1 2-0-1 5 4 CE.343 Reactor Design 2-0-1 2-0-1 4 5 CE.344 Heat Transfer 2-0-1 2-3-1 5 6 CE.345 Equipment Design 2-2-1 2-0-1 5 7 CE.332 Numerical Analysis 0-0-0 2-2-1 3 8 CE.346 Chemicals from Petroleum 2-0-1 0-0-0 2 9 CE.348 Combustion Eng. 2-0-1 0-0-0 2

10 CE.3410 Storage & Transport of Crude oil & petroleum Products 0-0-0 2-0-1 2

Total 16-5-8 16-7-8 37 Hours/Week 29 31

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Fourth Year

B.Sc.\Chemical Processing Engineering

Serial Number

Subject Code Subject

Hours / Week Credits First Term Second Term

L-P-T L-P-T 1 CE.441 Project 1-2-0 1-2-0 4 2 CE.442 Unit Operations 2-3-1 2-0-1 5 3 CE.443 Process Control 2-3-1 2-0-1 5 4 CE.444 Chemical Process Industries 1-3-1 1-3-1 4 5 CE.445 Petroleum Refinery Eng. 2-0-1 0-0-0 2 6 CE.446 Catalysis & Catalytic Eng. 2-0-1 0-0-0 2 7 CE.431 Industrial Management 0-0-0 2-0-1 2 8 CE.446 Environment Eng. & Industrial Safety 2-0-1 0-0-0 2 9 CE.447 Corrosion Eng. 0-0-0 2-0-1 2 10 CE.432 Optimization 0-0-0 2-0-1 2 Total 12-11-6 12-5-6 30 Hours/Week 29 23

Fourth Year

B.Sc.\ Oil and Gas Refinery Engineering

Serial Number

Subject Code Subject

Hours / Week Credits First Term Second Term

L-P-T L-P-T 1 CE.441 Project 1-2-0 1-2-0 4 2 CE.442 Unit Operations 2-3-1 2-0-1 5 3 CE.443 Process Control 2-3-1 2-0-1 5 4 CE.448 Petroleum Refinery Eng. 2-3-1 2-3-1 6 5 CE.449 Gas Technology 2-0-1 0-0-0 2 6 CE.4410 Catalysis in Petroleum Refineries 0-0-0 2-0-1 2 7 CE.431 Industrial Management 2-0-1 0-0-0 2

8 CE.4411 Environment Pollution & Safety in Petroleum Refineries 0-0-0 2-0-1 2

9 CE.447 Corrosion Eng. 2-0-1 0-0-0 2 10 CE.432 Optimization 0-0-0 2-0-1 2

Total 13-11-6 13-5-6 32 Hours/Week 30 24

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Hours/unit

In 4-years

Chemical Processing Engineering

Oil and Gas Refinery Engineering

First Term Second Term Two Terms First Term Second Term Two Terms

Number Lecture hr

55 55 110 56 56 112

Number Theoretical hr

29 29 58 29 29 58

Number Practical hr

36 32 68 36 32 68

Total hr 120 116 236 121 117 238

Total units 139 141

Summary Weekly Load

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Comprehension Reading Passages Related to Chemical Engineering What chemical engineers do, Research and development, Process design, Plant operation.

(20 hrs) English Grammar A- Parts of Speech Nouns, Pronouns, Adjectives, Articles, Verbs and verbal's, Adverbs, Conjunctions, Prepositions, Words that need watching, Interjections. B- Analyses of Sentences Classification according to form, Classification according to number of statements. (40 hrs) References

(1) The language of chemical engineering in English, Roy V. Hughson, Regents Publishing Company, Inc. (2) An English Grammar “for use of high school, academy, and college classes”, W. M. Baskervill and J.W. Sewell, The Project Gutenberg eBook, 2004. (3) Practical Exercises in English, Huber Gray Buehler, American Book Company, 2004. (4) English Vocabulary in Use, Stuart Redman, Cambridge University Press, 1997.

First Year –Technical English

Chemical Processing Eng. & Oil and Gas Refinery Engineering

Units 4 Theoretical 2hr/week Tutorial - hr/week Practical -hr/week

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Revision Domain and Range, functions and graphs, even and odd functions, how to shift graph, inverse functions, Trigonometric Functions.

(4 hrs) Limits and Continuity Properties, limits involving infinity, limits of exponential functions

(4 hrs) Transcendental functions Logarithmic and exponential functions, Inverse trigonometric functions, hyperbolic functions, inverse hyperbolic trigonometric functions.

(4 hrs) Derivatives

Definition, second and higher order derivative, implicit differentiation, the chain rule, derivative of inverse trigonometric functions, derivative of hyperbolic functions, derivative of inverse hyperbolic functions, derivative of exponential and logarithmic functions, hopitals rule, partial derivative, Improper Integrals (conv and dity).

(10 hrs) Integration

Indefinite integration, integration of trigonometric functions, integration of inverse trigonometric functions, integration of logarithmic and exponential functions, integration of hyperbolic functions, integration of inverse hyperbolic functions, integration methods; (substitution, by part, power trigonometric functions, trigonometric substitution, by partial function).

(14 hrs) Definite Integration and Applications

Area between two curves, length of curves, surface area, volumes (8 hrs)

Complex Algebra Definitions, Graphing in complex number ( Argand Diagram), Polar form of complex number,

power of complex number, derivatives of complex variable and Cauch Remann, analytic functions, integration of functions.

(6 hrs) Polar Coordinates Definition, Cartesian versus polar coordinates, graphing in polar coordinate.

(4 hrs) Vector Analysis Definitions, properties, vector in space, scalar and cross product of vector.

(6 hrs) References

1- B. Thomas George, "Thomas Calculus". 2- G. Stephenson, "Mathematical methods for science students",2P

ndP edition.

3- V.G. Jenson and G.V. Jeffreys, "Mathematical methods in chemical engineering",2P

ndP

edition.

First Year – Mathematics(I)

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 4 Theoretical 2hr/week Tutorial 1hr/week Practical - hr/week

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General Knowledge of Chemical Engineering Definition of chemical engineering, Chemical process industries (CPI), Generalized chemical Process, Flow sheet and representation of a chemical process (PFD), The difference between the chemist and the chemical engineer . (4 hrs)

Mathematical , Physical and Chemical Principles Dimensions, units, symbols and conversion factors , Precision and significant figures., Density and specific gravity, Temperature, Pressure, The mole unit , Composition and concentration, Basis of calculation, Principles and expressions of stoichiometry. (20 hrs)

Material Balances

Concepts of material balance, Systematic steps of solving material balance problems, Material balances without chemical reactions, Material balances with chemical reactions , Material balances on combustion processes, Material balances involving recycle, bypass and purge streams. (20 hrs)

Gases and Vapors Ideal gas law, Ideal gas mixtures, Real gas relationships, Real gas mixtures, Vapor pressure and saturation. (16 hrs)

References 1- Himmelblau, D.M. and J.B.Riggs," Basic principles and calculations in chemical engineering",8ed , Prentice-Hall Inc., New Jersey,2013. 2- Sikdar, D.C., Chemical process calculations, PHI Learning private ltd., New Delhi, 2013

First Year - Basic Principles of Chemical Engineering(I)

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units: 4 Theoretical 2hr/week Tutorial 1hr/week Practical - hr/week

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Part 1 : Analytical Chemistry Introduction to Analytical Chemistry , Atomic weight , Molecular formula, Chemical , equations, Mole concept, Chemical, equilibrium, equilibrium constants, Solution, Definition , Preparation and properties, Molarity, Normality, Formality, pH, pOH, Buffers, Solubility , Analytical Methods of Analysis , Qualitative Analysis, Quantitative Analysis, Gravimetric Analysis, Precipitation reaction, Direct and indirect method of analysis, Ksp, Volumetric Analysis, Acid Base (Neutralization Titration), Oxidation Reduction Titr, Ion exchange reactions , Potentiometric Titration, Precipitation, Complex titration , Methods of calculation, Titration curves, Instrumental Methods of Analysis, Photometric , Colorimetric, Potentiometric titration, pH measurements, Chromatography, Atomic absorption , Atomic emission Spectroscopy, Errors & Statistical Treatment of Analytical Data (30 hrs)

Part 2: Organic chemistry

Introduction to hydrocarbon, Definition Classification , Aliphatic compounds, Nomenclature, Preparation, Properties, Reactions, Alkanes, Alkenes, Alkynes, Aliphatic Derivatives , (alkyl halides, alcohol's, ethers, aldehydes, ketones, esters, carboxylic acid, amines ,amides, mercaptans, carboxylic acids, thiophenes, disulphide), Aromatic compounds, Structural formula of benzene ring, Nomenclature, Preparation, Properties, Reactions, Nitration, Sulphonation, Halogenation, Alkylation, Benzenehomologues (Preparation, Properties, Reactions, Chemical reaction of (Toluene, Xylene, Ethyl benzene, styrene, Phenols, Anilines, Naphthalene Heterocyclic compounds, Pyridine Furan, Pyrrole, Thiophenes, Quinoline , Introduction to polymer and carbohydrate , Disaccharides, Polysaccharides, Proteins , amino acids , polypeptides and proteins, proteine structure, Organo metallic compounds, Identification of organic compound, Spectrophotometric, Infrared Spectrophotometric, Ultra violet rays. (30 hrs)

References: 1- Brown, LeMay, Bursten, "Chemistry the central scince", 8th

2- john wiely and sons," Organic chemistry ", 4 edition .

th

3- Janice Gorzynski smith ,"Organic chemistry" ,1 edition , (2001).

st

4- Y.Anjaneyulu, K.chandrasekhar " Analytical chemistry", (2006) edition , (2006)

5- prentice –Hall of INDIA private limited new dellhi "Organic chemistry", (1971)

First Year – Chemistry

Chemical Processing Eng. Branch

Units: 6 Theoretical 2hr/week Tutorial 1 hr/week Practical 2 hr/week

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Part 1: Organic chemistry The properties and chemistry of Petroleum and to some of central concepts of organic chemistry: naming, properties, covalent bonding, isomers and petrochemical synthesis. Definition of Organic chemistry and Organic compounds, Origin of Organic compounds (vital force theory), Tetra covalency and catenation property of carbon.

Organic Compounds Classification of Organic compounds, Functional group and homologous series, Introduction to hydrocarbon: (Alkanes, Alkenes, Alkynes) Definition, Classification, Aliphatic compounds ,Nomenclature, Common names, IUPAC system , Preparation ,Properties, Reactions.

Aliphatic derivatives: ( alkyl halides, Alcohol's, ethers, Aldehydes, Ketones, Esters , Carboxylic acid, Amines , Amides, Mercaptans, Carboxylic acids, Thiophenes, Disulphide, glycols): Definition, Classification Aliphatic compounds, Nomenclature, Common names, IUPAC system, Preparation, Physical and chemical Properties, Reactions.

Aromatic compounds Structural formula of benzene ring, Nomenclature, Common names, IUPAC system,

Preparation, Physical and chemical Properties, Reactions, Nitration, Sulphonation, Halogenation, Alkylation

Structure isomerism in organic compounds

Definition of Structure isomerism

Benzene homologues Preparation, Properties, Reactions of, Toluene, Xylene ,Ethyl benzene, Styrene, Phenols,

Anilines ,Naphthalene

Heterocyclic compounds Pyridine, Furan, Pyrrole, Thiophenes, Quinoline

Mechanism of :

Electrophile, nucleophiles and freeradicals, Decarboxylation, Catalytic hydrogenation, Using Grigrand’s, Eagent, Wurtz reaction, From aldehydes and ketones , Isomerization, Reforming processes, Hydrogenation, Cracking (pyrolysis).

Introduction to polymer Mechanism of Polymerization

Organo metallic compounds

Identification of organic compound: Spectrophotometric, Infrared Spectrophotometric, Ultra violet rays (30 hrs)

First Year - Chemistry of Petroleum

Oil and Gas Refinery Eng. Branch

Units 6 Theoretical 2 hr/week Tutorial 1 hr/week Practical 2 hr/week

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Part 2 : Analytical Chemistry Introduction to Analytical Chemistry, Atomic weight , Molecular formula, Chemical equations, Mole concept, Chemical equilibrium, equilibrium constants, Solution Definition ,Preparation and properties, Molarity, Normality, Formality, pH, pOH, Buffers, Solubililty.

Analytical Methods of Analysis Qualitative Analysis, Quantitative Analysis, Gravimetric Analysis, Precipitation reaction, Direct and indirect method of analysis, Ksp, Volumetric Analysis , Acid Base (Neutralization Titration), Oxidation Reduction Titration, Ion exchange reactions , Potentiometric Titration, Precipitation ,Complex titration ,Methods of calculation ,Titration curves. (30 hrs)

References 1- Brown, LeMay, Bursten, "Chemistry the Central Science", 8th

2- John Wiely and Sons, "Organic chemistry", 4 edition.

th

3- Janice Gorzynski Smith, "Organic Chemistry", 1 edition , (2001).

st

4- Y.Anjaneyulu, K.chandrasekhar, "Analytical Chemistry" ,(2006) edition , (2006)

5- "Organic Chemistry", prentice –Hall of INDIA private limited new dellhi, (1971)

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(A)

Exp. Name Exp. No. Preparation of standard solution of NaR2RCOR3 Exp. No. 1 Preparation of Standard solution of HCl Exp. No. 2 Standardization of HCl and the determination of sodium hydroxide solution normality Exp. No. 3

Quantitative determination of a carbonate and hydroxide in mixture Exp. No. 4

Titration Curves Exp. No. 5 Back titration Exp. No. 6 Determination of Chloride Ions in Water Exp. No. 7 Standardization of KMnOR4R and the determination of ferrous sulfate

Exp. No. 8

Determination of Hardness of Water Exp. No. 9 Acidity of Vinegar Exp. No. 10 Paper Chromatography Exp. No. 11 Qualitative analysis silver group Exp. No. 12

(B)

Exp. Name Exp. No.

Boiling point determination Exp. No. 1

Melting point determination Exp. No. 2

Simple Distillation Exp. No. 3

Preparation of aspirin Exp. No. 4

Preparation of ester Exp. No. 5

Identification of functional groups Exp. No. 6

Saponfication reaction Exp. No. 7

Dye &Colorants Exp. No. 8

Preparation of acetic acid Exp. No. 9

First Year - Chemistry Laboratory

Chemical Processing Eng.

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(A)

Exp. Name Exp. No. Preparation of standard solution of NaR2RCOR3 Exp. No. 1 Preparation of Standard solution of HCl Exp. No. 2 Standardization of HCl and the determination of sodium hydroxide solution normality Exp. No. 3

Quantitative determination of a carbonate and hydroxide in mixture Exp. No. 4

Titration Curves Exp. No. 5 Back titration Exp. No. 6 Determination of Chloride Ions in Water Exp. No. 7 Standardization of KMnOR4R and the determination of ferrous sulfate

Exp. No. 8

Determination of Hardness of Water Exp. No. 9 Acidity of Vinegar Exp. No. 10 Paper Chromatography Exp. No. 11 Qualitative analysis silver group Exp. No. 12

(B)

Exp. Name Exp. No.

Boiling point determination Exp. No. 1

Melting point determination Exp. No. 2

Simple Distillation Exp. No. 3

Preparation of aspirin Exp. No. 4

Preparation of ester Exp. No. 5

Identification of functional groups Exp. No. 6

Saponfication reaction Exp. No. 7

Dye &Colorants Exp. No. 8

Preparation of acetic acid Exp. No. 9

Octane Number Exp. No. 10

First Year - Chemistry Laboratory

Oil and Gas Refinery Eng. Branch

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Part 1- Engineering Drawing Introduction General Information about Engineering Drawing and its Importance, Drawing Instruments Types of Lines used in Drawing, Planing of Drawing Paper. (1 hrs)

Projection Drawing First and Third Angle Projection (3 hrs)

.

Sectioning Drawing Full and Half Section. (2 hrs)

The Finding of Third View. (2 hrs)

Pictorial Drawing

Isometric and Oblique. (2 hrs)

Part 2-AutoCAD 1.Definition of AutoCAD Programs, its Applications, Relationship Between CAD and

Engineering Drawing. (2hrs)

2. AutoCAD Drawing Commands and Applications (Line, Circle,….etc). (6 hrs) 3. Projection Drawing (2D) in Engineering Shape. (3 hrs) 4. Sectioning Drawing (Full and Half Section). (4 hrs) 5. Three-Dimensional Drawing (3D). (2 hrs) 6. Simple Shape for Three-Dimensional Drawing. (3 hrs)

References

1993الرسم الهندسي ، تأليف (عبد الرسول الخفاف)،الطبعة الثانية، .1

2- R.P. Hoelscher and C.H.Springer, "Engineering Drawing and Geometry", 2P

ndP edition.

First Year - Engineering Drawing

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 4 Theoretical 1 hr/week Tutorial - hr/week Practical 2 hr/week

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A: Mechanics Principles of Static Mechanics definition, Rigid bodes, Force systems, Static [Equilibrium], Dynamics, Scalar and vector quantities. (2 hrs) Resultants of Force System Resultant, Composition and resolution of forces. (4 hrs)

Equilibrium of Force System Condition of Equilibrium, Moment of force. (6 hrs)

Friction Theory of friction, friction on an inclined plane. (6 hrs)

Centroid and Center of Gravity (6 hrs)

Moment of Inertia (Second moment of the axis) Polar moment of inertia, Transfer formula for moment of inertia. (6 hrs)

B: Strength of Materials 1. Introduction Force in Rigid Bodies: (1 hr) 2. Definition of Stress and Strain: (1 hr) 3. Stress – Strain Diagrams: (2 hrs) 4. Proportional Limits: (4 hrs) Elastic limit, Stiffness elasticity, Plasticity, Hardness and working stress. (2 hrs) 5. Hook ُ◌s Law: 6. Poisson, Ratio, Composite Stresses: (4 hrs) 7. Volumetric Stress, Bulk Modules: (4 hrs) 8. Thin Walled Cylinders: (4 hrs) 9. Thermal Stress: (4 hrs) 10. Shear and Bending Moments in Beam: (4 hrs)

References 1- A.Higdon and W.B. Stiles, "Engineering mechanics- statics and dynamics", vol.1,3P

rd Pedition,

Prentice-Hall, India, 1986. 2- F.L. and A.Pytel ,"Stregth of materials", 3P

rd Pedition, Harper and Row, London,1980.

First Year - Engineering Mechanics & Strength of Materials

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 4 Theoretical 2 hr/week Tutorial 1 hr/week Practical -hr/week

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Introduction To Dc Circuit Material use in electric component, ohms law, temperature Coefficient, Review of Kirchhoff's Laws Series Parallel circuit, equivalent resistance, star / delta Conversion (5 hrs)

Ac Circuit Concepts of AC circuit, rms value Average value, from and peak factors, real and Reactive power – power factor. (5 hrs)

Node And Mesh Analysis

Node and Mesh methods of analysis of DC Circuit and Simple AC Circuits (5 hrs) Polyphases Circuit

Introduction to three phase circuits, Introduction to three phase system , Phase and line parameter – relations ,Power measurement , Voltmeter and ammeter method (5 hrs)

Dc And Ac Generator And Motor

Principle of DC generator and motor, Transformer, Introduction motor(Single phase) (10 hrs) Source For Electrical Energy And Distribution Source for electric for electrical energy conversion – thermal and hydraulic Plan, (Block diagram approach only ), Components of AC transmission and distribution system – line diagram Semi Conductor Devices Doping transistor diode and rectifier (half and full wave rectifier), Amplifier (common emitter

and common amplifier) Measuring Instruments Transducers, Resistance temperature detector, thermocouple and temperature Controller strain gauge – piezo electric transducer. References

1- John Bird," Electrical Circuit theory and Technology ", second edition.

2- John Bird, "BSc. (Hons), CEng, MIEE, FIEIE, CMath FIMA, FCollP,Oxford Amsterdam Boston London, New York Paris.

3- Huge," Electrical Technology ".

First Year - Electrical Technology

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 2 Theoretical 1hr/week Tutorial : 1 hr/week Practical : -hr/week

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Microsoft Office Microsoft word, Microsoft excel, Microsoft power point. (3 hrs)

Introduction to Visual Basic Programming

Menu bar, Tools bar, Project explorer, Tool box, Properties windows, Form, Code, Controls, Command Buttons, Label, Textbox, Pointers, Picture box, frame, Naming Controls, Properties for controls: Height, Width, Left, Top, Font, Forecolor, Backcolor, Name, Caption, Text, and Visible, Events, Saving Visual Basic Project, Examples, Chemical Engineering Applications. (3 hrs)

Mathematics

Arithmetic Operations: +, , *, /, \, mod, ^. (Using Simple Example for each Operation), Logical Operations. AND, OR, NOT. And the Truth Table for each Operation, (Using Simple Example for each Operation), Relational Operation: >, <, >=, <=, <>, =, String Concatenation (&), Operation Precedence. For all arithmetic, logical, relational operators, Print statement and Formatting. Illustrate (colon, comma, and semicolon), Examples: Chemical Engineering Applications (3 hrs)

Built in Functions

Builtin math functions, Abs(x), Int(x), Rnd(x), sgn(x), sqr(x), str(x), val(x), round(x, n), CInt(x),Fix(x), String Functions, InputBox, MsgBox, Examples: Chemical Engineering Applications. (3 hrs)

Selection Structure Single Selection: If/Then structure, Double Selection: If/Then/Else structure, Nested If/Then/Else structure, Select Case Multiple Selection Structure,

Examples: Chemical Engineering Applications. (3 hrs)

Reputation Structure For ... Next Loop, While ... Wend, Do .... While ... Loop, Do ... Loop Until, Exit Do, Exit For

Examples: Chemical Engineering Applications. (2 hrs) Variables Data Types: Boolean, Integer, Long, Single, Double, String, Valid Naming of Variables, Initial

Value for each Type of the Variables (Initial Value for each Data Type), Size of each Variable Type in Bytes, How to Declare Variables. (Dim statement), Using: Dim variable name As Data type, Using Suffix: Integer, Long, Single, Double, String, Constant Variable.

Examples: Chemical Engineering Applications. (6 hrs)

Arrays Introduction: Defining Arrays, Array Declaration Statement, Assigning Values for Arrays (i.e. filling array's element value either by loop or by direct assignment statement), Re Dim Statement, Using Loops with Arrays. (i.e. writing an application on array using loops),Two Dimensional Arrays, Operations on Arrays, Fill Array Elements with Random Numbers using and Function, Sorting, Searching. (i.e. Linear search), Swapping Two Elements.

Examples: Chemical Engineering Applications. (3 hrs)

First Year - Computer Programming(I)

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 4 Theoretical 1hr/week Tutorial 1hr/week Practical 2 hr/week

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Graphics in Visual Basic

Graphics control, Picture box, Image box, Coordinate system, Pixel, Graphics methods (Line, Circle, pset) Examples: Chemical Engineering Applications. (2 hrs)

Graphics in Visual Basic Graphics control, Picture box, Image box, Coordinate system, Pixel, Graphics methods (Line, Circle, pset)

Examples: Chemical Engineering Applications. (2 hrs)

Database Accessing Database, Data Control DAO, ADO, RDO, Visual Basic and Access Connectivity Examples: Chemical Engineering Applications. (2 hrs)

Designing Reports Introduction, Objective, Introduction to Report Designer, Creating Report, Data , Report, Data Environment. Examples: Chemical Engineering Applications. (2 hrs)

Reference 1- Working in Microsoft Office By Ron Mansfield 1996

2- Visual Basic By Abdul Mutalib 3- Programming in VB By: P.K. McBride 4- Mastering in VB By: Evangelos Petroutsos 5- Visual Basic 6 By: Noel Jerke 6- Programming in VB.6 By: Rajendra Salokhe 7- Visual Basic 6 By Gary Cornell 8- Visual Basic 6 By Steve Brown 9- Muvach’s Visual Basic 6 By Muvach

Page 22: Mathematics (Ι) B - University of Technology, Iraq€¦ · Mathematics (Ι) 10 Basic Principles of Chem. Eng. (I) 11 . Chemistry . 12 : Chemistry of Petroleum 13 Chemistry Laboratory

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12 hours Electricity division

12 hours Forming division

12 hours Filing division

12 hours Training carpentry division

12 hours Steel metal forming division

12 hours Casting division

12 hours Lathe division

12 hours Welding division

12 hours Automotive division

First Year - Workshop

Chemical Process Eng. & Oil and Gas Refinery Eng. Branch

Units 4 Theoretical -hr/week Tutorial -hr/week Practical 6hr/week

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1) Psychological construction and its relationship with human rights: the feeling, the unconscious, psychological construction positives. (2 hrs)

2) Human Rights: History, definition, characteristics, goals, human rights violations. (1 hr)

3) Contemporary ArabP

’Ps currents, its position on human rights. (1 hr)

4) Secular: the early stages of itP

’Ps development, disadvantages, her features. (1 hr)

5) How can you balance between civil rights and social. (1 hr) 6) Capitalist and socialist society with human rights. (1 hr) 7) Closed society and an opened society: its position throughout human rights. (1 hr) 8) Theory of the social contract . (3 hrs)

Thomas Hughes, Jan-Jack Rousseau, Volter, Auxt Comte, Max Weber, Montesquieu 9) Relationship of rights to democracy. (1 hr)

10) Relationship of rights to urbanization. (1 hr) 11) Relationship of rights with globalization. (1 hr) 12) Globalization: between rejection and acceptance. (1 hr) 13) How can rooting the values of human rights in : (1 hr)

Arab Culture, in the great cultures

المصادر حقوق االنسان والثقافة الديمقراطية (د. حميد عبد الجبار) -1 حقوق االنسان / تطورها ، مضامينها حمايتها.(د.رياض عزيز صادق) -2 مبادئ وقواعد عامة في حقوق االنسان. (د.صالح حسن مطرود) -3 حقوق االنسان بين االعالنيين االسالمي والعالمي (د.محمد علي ) -4 محاظرات في سياسيات حقوق االنسان (مؤلف جماعي) -5 حقوق االنسان والطفل (د.ماهر صالح الجبوري ) -6 حقوق االنسان واالنتخابات (مركز الحقوق /االمم المتحدة) -7مشكله الحرية /فلسفة معاصرة (د.زكريا ابراهيم ) -8

Second Year - Human Rights

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 1 Theoretical : 1hr/week Tutorial : 1hr/week Practical : -hr/week

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1 - Democracy: definition, a brief history, characteristics advantages of democracy and it P

,Ps

disadvantages. (1hr)

2 - The most important problems facing the implementation of democracy in the Arab-Muslim

world. (1hr)

3 - Relationship awareness in the application of democracy. (1hr)

4 - How can we adapt our culture with the principles of democracy. (1hr)

5 – Democratic between changes and external pressures, A pressure group, the difference between them and the political parties. (1hr)

6 - The advantages of democracy and the disadvantages of secularism and Islam. (1hr)

7 - The role of the middle class in the social and political life. (1hr)

8 - The theory of social determinism in state-building. (1hr)

9- Relationship between democracy and globalization. (1hr)

10- Factors that lie behind the emergence of democracy. (1hr)

11 - Development and democracy. (1hr)

12 - Religion and Democracy. (1hr)

13 –The third way between socialism and capitalism. (1hr)

14 - Reasons for the spread of financial and administrative corruption and how to confront it. (1hr)

15 - The reasons for the collapse of democracy, The relationship between the intellectual and power, The relationship between consciousness and the rooting of democracy. (1hr)

المصادر

هرطقات عن الديمقراطية والعلمانية (.جورج طرابيشي) -1الديمقراطية ،(تشارلز بيمتز) -2نماذج الديمقراطية .(ديفيد هيلد) -3 الديمقراطية وحقوق االنسان (د.محمد علي الشربجي) -4 الديمقراطية وجهات نظر اسالمية. (هاشم مرتضى) -5 مفهومان للديمقراطية.(د.محمد عبد الجبار) -6مستقبل الديمقراطية.(د.ثناءفؤاد عبد هللا) -7

Second Year - Democracy

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 1 Theoretical : 1hr/week Tutorial : 1hr/week Practical : -hr/week

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Partial Differentiation Function of two or more variables, partial derivatives, Directional derivatives, higher order

derivatives, Maxima, minima and saddle point, Lagrange multipliers. (10 hrs) Ordinary differential equations Solution of first order ordinary differential equations, Solution of second order ordinary differential equations, and higher order differential equations. (10 hrs)

Multiple Integrals Double Integral, Area, Volume, Double Integral in polar coordinates, Triple Integral in

rectangular coordinates, physical application of double and triple integration. (10 hrs)

Function and definite Integrals The error function, the gamma function, the beta function, factorial function. (5 hrs)

Infinite Sequences and Series Sequences, Convergence, Geometric series, nth partial sum, tests of convergence, alternating series, power and Taylors series. (6 hrs) Fourier series Periodic functions, Fourier series, Even and odd functions, Half range expansion. (6 hrs) Vectors and Vector functions Products of three vectors, Equations of lines and planes, Vector function and motion (velocity and acceleration). (5 hrs) Matrices Solution of system of linear equations by matrix (Inverse of matrix, Gauss elimination), Rank of matrix, Eigen values and Eigen vectors. (8 hrs)

Reference 1- G. B. Thomas, M. D. Weir and J. R. Hass, "Thommas' Calculus", 12th

2- Howard Anton, "Calculus with Analytical Geometry", (3 Edition.

rd edition), John Wiley & Sons 1988.

Second Year - Mathematics (II)

Chemical Processing Eng. & Petroleum Refinery Eng. and Gas Technology Branch

Units 4 Theoretical : 2hr/week Tutorial : 1hr/week Practical : -hr/week

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Energy Balances Basic concepts and definitions, Forms of energy, First law of thermodynamics, Energy balance on closed and open systems without chemical reaction Reversible processes, and mechanical energy balance equation, Heat capacity (Cp and Cv ),Calculation of enthalpy changes: Enthalpy changes without change of phase , Enthalpy changes with phase transitions, Enthalpy balance on heat exchange unit, Enthalpy changes using steam tables, Energy balances with chemical reactions. (24 hrs)

Simultaneous Material and Energy Balances

Material and energy balances for steady state processes, Heats of solution and mixing, Enthalpy – concentration charts, Partial saturation and humidity, Psychometric (humidity) charts. (20 hrs)

Unsteady State Material and Energy Balances

Representation of a general unsteady-state process, Unsteady-state material balance without generation, Material balance on batch distillation, Unsteady-state chemical reaction, Unsteady-state energy balance. (16 hrs)

Principles of Renewable energy (2 hrs)

Types of Renewable energy (2 hrs) References 1-Himmelblau, D.M., and J.B.Riggs, Basic Principles and Calculations in Chemical Engineering

,7th edition, PrenticeHall Inc., New Jersey, 2004.

2-Felder,R.M.,and R.W.Rousseau,Elementry Principles of Chemical Processes, 3rd edition,

John Wiley, New York, 2005.

3-Bhatt ,B.I, and S.M.Vora, Stoichiometry, 4th edition,Tata Mc-Graw Hill, New Delhi,2004.

4-Williams,E.T.and R.C.Johnson,Stoichiometry for Chemical Engineers, Mc-Graw Hill, New

York,1958.

5-Sinnott,R.K.,Chemical Engineeing Design (Coulson & Richardson’s Chemical Engineering

Series,Vol.6),4th edition ,Elesevier,Amsterdam,2005.

6-Schmidt,A.X.,and H.L.List ,Material and Energy Balances,Prentice-Hall Inc.,New Jersey,1962.

7-Kammermeyer,K.,and J.O.Osburn, Process Calculations, Prentice-Hall Inc.,New Jersey,1956.

Second Year – Basic Principles of Chemical Engineering (II)

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 4 Theoretical 2hr/week Tutorial 1 hr/week Practical - hr/week

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Introduction Definition of a fluid, fluid mechanics, Physical properties of fluids: Density, specific gravity, viscosity, Kinematic viscosity, Newton’s , law of viscosity, surface tension and capillarity, bulk modulus of Elasticity, Pressure, Types of Fluids, Newtonian, non-Newtonian fluids ideal and real fluids. (2 hrs)

Dimensional Analysis Fundamental dimensions, dimensions, Dimensional homogeneity, methods of dimensional analysis, Rayleigh’s method (power series) , Buckingham’s Π method / Theorem

Dimensionless numbers (4 hrs)

Fluid Statics Basic equation of fluid statics, pressure head of liquid, Pressure force on surfaces, Buoyancy Measurement of pressure: (Piezometer, Manometers, types of Manometers, Mechanical

Gauges). (4 hrs) Fluid kinematics

Types of fluid flow (steady and unsteady flows, uniform and non-uniform flows, one, two, and three dimensional flows, Rotational and ir-rotational flows, laminar and turbulent, compressible and incompressible flows), Boundary layer.

- Continuity equation - Momentum equation (2 hrs) Fluid Dynamics

Bernoulli’s equation, Euler’s equation of motion, modified Bernoulli’s equation for real fluid; correction of kinetic energy, correction of energy losses (viscous fluid), work. (4 hrs)

Newtonian’s Fluid (Incompressible flow in Pipe and Channels)

Reynolds experiment , Head losses (skin friction) in circular pipes for laminar flow by Hagen Poiseuille law and fore turbulent flow by Darcy equation, Head losses (form friction) in fittings, sudden expansion or contraction , Velocity distribution for laminar and turbulent flow , Flow in Branch Pipes, Flow in noncircular pipes, Flow in open channels. (6 hrs)

NonNewtonian Fluids in Pipes Definition, types of fluid depended on time, calculation of friction and pressure drop for general time independent in laminar and turbulent flow. (4 hrs)

Flow Measurement (Practical Application of Bernoulli’s Equation)

Pitot tubes, orifice meter, venturi meter, nozzle meter, Rotameters other types of flow meters, Fow in open channels and weirs. (6 hrs)

Pumping of Liquids

Total heads, NPSH, Horse Power and cost consumption, Pumping Efficiencies, Characteristics curves, Types of the pumps, Selection of Pumps, Centrifugal pump relations, homologous centrifugal pump, centrifugal pumps in series and in parallel. (4 hrs)

Second Year - Fluid Flow

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

Units 6 Theoretical 2hr/week Tutorial 1 hr/week Practical 2 hr/week

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Flow of Compressible Fluid

General equation, equation of state, sonic velocity in fluids , Isothermal, Non-isothermal and Adiabatic flow of an ideal gas in horizontal pipe, Converging-diverging nozzle for gas flow, Type of Compressor, Gas compression and compressors work and efficiency.

(8 hrs) Two Phase Flow

Flow regime, Pressure Momentum, and Energy relations, calculation of pressure drop by Lockhart and Martinelli method. (2 hrs)

Liquid Mixing Stirring and mixing, Stirred vessels (power consumption, power curve, scaledup), equipment. (4 hrs)

Motion of Particles in a Fluid

Drag force on a particle, terminal falling velocities , Sedimentation of fine and coarse Particles (4 hrs)

Flow of Fluid through Granular Bed and Packed Columns

Pressure drop in granular beds, packed columns: packings, Pressure drop estimation (Kozeny and Carmen equations) (4 hrs)

Fluidization Minimum fluidization velocity, Pressure, Pressure drop, Geldart Diagram, Ergun equation,bed expansion and transport of particles. (2 hrs)

References

1- “Chemical Engineering” Vol. I and II by Coulson and Richardson; 6th

Butterworth Heinemann, 1999

2- “Fluid Flow for Chemical Engineers”, by F.A. Holland and R. Bragg 2

ed.,

nd Ed. (1995) Elisevier

Ltd.

3- “Chemical Engineering Fluid Mechanics”, by DARBY. R. , M. Dekker 2nd Ed. (2001)

4-“Fluid Mechanics for Chemical Engineers”, by James O. Wilkes, Prentice Hall PTR, New

Jersey, USA, 1999.

5- “Fluid Mechanics for Chemical Engineers”, by De Nevers, N. (1991) Mc Graw Hill, Singapore.

6- “Fluid Mechanics”, by Streeter and Wylie, Mc Graw Hill (1981).

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(A)

Exp. No. Exp. Name.

Exp. No. 1 Calibration of Bourdon Tube Pressure Gauge

Exp. No. 2 Reynolds Experiment

Exp. No. 3 Energy Loss in Pipes

Exp. No. 4 Centrifugal Pump Characteristics

Exp. No. 5 Bernoulli’s Theorem Demonstration

Exp. No. 6 Friction Losses in Piping Systems

Exp. No. 7 Impact of Jet

(B)

Exp. No. Exp. Name.

Exp. No. 1 Discharge through an orifice.

Exp. No. 2 Open channel flow over weir.

Exp. No. 3 Flow through a venture meter.

Exp. No. 4 Fluidization.

Exp. No. 5 Forced vortex.

Exp. No. 6 Flow of compressible fluid.

Exp. No. 7 Gear pump.

Second Year - Fluid Flow Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

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Chemical Kinetic

The rate of chemical reactions, order of reaction and rate constant zero, first, second and third order rate equations, Reversible reactions, Consecutive reactions, Parallel reactions, Determination of the reactions order, , Effect of temperature on reaction rate, Activation energy. (12 hrs)

Catalysis

Reaction of catalyst in homogeneity system, Enzyme reactions and kinetic of reactions. (6 hrs)

Electrochemical cells

Electromotive force (EMF) of a cell, The polarity of electrodes, Electrode potential, The cell reaction and reversible cells, Types of half classificatio EMF, Standard electrode potentials,Thermodynamic data from cell E.M.F.S., Oxidation reduction cells, Concentration cells, ,The temperature dependence of the EMF, Simple applications of EMF measurements, Solubility of sparingly soluble salt, Conductivity measurements . (12 hrs)

Change of state

One component system , Vapor pressure and external pressure Liquid – vapor composition diagram , Liquid - Liquid binary solution mixture , roulettes law for ideal mixture, Non-ideal Liquid mixtures, the principle of distillation . (10 hrs)

Applications Of The Equations Of Ideal Gases

The PVT behavior of pure substances, The virial equation, The ideal gas, The constant volume process, The constant pressure process, The adiabatic process, The polytrophic process. (10 hrs) Heat Effects

Heat capacities of gases as a function of temperature. Solids and liquid, Heat change accompanying phase change, Heat of industrial reactions. (10 hrs)

Reference

1-P.Watkins and j. de paula, "physical chemistry", 8 th ed.(2006). 2-J.M. Smith, H.C. Van Ness., "Introduction to chemical engineering thermodynamics",4th

ed., 1977.

Second Year - Physical Chemistry

Chemical Processing Eng. & Petroleum Oil and Gas Refinery Eng. Branch

Units 5 Theoretical 2hr/week Tutorial 1hr/week Practical 2hr/week

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Exp. No. Exp. Name.

Exp. No. 1 Refractive index.

Exp. No. 2 Viscosity.

Exp. No. 3 Saponfication of acetate ethyl.

Exp. No. 4 Three component system( water, ethanol and ethyl acetate)

Exp. No. 5 Molecular weight determination by victor meyers method.

Exp. No. 6 Calorimeter Constant.

Exp. No. 7 Heat of solution

Exp. No. 8 Surface tension.

Exp. No. 9 Surface chemistry. Adsorption by solid from solution.

Exp. No. 10 Spectrophotometer analysis of kR2RCrR2ROR7R.

Second Year - Physical Chemistry Laboratory

Chemical Processing Eng. & Petroleum Oil and Gas Refinery Eng. Branch

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Starting With Matlab Starting MATLAB, MATLAB windows , Menus and the toolbar , Working in the command window , Arithmetic operations with scalars , Display formats , Elementary math builtin functions, Useful commands for managing variables, Script files and the Editor Debugger,Matlab Help System (2 hrs)

Symbolic Math Symbolic objects, and symbolic expressions, Changing the form of an existing symbolic expression, Solving algebraic equations, Differentiation, Integration , Solving an ordinary

differential equation (3 hrs)

Creating Arrays Creating a one-dimensional array (vector) , Creating a two-dimensional array (matrix) , The transpose operator , Array addressing , Using a colon: in addressing arrays, Adding elements to existing variables, Deleting elements, Built-in functions for handling arrays, Strings and strings as variables. (2 hrs)

Mathematics With Array Addition and subtraction , Array multiplication, Array division , Element-by-element operations ,

Using arrays in MATLAB built-in math functions, Built-in functions for analyzing arrays, Generation of random numbers, Solving Algebraic Equations. (3 hrs)

Polynomials, Curve Fitting, And Interpolation Polynomials , Curve fitting , Interpolation , Extrapolation. (2 hrs) Two-Dimensional Plots The plot command , The f-plot command , Plotting multiple graphs in the same plot ,

Formatting a plot, Plots with logarithmic axes, Plots with error bars, Plots with special graphics , Histograms, Plotting multiple plots on the same page , Multiple figure windows Graphics. (2 hrs)

Using Script Files The MATLAB workspace and the workspace window, Input to a script file , Output commands, The save and load commands, Importing and exporting data. (1 hr) Functions And Function Files Creating a function file, Structure of a function file, Local and global variables , Saving a

function file , Using a user-defined function , Examples of simple user-defined functions , Comparison between script files and function files , Function functions , Sub-functions

(2 hrs) Programming In Matlab Relational and logical operators , Conditional statements, The switch case statement , Loops,

Program Design and Development. (3 hrs) Three-Dimensional Plots Line plots, Mesh and surface plots, Plots with special graphics , The view command.

(2 hrs)

Second Year - Computer Programming (II)

Chemical Processing Eng. & Oil and Gas Refinery Eng . Branch

Units 4 Theoretical 1hr/week Tutorial 1hr/week Practical 2hr/week

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Numerical Analysis Solving an equation with one variable, Finding a minimum or a maximum of a function, Numerical

integration , Ordinary differential equations. (3 hrs)

Solving Chemical Engineering Problems

1- Rudra Pratap: Getting started with MATLAB 7, Oxford Press (Indian edition),2006.

Thermodynamic Applications , Material and Energy Balances, Fluid Flow Applications , Simulation of Chemical Process, Simulation of Chemical Process With Chemical Reaction , Simulation of Separation Processes. (5 hrs)

References

2- Desmond J. Higham and Nicolas J. Higham: Matlab Guide, SIAM, 2000. 3- Duane Hanselman and Bruce Littlefield: Mastering Matlab6: A Comprehensive Tutorial and Reference, Prentice Hall, 2001. 4- Delores M. Etter: Engineering problem solving with Matlab, Prentice Hall,1993. 5- Schilling R. J., Harries S.L., Applied Numerical Methods for Engineers using MATLAB & C, Thomson Books, 2002.

WEB SITES : 1- Documentation from www.Mathworks.com

2- File exchange from www .matlabcentral.com 3- http://www.mathworks.com/access/helpdesk/help/techdoc/learn_matlab/ 4- http://www.mathworks.com/academia/student_center/tutorials/

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Classification of Materials Classification of materials, classification of materials based on structure, advanced materials. (4 hrs) Mechanical Properties of Materials Stress-strain behavior, ductility, brittleness, toughness, modulus of resilience, poison,s ratio, ardness , effect of temperature. (6 hrs)

Atomic structure The structure of atom, atomic bonding, bonding energy and inter-atomic spacing . (6 hrs)

Atomic order in solids Types of atomic or ionic arrangements, crystal structure, lattice, unit cells, metallic crystal structure, crystal systems, crystal direction and crystal planes , diffraction techniques for crystal structure analysis . (8 hrs) Imperfections in solids Point defects, line defects, interfacial imperfections, Macroscopic defects . (6 hrs)

Atomic and ion movements in materials Stability of atoms and ions, mechanisms for diffusion , rate of diffusion (Fick,s first law), factors affecting diffusion ,non-steady state diffusion (Fick,s second law) . (6 hrs)

Thermal and electrical properties of materials

Heat capacity, thermal expansion, thermal conductivity, thermal stresses, electrical conductivity, electron mobility, electrical resistivity of metals . (4 hrs)

Solid solutions and phase diagrams. Basic concepts, solubility and solid solution, phase and phase diagram, unary phase diagram, binary Iso-morphous system, binary eutectic system. (6 hrs)

The Iron-Carbon system The Iron-Iron carbide phase diagram, development of microstructures in Iron-carbon alloys (6 hrs)

Ceramic materials Crystal structure, mechanical properties of ceramic, classification of ceramic materials on the basis of application . (4 hrs)

Composites Material combination, Reinforced composites, structural composites. (4 hrs)

References: 1-Donaled R. Askeland, The science and engineering of materials, international student edition, 2006 . 2-William D. Callister, Jr. , Materials science and engineering, Fifth edition, 2000. 3-Lawrence H. Vanvlack , Elements of materials science and engineering, Fifth edition, 1987.

Second Year - Material Science and Engineering

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 5 Theoretical 2hr/week Tutorial 1 hr/week Practical 2hr/week

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35

(A)

Exp. No. Exp. Name.

Exp. No. 1 Tension test

Exp. No. 2 Hardness Testing

Exp. No. 3 Bending Test

Exp. No. 4 Creep Test

Exp. No. 5 Abrasion Test

Exp. No. 6 Moisture Measurement in Engineering Materials

Exp. No. 7 Properties of Engineering Materials with Regular Shapes

Exp. No. 8 Impact Test

Second Year - Material Science and Engineering Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

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Energy and Fuel Energy and its, Classification in Technology section ,Physical and Chemical classification of fuel, solid fuels (coal),the industrial process on coal to derive different product. (4 hrs)

Petroleum and petroleum products Definition , Origin, Composition, Classification of Petroleum, Petroleum assay. (6 hrs)

PreTreatment of petroleum Dehydration & Desulting of crude petroleum. (2 hrs)

Gaseous Fuels Introduction, Natural gas, Refinery gas, Liquefied petroleum gas, Measurement of calorific

value of fuel gas, Fuel gas cleaning and purification. (2 hrs)

Petroleum Fractions Properties Gasoline, Naphtha, Kerosene, Diesel Fuel, Distillate Fuel oil, residual fuel oil, Lubricating oil, Grease, Wax, Coke (8 hrs)

Combustion Calculations Combustion process, Required air Excess air ,Stack gas analysis and Orsat analysis (4 hrs)

Burners Combustion of solid fuel, Grates, Solid fuel burner, Liquid fuel burner and gas fuel burner

(2 hrs) Furnaces

Furnace types in oil industrial, boilers and steam production that used in different industrial. (2 hrs)

Types Of Energy & Other Types of Energy Kinetic Energy, Potential Energy

Other Types of Energy Mechanical Energy, Chemical Energy, Electrical Energy, Gravitational Energy (2 hrs)

Power Sources: 1-Non-Renewable power sources 2-Renewable Power Sources: Water power (hydropower), Tidal (2 hrs)

References: 1- Nelson, W. L. Petroleum Refinery Engineering, Tata McGraw Hill Publishing Company Limited, 1985. 2- B.K. Bhaskara Rao, “Modern Petroleum Refining Processes” Edn. 3, Oxford & IBH Publishing Company Pvt. Ltd. New Delhi. 3- Gary J., Handework G., “ Petroleum Refining Technology and Economics”,Marcell Dekker Inc. 1984. 4- .Speight,J.G,Handbook of petroleum product analysis, John Willey & Sons,

2002. 5- Gupta,O.P.,Elements of Fuels,Furnaces & Refractories, Khanna publishers,5th ed,2008.

Second Year - Fuel's Technology

Chemical Processing Eng. Branch

Units 3 Theoretical 1hr/week Tutorial 1 hr/week Practical 2 hr/week

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37

Petroleum Analysis: Definitions ,Historical perspective ,Modern perspective ,Analysis and specification, Sampling ,Measurement. (2 hrs)

Petroleum and Petroleum Product: Petroleum: Definition, Petroleum assay(carbon residue , asphaltene content) Density ,distillation ,Light hydrocarbon, salt content , Sulfur content, Viscosity and pour point.

(2 hrs) Petroleum Product: Refinery gases (2 hrs) Naphtha[Production and Properties ,Test method(Aniline point and Mixed aniline point, Density ,Flash point, Volatility ,Evaporation Rate)]. (2 hrs) Gasoline:[Production and Properties ,Test method(Additives, Combustio Characteristic ,Flash point and Fire point, Oxygenates ,Volatility)] (2 hrs) Aviation Fuel:[Production and Properties ,Test method(Acidity ,Additives, Calorific value ,Density , Flash point , Freezing point, Pour point ,thermal stability). (2 hrs) Kerosene:[Production and Properties, Test method (Acidity ,Calorific value , Freezing point , Flash point , Smoke point, Viscosity, Water and Sediment)] . (2 hrs) Diesel fuel: [Production and Properties , Test method ( Acidity , Ash , Carbon residue , Cetane number and Cetane index ,Cloud point, Diesel index , Pour point and Volatility)]. (2 hrs) Distillate Fuel Oil : [Production and Properties ,Test method( Acidity ,Ash content, Cloud point , Flash point , Pour point, Volatility ,Viscosity )]. (2 hrs) Residual Fuel Oil[Production and Properties, Test method(Ash, Asphaltene content, Carbon residue, Element analysis, Flash point, Pour point)]. (2 hrs) Mineral Oil:[Production and Properties ,Test method(acidity, aniline Point, Asphaltene content , Carbonizabale substances ,Carbon residue , Interfacial tension ,iodine value , and smoke point)] (2 hrs) Lubricating oil ( production and properties , test method ,ash ,asphaltene content ,Carbonizabale substances, Color , Flash point , Viscosity)]. (2 hrs) Grease: [Production and Properties, Test method (Acidity , Anticorrosion properties , Dropping point , Oil separation , Penetration and Viscosity) (2 hrs) Wax:[Production and Properties, Test method( appearance ,barrier properties , color , hardness ,odor and taste , slip properties , strength)] (2 hrs) Asphalt[ Production and Properties, Test method (acid number , breaking point , carbon residue , flash point , penetration)]. (1 hr) Coke, [Production and Properties, Test method (ash ,calorific value , dust control material , proximate analysis , sulfur , volatile matter and water)] . (1 hr) References

1- Speight,J.G,Handbook of petroleum product analysis, John Willey&Sons,2002. 2- Speight,J.G, and Ozum,B; Petroleum Refinery Processes, Macel Dekker, New York,2002. 3- Speight,J.G, The chemistry and Technology of Petroleum.3P

rdP Edition .Marcel Dekker ,New

York,1999. 4-Institute of Petroleum.2001.IP Standard Methods. The Institute of Petroleum ,London, UK.

Second Year - Properties of Petroleum Products

Oil and Gas Refinery Eng Branch

Units 3 Theoretical 1hr/week Tutorial 1 hr/week Practical 2hr/week

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38

Exp. No. Exp. Name.

Exp. No. 1 ASTM distillation

Exp. No. 2 Viscosity

Exp. No. 3 Ash content

Exp. No. 4 Flash and fire point

Exp. No. 5 Gum Cotent

Exp. No. 6 Carbon residue

Exp. No. 7 Density and specific

Exp. No. 8 Salt content in crude oil

Second Year – Fuel's Technology Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

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39

Introduction: statistics, population & sample, descriptive and inductive stat. & graphical representation of data Frequency distribution table, raw data, arrays & types of frequencies Graphical representation of frequency distribution table Measures of central tendency Measures of dispersion Curve fitting, least squares method, straight line relation, straight line forms. Polynomial regression, variance and correlation coefficient Multiple and partial correlation: regression equation, normal equations for the least square regression, the coefficient for multiple correlation, relationship between multiple and partial correlations Probability distribution, continuous & discrete probability dist., normal dist., table of area under normal dist. The binomial distribution, the Possion probability distribution, approximation of standard distributions

The chisquare test, confidence intervals, degree of significant, test of hypothesis Chisquare test for goodnesss of fit of probability distributions, test of independence Comparing three or more means ( oneway analysis of variance ) (ANOVA), requirements of ANOVA test, ANOVA Ftest statistic, decision rule in ANOVA test Measurements: absolute & relative meas., dependent & independent Variables, classification of measurements Errors, types, estimation & propagation of errors . Measuring instruments, classification of methods for measuring pressure. & temp. level & velocity Pressure measurements by balancing against a column of liquid of a known density, and against the stress in an elastic medium Temp. meas., expansion thermometers, expansion of solids, liquids & gases Electrical methods, thermocouples, types, radiation pyrometers Measurement of level, direct methods, pressure operated methods Measurements of flow, quantity meters for liquids Quantity meters for gas, flowmeters for liquids, differential pressure methods

References 1-Murry R. Spiegel,Statistics, Mc Grow-Hill international book company 1st addition 2-Michael Sullivan III,Statistics informed decision using data 3rd addition ,pearson education international 2010. 3-Jones’ instrument technology. 4-Butterworth and co. (publishers) 2nd addition 1987.

Second Year - Statistics and Measurements

Chemical Processing Eng. & Oil and Gas Refinery Eng Branch

Units 3 Theoretical 1hr/week Tutorial 1hr/week Practical 2hr/week

(1hr)

(1hr)

(2hrs) (1hr) (1hr) (1hr)

(2hrs)

(2hrs)

(2hrs)

(2hrs) (1hr) (2hrs)

(2hrs)

(1hr) (2hrs)

(2hrs)

(2hrs) (1hr) (1hr) (2hrs) (1hr)

Page 40: Mathematics (Ι) B - University of Technology, Iraq€¦ · Mathematics (Ι) 10 Basic Principles of Chem. Eng. (I) 11 . Chemistry . 12 : Chemistry of Petroleum 13 Chemistry Laboratory

40

1st law and other basic concepts Review on 1st law and applications

(2 hrs) Volumetric properties of pure fluids Review on virile equation of state, cubic equation of state, generalized

correlations for gases and for liquids. (4 hrs)

The 2nd law of thermodynamics

Review on the 2nd law and Carnot heat engine, entropy balance for open system, calculation of ideal work, lost work.

(4 hrs)

Thermodynamic properties of fluids

Review on the property relations ( residual properties, two phase systems, thermodynamic diagrams and tables, generalized property correlations for gases.

(4 hrs)

Applications of thermodynamics to flow processes

Duct flow of compressible fluids, pipe flow, nozzles, throttling process, turbines, compression processes compressors, ejectors.

(6 hrs)

Production of power from heat

The steam power plant, Rankin cycle, the regenerative cycle, internal combustion engines Otto engine, diesel engine, gas turbine engine, jet engine.

(6 hrs)

Refrigeration and liquefaction

The Carnot refrigerator, the vapor compression cycle, the choice of refrigerant, absorption refrigeration, the heat pump, liquefaction processes.

(6 hrs)

Thermodynamic analysis of processes

Second law relation for steady state flow processes, calculation of ideal work, thermodynamic analysis of steady state flow processes.

(6 hrs)

Vapor\liquid equilibrium; introduction

The nature of equilibrium, the phase rule, duhems theorem, diagrams for vapor liquid equilibrium, simple models for vL equilibrium: Raults law, dew point and bubble point calculations, Henrys law, VLE by modified raults law, VLE from K value correlations, flash calculations.

(6 hrs)

Solution thermodynamics: theory

Fundamental property relations, the chemical potential and phase equilibrium, partial properties, ideal gas mixtures, fugacity and fugacity coefficient, the fundamental residual property relations, fugacity coefficient from the virial equation of state, generalized correlations for fugacity coefficient, the ideal solutions, Lewis-Randall rule, excess properties, the nature of excess properties.

(6 hrs)

Chemical Reaction equilibrium

The reaction coordinate, standard Gibbs energy change and equilibrium constant, effect of temperature on equilibrium constant, evaluation of equilibrium constant, liquid phase reactions, equilibrium conversion for singlereactions.

(6 hrs)

Third Year - Thermodynamics

Chemical Processing Eng. & Oil and Gas Refinery Eng, Branch

Units 5 Theoretical : 2hr/week Tutorial : 1hr/week Practical : 2hr/week

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41

Renewable energy Definitions and element of energy conservation, Solar energy, Wind energy, Energy efficiency as an investment in producing energy services.

References 1- J. M. Smith,H.C.Van Ness, Introduction to chemical engineering thermodynamics, 6th edition (International Edition), Mc-Graw Hall, 2008.” 2- K.V.Narayanan, Atext book of chemical engineering thermodynamics, prentice Hall of India, New Delhi, 2011. 3- B.G.Kyle, Chemical and process thermodynamics ,(3rd Edition), prentice Hall Inc.New Jersey, 1984. 4- J. Rayner, Basic engineering thermodynamics in SI units, printed in great Britain,1971.

(4 hrs)

Page 42: Mathematics (Ι) B - University of Technology, Iraq€¦ · Mathematics (Ι) 10 Basic Principles of Chem. Eng. (I) 11 . Chemistry . 12 : Chemistry of Petroleum 13 Chemistry Laboratory

42

Exp. No. Exp. Name.

Exp. No. 1 Joul-Thomson experiment.

Exp. No. 2 Compressibility factor and 2nd virial coefficient.

Exp. No. 3 Boyle law experiment.

Exp. No. 4 Refrigeration cycle.

Exp. No. 5 Steam power plant.

Exp. No. 6 Vapor – liquid equilibrium.

Exp. No. 7 Chemical reaction equilibrium.

Exp. No. 8 Ideal gas processes.

Exp. No. 9 Calculation of gamma (ratio of Cp to Cv).

Exp. No. 10 Calculation of dryness fraction.

Third Year – Thermodynamics Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng. Branch

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43

Reviews solution methods of 1P

stP and 2 P

ndP ordinary differential equations (linear and

nonlinear, homogeneous, …etc). (6 hrs)

Mathematical Statement of the Problem Representation of the problem, Absorption with chemical reaction, Reaction in a spherical and cylindrical catalyst, Radial heat transfer through a cylindrical conductor, Simultaneous diffusion and chemical reaction in a tubular reactor. (9 hrs)

Solution by Series

Infinite series by Taylor theorem, Method of Frobenius (Case I, II, IIIa, and IIIb), Bessels’s and Modified Bessel’s Equation, Properties of Bessel Functions, Applications in chemical engineering ,Tubular Gas Preheater, Reaction in axisymmetric Spherical and Cylindrical pellets. (15 hrs)

Laplace Transformation

Definition of Laplace Transformation, Inverse Transform, Properties of the Laplace Transformation, The Step Functions, Convolution, Inversion by Elementary Integration, Inversion by Residual Method, Applications in Chemical Engineering. (10 hrs)

Partial Differential Equations

Interpretation of Partial Derivatives, Formulating of Partial Derivatives, Typed of boundary Conditions, Partial Solutions of Partial Differential Equations, Combination of Variables Method, Separation of Variables Method, Laplace Method. (10 hrs)

Finite Differences

Nonlinear mathematics for 1P

stP & 2P

ndP order ordinary differential equations, Symbolic Operators,

Backward Difference Operator, Forward Difference Operator, Central Difference Operator and The Average Operator, Difference Equation and Their Solutions, Interpolations of Equally Spaced Points ,Interpolations of Equally Spaced Points ,Applications in Finite Difference Equation, Linear Finite Difference Equations, NonLinear Finite Difference Equations and Their Solutions. (10 hrs)

References

1- Jenson and Jeffreys,"Mathematical Methods in Chemical Engineering", (International Edition), Prentice Hall, 2001.”

2- W. Bequette, "Process dynamics ,Modeling ,Analysis and Simulation" (3 P

rdP edit), John

Wiley & Sons 2006.

Third Year - Applied Mathematics

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 4 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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44

Mass Transfer Fundamentals Steady State mass transfer .Diffusion in binary and multicomponent gases. Diffusion in binary and multicomponent Liquids. Convective mass transfer .Mass transfer coefficients .Two film theory (12 hrs) Boundary Layer

Boundary layer in laminar and turbulent flow, boundary layer in laminar sub layer, transition layer. Velocity distribution on surfaces and pipes, momentum ,heat and mass transfer molecular diffusion. Eddy transfer (8 hrs)

Methods of gas-liquid separation (Absorption & Stripping )

Determination of interfacial mole fractions. Individual and overall mass transfer coefficients. Single stage absorption, multistage absorption .Finding number of stages graphically and through use of correlations for absorption and stripping. Design of packed beds for dilute and concentrated solutions. Finding number of transfer units (16 hrs)

Binary Distillation

Introduction, (T – X – Y) and (XY) equilibrium curves. Flash or equilibrium distillation for binary and multicomponent mixtures. Distillation with reflux using MckabeThiel .Sorel method to find number of stages .Fensk's equation to find minimum reflux ratio and minimum theoretical stages. Column efficiency Multicomponent differential distillation. (12 hrs)

Multi component distillation

Dew and Bubble points calculation methods. Multicomponent equilibrium relationships. Minimum reflux and minimum number of stages. (12 hrs)

References

1- Coulson and RichardsonP

,Ps ," Chemical Engineering", volume 1, 6P

thP Edition, (International

Edition), Butterworth-Heinemann, 1999. 2- Coulson and RichardsonP

,Ps," Chemical Engineering", volume 2, 5P

thP Edition, (International

Edition), Butterworth-Heinemann, 2002. 3- R.E. Treybal," Mass transfer operations", (3P

rdP edit), McGraw Hill-2003.

Third Year - Mass Transfer

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 5 Theoretical 2hr/week Tutorial 1hr/week Practical 3hr/week

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45

(A)

Exp. No. Exp. Name.

Exp. No. 1 Fluid Mechanics of Packed Beds.

Exp. No. 2 Sieve Analysis.

Exp. No. 3 Liquid – liquid Diffusion.

(B)

Exp. No. Exp. Name.

Exp. No. 1 Gas – solid fluidization

Exp. No. 2 Absorption

Exp. No. 3 Batch distillation column

Third Year - Unit Operation / Mass Transfer Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

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46

Introduction Irreversible and reversible reactions, limiting reactant Stoichiometric coefficients , conversion , yield , selectivity , reaction rate law ,Reaction rate constant. (6 hrs)

Types of Reactors Batch reactor , semi – batch reactor , continuous flow reactors( i.e. CSTR, PFR) , comparison of batch and continuous (2 hrs) Batch reactors

Design equation , reaction time , constant volume and constant pressure , batch reactor , isothermal and non-isothermal operations ( adiabatic and non adiabatic ) , Optimal performance for maximum production rate (2 hrs)

Semi – Batch Reactors

Advantages and disadvantages , design equation . (12 hrs) Continuous Stirred Tank Reactors

Design equation for isothermal operation , constant – density and variable – density systems . CSTRs in Parallel and in series , Graphical method for multistage CSTR (12 hrs)

Tubular Reactors

Design equation for isothermal operation ,residence time , number of tubes , space velocity , Pressure drop , recycle operation of a . PFR . (12 hrs)

Multiple Reactions Operation in parallel and in series for single and multiple reactions to obtain maximum amount of desired product . (8 hrs) Design Of Industrial Reactors

Design considerations, steps of design , applications . (6 hrs) Application Of Renewable Energy In Reaction Engineering

Photochemistry, Fundamental parameters in photo catalysis, Water decant animation by solar detoxification, Types of solar reactor, Design equation of catalytic solar reactor. (4 hrs)

References 1- Ronald W. Missen et al., (1999), "Introduction to chemical reaction engineering and kinetics", 1P

stP edition, John Wiely & Sons, (USA).

2- J.M. Smith (1981), "Chemical engineering kinetics", 3P

rdP edition, McGrowHill, Singapore.

3- H. Scott. Fogler (2006), “ Elements of Chemical Reaction Engineering”, 3P

rdP edition,

PrenticeHall of India, New Delhi 4 -Octave Levenspiel (1999), “ Chemical Reactor Engineering” , 3P

rdP edition, John Wiely & Sons,

(USA).

Third Year - Reactor Design

Chemical Processing Eng.

Units 4 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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47

Introduction Stoichiometry, single reaction (reversible and nonreversible), conversion, yield, activation energy, reaction rate law, rate constant, order of reaction, elementary reaction, Arrhenius equation, Vant Hoff. equation. (6 hrs)

Complex reactions Parallel reactions, series reactions, selectivity, product distribution. (2 hrs) Type of reactors Batch reactors, continuous flow reactors (i.e., CSTR, fixed bed reactor, slurry reactor). (2 hrs) Batch reactor

Design equation for isothermal and non-isothermal operation, maximum production rate. (12 hrs)

Fixed-bed reactor Design equation for isothermal and non-isothermal operation, space time, space velocity, weight of catalyst, number of tubes. (12 hrs)

Continuous stirred tank reactor

Design equation for isothermal and non-isothermal operation, space time, space velocity, optimum operating conditions. (12 hrs)

Slurry Reactor Introduction, rate law, controlling step. (8 hrs)

Industrial Study Cases of Reaction Kinetics Cracking of ethane in fixed bed reactor, hydrogenation of oil in batch reactor. (6 hrs) Application of Renewable Energy in Reaction Engineering Photochemistry, Fundamental parameters in photo catalysis, Water decant animation by solar detoxification, Types of solar reactor, Design equation of catalytic solar reactor. (4 hrs)

References 1- Ronald W. Missen et al., (1999), "Introduction to chemical reaction engineering and kinetics", 1 P

stP

edition, John wiely & Sons, (USA). 2- J.M. Smith (1981), "Chemical engineering kinetics", 3P

rdP edition, Mc Grow Hill, Singapore.

3-H. Scott. Fogler (2006), “ Elements of Chemical Reaction Engineering”, 3 P

rdP edition, PrenticeHall

of India, New Delhi 4- James G. Speight and Baki Ozum, (2002) “ Petroleum Refinery Processes” 1P

stP edition, Marcel

Decker Inc., (USA)

Third Year - Reactor Design

Oil and Gas Refinery Eng .Branch

Units 4 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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48

Modes of Heat Transfer Conduction, Convection and Radiation. (2 hrs) Steady State Heat Conduction in One Dimension

Plane wall, radial systems, heat source systems, Boundary surrounded by fluids, overall heat transfer coefficient, extended surface, conduction convection systems and fins.

(14 hrs) Principles of Convection

Transport equations, Fluid mechanism aspect of convection, laminar boundary layer, Thermal boundary layer, Empirical and practical relations for pipe and tube flow and flow normal to single and tube banks.

(10 hrs) Heat Exchangers Various types and their general characteristics, fouling factor, Heat exchangers mean temperature differences and Co-current and countercurrent flow. (10 hrs) Shell and Tube Exchanger Types and various specifications, design calculations by conventional and by effectiveness (NTU) methods and optimum design calculation. (6 hrs) Condensation and Boiling Heat Transfer Condensation of single vapors, Design calculations for condenser, Pool and flow boiling. (4 hrs) Radiation and Furnace design Radiation properties, shape factor, heat exchange for non black bodies, parallel planes, shields, gas tradition. (4 hrs) Unsteady State Heat Transfer Temperature as a function of time, lumped capacity system, quenching of small bodies and

heating of tank (6 hrs) Renewable Energy

Solar radiation, Solar water heater, Solar air heaters , Heat exchangers for ocean thermalenergy, Heat storage and transmits. (4 hrs)

References

1- J.P. Holman," Heat Transfer", 9th edition. 2- P.Frank Incropera , P .David Dewitt," Fundamentals of Heat and Mass Transfer", 5th Edition .

Third Year - Heat Transfer

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 5 Theoretical 2hr/week Tutorial 1hr/week Practical 3hr/week

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49

(A)

Exp. No. Exp. Name.

Exp. No. 1 Conductive Heat Transfer in Steady State.

Exp. No. 2 Coil heat Exchanger.

Exp. No. 3 Determination of overall heat transfer coefficient on air velocity

(B)

Exp. No. Exp. Name.

Exp. No. 1 Preference of cooling tower

Exp. No. 2 Graphite heat exchanger

Exp. No. 3 Extended surface

Third Year - Unit Operation / Heat Transfer Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Page 50: Mathematics (Ι) B - University of Technology, Iraq€¦ · Mathematics (Ι) 10 Basic Principles of Chem. Eng. (I) 11 . Chemistry . 12 : Chemistry of Petroleum 13 Chemistry Laboratory

50

Part A-Equipment Design Process planning

Introduction, Nature of design ,the organization of a chemical engineering projects Scheduling .Standards and codes. Flow sheet design, flow sheet types and designation .Block diagram .Process flow sheet .Piping and instrumentation diagram .Utilities, Computer aided drafting ,process simulation programs .Layout and plot plan .Project evaluation and cost estimation (6 hrs)

Piping network and Pumps Valves selection . Piping design standards and codes . Pipe size selection .Mechanical design of piping system. Pump type, pump specifications, and pump data sheet (4 hrs)

Vessels and tanks

Types of vessels. Criteria in vessel design ,stress considerations . Materials of construction commonly used in vessels tanks. Design of tall vertical vessels . Pressure vessels Design. Vessels supports and foundations (4 hrs)

Solid Handling

Screening Classification with Streams of Air or Water Air Classifiers . Size Reduction . Equipment for Size Reduction Particle Size Enlargement Extrusion Processes (4 hrs)

Heat Transfer Equipments Heat exchanger types and applications. Basic design procedure and theory. Overall heat transfer coefficient. Heat exchanger data sheet. Furnaces convection and radiation zone. Steam boilers (6 hrs) Mass Transfer Equipments Columns types . Plate Types. Packing types . Pressure drops in columns . Column data sheets (6 hrs) Part B-Equipment Design With Computer Aided Design

Applied Design for Pressure vessels ,pumps and compressors flash drum, gas-liquid separator, liquid-liquid separator, gas movers and compressors manually and with computer aided (10 hrs)

Applied Design for heat equipments ( shell And tube heat exchanger, plate heat exchanger , coil type exchanger, condenser, vaporizer, air cooler …….etc ) manually and with computer aided

(10 hrs) Applied Design for mass transfer equipments ( distillation column, absorber column, leaching equipment, scrubber …………..etc) manually and with computer aided (10 hrs)

References 1- G.Tower and R. Sinnott, "Chemical Engineering Design " ,2nd

2- M.Peters, D. Timmerhaus and R. West ,"Plant Design and Economics for Chemical Engineering", 5 edition, 2013 ,Elesvier.

th

3- A.Coker,"Luwdwigs Applied Process Design for Chemical and Petrochemical Engineers",4

edition, 2005, McGraw – Hill.

th

edition,vol.1&2,2007, Elesvier.

Third Year - Equipment Design

Chemical Processing Eng. Branch

Units 5 Theoretical 2hr/week Tutorial 1hr/week Practical 2hr/week

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51

Part A-Equipment Design Process planning: Introduction, Nature of design ,the organization of a chemical engineering projects Scheduling

.Standards and codes. Flow sheet design, flow sheet types and designation .Block diagram

.Process flow sheet .Piping and instrumentation diagram .Utilities, Computer aided drafting ,process simulation programs .Layout and plot plan .Project evaluation and cost estimation

(6 hrs)

Piping network and Pumps Valves selection . Piping design standards and codes . Pipe size selection .Mechanical design of piping system. Pump type, pump specifications, and pump data sheet (4 hrs) Gas-Gas separation (adsorption, membrane …….etc); Solid-Solid separation ;Liquid-Solid Separation (4 hrs)

Solid Handling Screening Classification with Streams of Air or Water Air Classifiers . Size Reduction. Equipment for Size Reduction Particle Size Enlargement Extrusion Processes (4 hrs)

Heat Transfer Equipments

Heat exchanger types and applications. Basic design procedure and theory. Overall heat transfer coefficient. Heat exchanger data sheet. Furnaces convection and radiation zone. Steam boilers (6 hrs)

Mass Transfer Equipments Columns types . Plate Types. Packing types . Pressure drops in columns . Column data sheets (6 hrs)

Part B-Equipment Design With Computer Aided Design

Applied Design for Pressure vessels ,pumps and compressors flash drum, gas-liquid separator, liquid-liquid separator, gas movers and compressors manually and with computer aided (12 hrs)

Applied Design for heat equipments (shell And tube heat exchanger, plate heat exchanger , coil

type exchanger, condenser, vaporizer, air cooler …….etc) manually and with computer aided (12 hrs)

Applied Design for mass transfer equipments (distillation column, absorber column, leaching equipment, scrubber…………..etc) manually and with computer aided (6 hrs)

References 4- G.Tower and R. Sinnott, "Chemical Engineering Design " ,2nd

5- M.Peters, D. Timmerhaus and R. West ,"Plant Design and Economics for Chemical Engineering", 5 edition, 2013 ,Elesvier.

th

6- A.Coker,"Luwdwigs Applied Process Design for Chemical and Petrochemical Engineers",4

edition, 2005, McGraw – Hill.

th

edition,vol.1&2,2007, Elesvier.

Third Year - Equipment Design

Oil and Gas Refinery Eng .Branch

Units 5 Theoretical 2hr/week Tutorial 1hr/week Practical 2hr/week

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52

Roo Finding Bisection method , Newton's method , Secant method, Roots of polynomials (4 hrs)

Interpolation and Approximation (Curve Fitting) Lagrang form of the interpolation polynomial, Piecewise linear interpolation, Cubic spline interpolation, Regression (6 hrs)

Numerical Integration Equally spaced base points, Newton cotes closed integration formulas, Newton cotes open

integration formulas, Numerical Integration with in-equally spaced base points, Orthogonal polynomials, Numerical differentiation (8 hrs)

System of Equations

Elementary transformation of matrix, Gaussian elimination, Gauss-jordan elimination, Jacobi iterative method, Newton-raphson iteration for nonlinear equations (6 hrs)

Approximation of Solution Ordinary Differential Equation Solution of first-order ordinary differential equations, Taylor's methods, Eular method, Runge- Kutta methods, Simultaneous ordinary differential equations,Predictor –corrector methods

(6 hrs) Reference

Applied Numerical methods

Third Year - Numerical analysis

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 3 Theoretical 2hr/week Tutorial 1hr/week Practical 2hr/week

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53

Introduction, definition. (4 hrs) Enzymes. Classification of enzyme, the role of enzyme in biological reactors, enzyme kinetics (Michaelies- Menten and Briggs –Haldane model), evaluation of kinetic parameters. (6 hrs)

Enzyme reactor (Bioreactor) with simple kinetics. Batch or plug – flow bioreactor, Continuous stirred –tank bioreactor (3 hrs) Effect of mass transfer resistance in enzyme reactor. External mass transfer, Internal mass transfer. (2 hrs)

Fermenters. Classical growth curve (biocell growth), Deep tank fermenter, Type of aerobic fermenter designs, Mass transfer in aerobic fermenter and oxygen through gas –liquid interface. (4 hrs)

Cell Kinetics and Fermenrer Design Batch fermenter, Continuous fermenter, Multiple fermenter connected in serie (6 hrs)

Heat Transfer in biological reactor. Sterilization. (2 hrs)

Waste water treatment.

Aerobic biological treatment processes (2 hrs)

Antibiotics Production. (1hr)

Renewable Energy, Definitions. Biomass, Biogas, Bioethanol, Anaerobic Fermentation Processes, Acetone – Butanol (From corn starch), Citric acid (From sugar beet), Biocell growth (4hrs)

References 1-Rajiv Dutta, " Fundamentals of Biochemical Engineering", Any Books, Iindia, 2007. 2-Nukesh Doble , " Biochemical Engineering" , by Prentice-Hall of India private limited ,New Delhi, 2007. 3 - James E.Bailey , David F. Oils, "Biochemical Engineering Fundamentals",2P

ndP ,1986.

4 –Ronald W. Missen; charles A. Mims ; Bradley A.saville (1999),INTRODUCTION TO CHEMICAL REACTION ENGINEERING AND KINETICS,1st edition ,John Wilely and Sons Inc.,USA.

Third Year - Bio Chemical Eng.

Chemical Processing Eng. Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction to particles technology What is particle technology, Definitions of size, shape, sampling, Methods of measurement and particle size distribution: (Microscopic analysis , Sieving Sedimentation , Electronic particle counters , Laser diffraction methods), Methods of particles size reduction: (Precipitation method , Mechanical process). (15 hrs)

Nanotechnology Definition of nanotechnology, preparation, properties and behavior of nanomaterials, Characteristic methods of nanoparticles: (SEM ,TEM ,XRD ,XRF, AFM ,IR ,UV), Application of particles and nanoparticles in chemical engineering. (15 hrs)

References

1- Martin Rhodes ,” Particle technology “,2009.

2- Henrik Buas , “Introduction to nanotechnology” ,2004.

Third Year - Particles & Nano Techonlogy

Chemical Processing Eng. Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction (2 hrs) Chemical process industries

Basic Petrochemical Materials low Olefins: steam Cracking processes, Cooling, Purification Processes, Compression, Separation operations, Energy system, Diolefin: Sources of diolefins, Butadiene Separation, Isobutylene production, Conversion process for production of diolefins, Higher Olefins: production methods of higher olefins, Linear: Alkyl benzene Complex, Aromatics: Basic materials, Aromatic Sources, Separation of benzene Toluene Xylene, Syntheses gas:H2

1- Polymers: (6 hrs)

production: Steam reforming, Partial Oxidation (8 hrs)

Intermediate Petrochemic.als:

Methanol, Ethylene Oxide, Acetic acid, Ethanolamine, Vinyl chloride, Ethylene glycol , Acrylonitrile, Adipic Acid, Methyl Tetra butyl ether, Ethyl benzene, Styrene, Phenol, Nitrobenzene, Cyclohexane, Benzoic acid, Terephthalic acid. (8 hrs)

LDPE, HDPE, PP, PVC,PS 2- Synthetic Fibers (3 hrs) 3- Petrochemical Complexes (3 hrs)

References

1- Shreve's Chemical Process Industries ,5th edition,1988 2- KikOthmer, Encyclopedia of chemical technology, 3th edition,1984. 3- Mcletta, Encyclopedia of chemical processing and design, 1987 4- Ullmans' , Encyclopedia of technology ,1987

Third Year - Petrochemical Industries

Chemical Processing Eng. Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction Raw material, characterization (1 hr)

Primary Petrochemicals Olefins, Diolefins, Higher Olefins, LAB, Aromatics, separation Aromatics, Syn gas, H2 production,

steam reforming ,PO (6 hrs)

Intermediate and derivatives Syn gas derivatives: Methanol, Acetic acid. (2 hrs)

Ethylene derivatives

Vinyl chloride, Ethanol, Ethylene Oxide Ethylene glycol, Mono ethanol amine, DEA&TEA (4 hrs) Propylene derivatives Acrylonitrile, isoprene (2 hrs) Derivatives of C4 hydrocarbon Separation of C4

1. Shreve's Chemical Process Industries ,5th edition,1988

HCS,MTBE (2 hrs) Benzene derivatives Ethyl benzene, styrene, nitrobenzene, aniline, cyclohexane, cumene, Phenol, acetone, adipic acid (4 hrs) Toluene derivatives Benzoic acid (1 hr) Xylene derivatives Terephthalic acid (1 hr)

End Products polymers: LDPE, HDPE, PVC, PP, PS, Fibers, Polyester, Nylon6, Nylon66, Acrylic fibers(6 hrs)

Petrochemical complex (1 hr)

References

2. KikOthmer, Encyclopedia of chemical technology, 3th edition,1984. 3. Mcletta, Encyclopedia of chemical processing and design, 1987 4. Ullmans' , Encyclopedia of technology ,1987

Third Year - Chemicals from Petroleum

Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Scope and History of Combustion: The nature of combustion, Historical perspective of fuels, Historical perspective of combustion

technology (lighting /steam boilers/ internal –combustion engines/compression ignition engines/gas turbines/rocket engines). (2 hrs)

Combustion of Gaseous and Vapourized Fuels Gas –fired furnace combustion

Furnaces and tubular furnace, energy balance and furnace efficiency ( Furnace efficiency and heat loss calculations), burners types, radiation and convection rooms in furnace, furnace wall layers and refractories, chimney height calculation, tube layers in furnaces.

Flames: First law combustion calculations (adiabatic flame temperature), Laminar premixed flames: (effect of stoichiometry on laminar burning velocity /effect of reactant pressure and temperature on laminar burning velocity/stabilization of a premixed flame), laminar flame theory(laminar burning velocity theory /simplified laminar flame model), diffusion flames, combustion zones and temperature profiles, flammability limits, flame stability, flame and combustion speed. (16 hrs)

Combustion of Liquid Fuels Spray Formation And Droplet Behavior Spray formation, size distributions, fuel injectors, spray dynamics (diesel spray dynamics, single

–droplet dynamics), vaporization of single droplets.

Oil –Fired Furnaces Combustion Gas turbine sprays combustion, Gas turbine operating parameters, combustor design, combustion rate, Liner heat transfer.

Direct –Injection Engine Combustion introduction to diesel engine combustion, fuel injection, combustion rates (10 hrs)

Combustion of Solid Fuels Solid Fuel Combustion Mechanisms solid fuel, drying of solid fuels, devolatilization of solid fuels.

(2 hrs) References: 1- Gary L.borman,Combustion Engineering,1998 by Mc Grawhill

2- Stephen R.turns, An introduction to Combustion, 2000 by Mc Grawhill. 3- F .ElMahallawy and S.ElDin Habik ," Fundamentals and Technology of Combustion",2002

by Elsevier Science . 4- W.Francis and M.C.Peters, 1980, Fuels and Fuels Technology 5- Charles E.Baukal,JR.Robert E.Schwartz,P.E,The John Zink Combustion Hand Book,2000,

London, New York Washington D.C.

Third Year - Combustion Eng.

Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Fluid Flow Theory Hydrocarbon Liquid Flow

(Press. drop, type of flow, calculation of pipe diameter and line capacity, complex liq.

Gathering, systems, flow splitting).

Hydrocarbon Gas Flow (Principles, sizing a line based on velocity, static press. (Head) in flow line, complex flow

system, single phase vertical gas flow).

Tow Phase Flow (Importance of two phase flow, two phase flow and related dimensionless numbers, vertical

and horizontal two phase flow regimes, correlations, two phase flow in grid system).

Pipe Diameter (Hydraulic and economic diameter roughly).

Unsteady State Flow (Transient pipeline flow, blow down and purge, pressure surges on closing a valve, pressure

surges on closing valve, press. testing). (12 hrs)

Transportation Sea transportation, Railway and Road transportation, Pipeline, Gathering system, Pump and compressor stations, (Power sources, type of pumps, instrumentation and control), Improving flow characteristic of oil and increasing pumping rate by heat treatment looping system, solvent treatment (mixing), and additive. (8 hrs)

Storage Selection of storage type and its pressure, Storage losses, (Breathing, Filling, leakage, and reducing them), Mechanical design, Classification of press. Vessels and its codes and standard, Fundamental principles and equations:, (Theories of failure, elastic stability, membrane stress in shell of revolution, flat plate, dilation of vessels, secondary stress), General design consideration, (Design pressure, design temp., materials, design stress, welded joint efficiency, corrosion allowance, design loads, min. practical wall thickness), The design of thin walled vessels under internal pressure, Cylinders and spherical shells, Heads and closures, Design of flat ends, Design of domed ends, Conical sections and end closures, Compensation for openings and branches, Design of vessels subject to combined loading, Weight loads, Wind loaw Earthquake loading (10 hrs)

Third Year - Storage & Transport of Crude Oil & Petroleum Products

Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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References 1- Campbell, J.M (1981) Gas conditioning and processing, vol. 1, published by: Campbell Petroleum Series, Inc. 2- Nelson, N.L (1963) Petroleum Refinery Engineering, 4th ed. Mc Graw Hill book company, Inc. 3- Jacques Vincent Genod (1984) Fundamentals of pipeline engineering gpc. 4- Sinnot, R.K (1983) Chemical Engineering Design vol.6, 4th ed. Elsevier. 5-Bllad, W.F and Davidson R.L (1967) Petroleum Processing Handbook, Mc Graw Hill Book co., Inc. 6- Couper, J.R, Penney, W.R, Fair, J.R, and Walas, S.M, Chemical Process Equipment Selection and Design © 2005, Elsevier, Gulf Professional Publishing. 7- King, R.C (1930) Piping Handbook (5th edition 1973), McGraw Hill. 8-Szilas, A.P (1975) Production and transport of oil and gas, Elsevier Scientific Publishing Company. 9-Noel de Nevers (1991) Fluid mechanics for chemical Engineering, Mc Graw Hill chemical Engineering series.

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Introduction to Design The anatomy of chemical manufacturing process, general overall design considerations , development of design data base , process creation ,types of process design. (5 hrs)

Design Information and Data Source of information of physical properties , predication of physical properties ( density, viscosity, thermal conductivity , etc ) (5 hrs)

Material and Energy Balance

Review of material and energy balance, flow sheet symbols, PFD information in flow diagram

(6 hrs) Choice Of Plant Location and Layout Standard (4 hrs) Industrial Services Utilities(Cooling Tower, Boiler, Refrigeration System Etc) (6 hrs)

Design With Computer Aided (4 hrs)

References

1- Coul-Jeffery,G(1981) Aproblem in Chem.. Eng. Design,Inst Ch. Eng,London.

2- Brownell,L,(1959)Process Eq. design (Wiley)son J M and Richardson J F,(1983)Chemical Engineering,Vol 6

Fourth Year – Project

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 4 Theoretical 1hr/week Tutorial -hr/week Practical 2hr/week

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Drying Introduction and general Principle in drying, Rate of drying, the mechanism of moisture movement, Calculation of rate of drying, moisture transport in Solids at Constant in Continuous dryers, Types of Dryers and falling rate Period, Capillary movement, Material and Energy Balances (6 hrs)

Humidification, dehumidification and Cooling towers Humidification, dehumidification, Temperature humidity Chart for air – water system . Enthalpy – humidity –temperature chart. Addition of Vapor or liquid Stream to a gas Stream. Mechanism of dehumidification Evaluation of heat and Mass transfer Coefficient, Cooling tower, height of Packing in Cooling towers, Minimum gas Condition. (13 hrs)

Evaporation Introduction, Types of Evaporations, Evaporation Equipment, Heat transfer in Evaporation Process, single, double and Multi effect Evaporators, Design of evaporators, Comparison of Forward, backward and Parallel effect evaporators, boiling Point rise. (10 hrs)

Extraction

Definition, Extraction process, Equilateral Triangular coordinates (Ternary Diagram), system of three liquid _ one pair partially soluble, choice of solvent, Equipment in extraction cross _ current extraction, multi stage Cross Current extracting cross current for insoluble Liquid , Continuous Counter current extraction , Continuous Counter Current in Soluble , Liquid , Minimum Solvent .

(15 hrs) Filtration

Type of Filters, Filtration theory, Plate and frame filter press, leat filter, filtration at Constant ΔP, Filtration at Constant rate, washing Time. (8 hrs)

Membrane Introduction , classification of membrane processes , general membrane equation , liquid permeation membrane processes , gas permeation membrane processes reverse osmosis , reverse osmosis with water treatment plant , ultra filtration membrane processes , micro filtration membrane processes . (4 hrs)

Reynolds analogy Momentum, heat and mass transfer molecular diffusion, Eddy transfer, Reynolds analogy, Modified Reynolds analogy, Chilton and Colburn analogy. (6 hrs)

References 1- J.M. Colulsson and J.F.Richardson, "Chemical Eng.",vol.1,3rd

2- J.M. Colulsson and J.F.Richardson, "Chemical Eng.",vol.2,3

edition, Robert Maxwell. rd

edition, Robert Maxwell.

Fourth Year - Unit Operation

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 5 Theoretical 2hr/week Tutorial 1hr/week Practical 3hr/week

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Exp. No. Exp. Name.

Exp. No. 1 Tray Dryer.

Exp. No. 2 Plate and Frame Filtration.

Exp. No. 3 Rotary Drum Filtration.

Exp. No. 4 Design of Cooling Tower.

Exp. No. 5 Sedimentation.

Exp. No. 6 Liquid - Liquid Extraction

Fourth Year - Unit Operation Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

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Linear Open-Loop Systems Response of First-order Systems, Transfer Function, Transient Response.

(6 hrs) Physical Examples of First Order Systems Dynamic behavior of 1st order system, Linearization.

(6 hrs) Response of First-Order Systems in Series Non-interacting System, Interacting System.

(2 hrs) Higher-Order Systems 2nd order Under-damped System, 2nd order Over-damped System, Transportation Lag.

(6 hrs) Linear Closed Loop Systems The Control System, Controllers and Final Control Elements, Block Diagram of Chemical reactor

Control System, Overall Closed-Loop Transfer Functions. (10 hrs)

Characteristics of the Closed Loop System Transient Response of Simple Control Systems, Stability. (6 hrs)

Frequency Response Methods Introduction to Frequency Response, Bode Diagrams, Control System Design by Frequency Response, Ziegler-Nichols Controller Settings.

(10 hrs) Controller Mechanisms Pneumatic Controller Mechanisms, Industrial Pneumatic Controller, Final Control element.

(4 hrs) Control of Complex Processes Distillation Column, Heat Exchanger, Chemical Reactor. (2 hrs)

Control Systems Feedback control, Feed-forward Control, Ratio Control, Cascade Control, Adaptive Control, Selective Control Systems. (6 hrs)

Computer Control of Chemical process Analog Computer, Digital Computer, Computer Control Loops. (2 hrs)

References 1- D.R. Coughanowr and S. LeBlanc, "Process Systems Analysis and Control", McGraw-Hill, 3rd edition, 2008. 2- G.Stephanopoulos, “Chemical Process Control-An Introduction to Theory and Practice”, Prentice -Hall, New Jersey, 1984. 3- W. L. Luyben, “Process Modeling, Simulation and Control for Chemical Engineers,” McGraw-Hill, New York, 2nd edition, 1990 . 4- W. Bequette "Process Dynamics: Modeling, Analysis and Simulation".

Fourth Year - Process Control

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 5 Theoretical 2hr/week Tutorial 1hr/week Practical 3hr/week

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Exp. No. Exp. Name.

Exp. No. 1 Flow rate Control

Exp. No. 2 Temperature Control

Exp. No. 3 Dynamic Behavior of Second Order System

Exp. No. 4 Dynamic of Stirred Tanks

Exp. No. 5 Dynamic of Stirred Tanks Heater

Exp. No. 6 Feedback Control

Exp. No. 7 Pressure control

Exp. No. 8 PH control

Fourth Year - Process Control Laboratory

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

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1.Chemical Processing (1 hr) 2.Sulfur and sulfuric acid (1 hrs) 3.Ammonia and nitric acid (2 hrs) 4.Nitrogenous fertilizers (2 hrs) 5.Phosphoric acid (2 hrs) 6.Phosphate fertilizers (2 hrs) 7.Electrolytic industries (2 hrs) 8. Industrial salts (2 hrs) 9. Ceramic industries (2 hrs) 10. Cement industries (2 hrs) 11. Glass industries (2 hrs) 12. Surface coating industries (2 hrs) 13. Oils and fats (2 hrs) 14.Soap and detergents (2 hrs) 15. Sugar industries (2 hrs)

16.Production of liquid biofuels from renewable resources (2 hrs)

References 1. N. Naderpour "Petrochemical Production Processes" 1P

stP reprint, sbs publishers, New

Delhi,2009 2. Hydrocarbon processing" Petrochemical processes"2005 2004د.جابر شنشول جمالي،الصناعات البترو كيمياوية، الجامعة التكنولوجية .3 4. H.L. List "Petrochemical Technology" PrenticeHal Vew Jersey, 1986. 5. L.F. Hatch and Samatar "From, hydrocarbon to Petrochemicals" Gulf Publishing company 2P

ndP

printing, 1982 6. A.L.Waddams"chemical from petroleum"4P

thP edition John Murray,London,1978

Fourth Year - Chemical Process Industries

Chemical Processing Eng. Branch

Units 4 Theoretical 1hr/week Tutorial 1hr/week Practical 3hr/week

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(A)

(B)

Exp. No. Exp. Name.

Exp. No. 1 Ethanol production.

Exp. No. 2 Ethyl Acetate production.

Exp. No. 3 Chloroform Production.

Exp. No. 4 Production of Soap.

Exp. No. 5 Production of Urea-Formaldehyde

Exp. No. Exp. Name.

Exp. No. 1 Water treatment by ionic exchange.

Exp. No. 2 Extraction 1Tof1T 1Tvegetable1T 1Toils1T.

Exp. No. 3 Production of Fatty Acids.

Exp. No. 4 Sulfonation of Detergent-Alkylates.

Exp. No. 5 Biodiesel Production

Fourth Year - Chemical Process Industries Laboratory

Chemical Processing Eng. Branch

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Petroleum Processing Overview History of Petroleum Production, What is Petroleum, History of Petroleum Processing, Modern Petroleum Processing. (2 hrs) Refinery Feed-stocks and Products (2 hrs) Thermo-physical Properties of Petroleum Fractions and Crude Oils Specific Gravity , Boiling Point Curves, Breakup of TBP Curve into Pseudo-components,

Thermo-physical Properties Calculation. (4 hrs) Crude Distillation Desalting Crude Oils. Atmospheric Distillation Unit { Material and Energy Balances, Reflux, Overflash, Overhead Temperature, Side Draw Temperature, Bottom Temperature, Tower Diameter},Vacuum Distillation Unit. (6 hrs) Conversion Processes Visbreaking, Coking, Fluid Catalytic Cracking, Hydrotrating and Hydrocracking. (6 hrs) Upgrading Naphtha Catalytic Reforming, Isomerization. (4 hrs) Product Blending Reid Vapor Pressure, Octane Blending. (2 hrs) Supporting Processes Hydrogen Production, Gas Processing Unit, Acid Gas Removal, Sulfur Recovery Processes. (4 hrs) References

1- 4TNelson, W. L. "Petroleum Refinery Engineering", Tata McGraw Hill Publishing Company Limited, 1985.

2- 4TGary J., Handework G., “Petroleum Refining Technology and Economics”,Marcell Dekker Inc. 1984.

3- 4TAddelAal H. A. and Mohamed Aggour "Petroleum and Gas Field Processing" Marcel Dekker Inc. 2003.

4- 4TChang S. Hsu and Paul R. Robinson "Practical Advances in Petroleum Processing Volume 1" Springer Science Business Media, Inc. 2006.

Fourth Year - Petroleum Refinery Eng.

Chemical Processing Eng. Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction Properties of catalyst, determination of surface area, void volume and solid density, pore volume, distribution, classification of catalyst, promotes and inhibitors. (4 hrs) Rate equations of fluid solid catalytic reactions

Rate of adsorption, desorption and surface reaction, rate of limiting step, (CVD) chemical vapor deposition (6 hrs)

External and internal diffusion effects on the heterogeneous reactions

External resistance to mass transfer, mass transfer coefficient, diffusion and reaction in spherical catalyst pellets, internal effectiveness factor, over all effectiveness factor, estimation of diffusion, Thiele type modulus. (6 hrs)

Practical example (Direct oxidation of methanol to formaldehyde) Analysis, developing the catalyst ,kinetic and mechanism of the reaction, composition of the catalyst , preparing the catalyst , using the catalyst (operating condition) , sizing the reaction the process flow scheme. (6 hrs)

G\L reactions on solid catalysttrickle beds slurry reactors and three phase fluidized beds The general rate equation, performance equations, which kind of contactor to use, hydrogenation of acetone in a packed bubble column. (4 hrs)

Developing industrial catalysts Properties and characteristics of industrial catalyst, activity, selectivity, stability, morphology, mechanical strength, thermal characteristics, regenerability, reproducibility, originality cost, optimization of a typical catalytic formula, deactivation. (4 hrs)

Fourth Year - Catalysis and Catalytic Eng.

Chemical Processing Eng. Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Management Principles of management, classification, management responsibility, organization responsibility, management planning, management's levels. (6 hrs)

Industrial project

Planning and preparation, economic feasibility study, plant layout, cost (fixed cost, working cost, cost index, project cash flow diagram, tax, budgetary control). (6 hrs)

Maintenance

Purpose of maintenance, types and classifications, cost of maintenance operations, machines replacement (principles and planning), Depreciation. (4 hrs)

ISO

Principles,( organization ,documentation, auditing ), requirements ,applications , iso series ,iso stages (preparation ,planning ,assessment ,implementation ,diversification ),total quality management TQM ,application ,corrective actions. (4 hrs)

Quality control

Specifications (types and classification), sampling techniques, quality cost, quality control chart, Deviation. (4 hrs)

Net work analysis

Principles and applications, critical bath method (CPM),Gntt chart ,pert techniques. (3 hrs)

process Samples Unit samples, sample schedule, types of samples. (3 hrs)

1- Banga T., and Sharma S. " Industrial Engineering Management including Production Management " Khanna publisher 11th edition 2008

2- Towler G. and Sinnott R " Chemical Engineering Design " 2nd edition 2013 Elesvier

3- Peters M. , Timmerhaus D. and West R. " Plant Design and Economics for chemical Engineers " 5th

edition 2005 McGraw-Hill

Fourth Year - Industrial Management

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction Definition: Environmental pollution, Historical brief on international concern with pollution, Causes Effects and control measures of different types pollutants of: Air, Water ,Soil, Marine, Noise pollution and Nuclear Hazards. Pollution allowable limits in the environment. (2 hrs)

Water Pollution Control

Water quality and pollution; Types and sources of pollution, Water quality changes, Water quality standard and Stream pollution.Water and Wastewater Treatment Plants and Systems; Physical, Chemical and Biological systems, Primary, Secondary and Tertiary treatment, Sedimentation, Coagulation, Flocculation, Filtration, Ammonia removal, Aeration, Anaerobic and Aerobic digestion, Activated sludge and Trickling filter.Industrial Wastewater Treatment: Characteristics of Industrial wastewater treatment levels and available technologies, Case study treatment (selection) of chemical industry effluent. Removal of Dissolved Salts (Reverse Osmosis, Electrodalysis) and Membrane Technology. (10 hrs)

Air Pollution Control

Air Contaminates Characterization, Source of air pollutants and their effects, Meteorological factors influencing air pollution measurement of air quality, Approaches of air pollution control, Control equipment for Particulates emission ( Settling chamber, Cyclone, Bag or Fabric filter, Wet collectors, Venturi scrubber, Electrostatic precipitators) and Gaseous pollutants. Case study treatment of gaseous effluent in typical industry. (8 hrs)

Solid and Hazardous Wastes Law Solid Wastes Characterization, Nonhazardous and Hazardous solid waste, Solid wastes treatment.

(4 hrs) Industrial Safety

Hazards: Toxicity, Flammability, Explosions, Sources of ignition, Ionizing radiation, Pressure, Temperature deviations and Noise. Dow fire and explosion index. Fire and protection, Biological effects. Designing for safety, Personal protective equipment. (6 hrs)

References (1)M.L. Davis & D.A. Cornwell. "Introduction to Environmental Engineering" Tata McGraw & Hills, 2007. (2) L.K. Wang, "Air Pollution Control Engineering" Humana Press Inc., 2Rev Ed. Edition, 2004 (3) R. Weiner & R. Matthews, "Environmental Engineering" Butter wothHeinemann, 2003. (4) N.W. Jern, "Industrial Wastewater Treatment" Imperial College Press, 2006. (5) S.D. Lin & C.C. Lee, "Water and wastewater Calculation Manual" McGrawHill, 2001. (6) M.J. Hammer,"Water & Wastewater Technology" John wiley & Sons, End Edition. (7) P.A. Vesilind & J. Jeffrey, "Environmental Engineering" Ann Afbar Sc., 2003. (8) Ray Asfahl, "Industrial Safety and Health Management" Prentice Hall

Fourth Year - Environmental Eng.& Industrial Safety

Chemical Processing Eng. Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction Definitions, Corrosive environment, Consequences of corrosion , Cost of corrosion, Why metals corrode ,Basic concepts in corrosion, Anodic and Cathodic reactions, Type of cells. (2 hrs)

Classification of corrosion

Wet corrosion , Dry corrosion, Forms of corrosion (4 hrs)

Kinetics of Aqueous corrosion Faraday's laws of electrolysis and its application in determining the corrosion rate, reversibility and exchange current density polarization, activation polarization, Concentration polarization, combined polarization (4 hrs)

Thermodynamics

Free energy, Cell potential, Reversible electrode potential, Nernst equation (2 hrs) Determining the corrosion rate Corrosion rate measurement units, methods determining corrosion rate; 1immersion test 2electrochemical technique a) Tafel extrapolation b) Linear polarization (4 hrs) Passivity Active Passive metals and conditions for passivity, Kinetics of passivity table passivity, Unstable passivity (2 hrs) 7. Reference electrodes Hydrogen electrode, Ag Ag Cl electrode, ZnZnClR2R electrode, PbPbClR2R electrode (2 hrs) 8.Corrosion prevention Materials selection , Alteration of Environment, Design , Coating , Catholic and anodic protection

(4 hrs) 9. Corrosion control by inhibition Important consideration in selection of inhibitor, Classification of inhibitors, Description of inhibitors Effect of inhibitors on Polarization behavior, Neutralizers, Scale inhibitors, Scavengers, Inhibitor efficiency and inhibitor concentration. (4 hrs) 10.Boiler corrosion Definition, Requirement of efficient boiler, Major corrosion problems in boilers oxygen corrosion, Caustic corrosion, Hydrogen damage, Stress corrosion cracking, corrosion Fatigue. (2 hrs)

References M.G. Fontana and N.D. Greene ,"Corrosion Eng.", 3rd edition, Mc Graw-Hill,1986.

Fourth Year - Corrosion Eng.

Chemical Processing Eng. Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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1- Introduction to Optimization. (2 hrs) 2- Recognizing an Optimization Problems and Their Solution. - Formulation of Optimization Problem. - Unconstrained vs. Constrained Problems. - Examples; Formulation of Industrial Optimization Problems. Economic Optimization of distillation column operation condition. - Homework and Tutorial Sheet. (6 hrs) 3- Optimization Methods For Single Variable Problems. - Analytical Method; Constrained vs. Unconstrained. - Graphical Method. - Numerical Methods: a- Unconstrained Functions; Fixed Step Method, DSC Method, Newton Method. b- Constrained Functions; Sequential Search, Dichotomous Search, Fibonacci Search, Golden Ratio Search. - Home work and Tutorial Sheet. (12 hrs) 4- Determining the Solution to Multivariable Optimization Problems. a- Unconstrained Minimization and Maximization strategy. - Solving Linear and Nonlinear Equations using Matrices. - Optimality Conditions for Unconstrained Problems. - Homework & Tutorial Sheet. - Lagrangian Criteria. - Simplex MethodDirection Step Length Calculations. b- Solution of Constrained Multivariable Problems. - Analytical Solution. - Lagrangian Duality. - Linearization of Nonlinear Optimization Problems. - Simplex Method. - Pivot Table Formulation. - Homework & Tutorial Sheet c- Linear Programming (LP) Problems. - Linear Programming Optimization Formulation . - Solving Linear system. - Basic Solution of an (LP) Problems. - Graphical Interpretation. - Homework and Tutorial Sheet. ( 10 hrs)

References 1- Optimization of Chemical Process” Edgar T.F., Himmelblau D.M. and Lasdon L.S.,

2P

ndP Edition, McGraw – Hill, Newyork, 2001

Fourth Year - Optimization

Chemical Processing Eng. & Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Evaluation of Oil Stocks: Characterization of Petroleum, Analysis of Crude Petroleum : True Boiling Point, ASTM and Equilibrium Flash Vaporization Curves. Mid Percent Curves, Yield Curves. (8 hrs)

Dehydration and Desalting of Crude Oil : Emulsion Treatment and Dehydration of Crude Oil, Desalting of Crude Oil (4 hrs)

Tube still heaters:

Types of stills, Radiation, Rate of Heat Absorption in Radiant Section, Convection. (4 hrs)

Fractionation of Petroleum: Atmospheric and Vacuum Fractionation (2 hrs)

Fractionation Towers: Material and Energy Balances, Reflux Temperate Distribution in Fractionation Tower, Tower Diameter. (8 hrs)

Petroleum Refining Overview: Type of Refineries. (4 hrs)

Treating Processes: Removal of Acid Gases, Sweetening Processes, Improvement in Performance and Storage Stability. (8 hrs)

Upgrading Processes: Thermal Cracking, Cooking. Visbreaking, Catalytic Cracking, Hydrocracking, Catalytic Reforming, Alkylation, Isomerisation. (12 hrs)

Product Blending:

Blending of Vapor Pressure, Octane Number, Viscosity, Flash Point, Aniline Point and Pour Point. (4 hrs)

Heavy Oils Processing: Heavy oils processing, Lubricating Oil and Wax Processing, Asphalt Manufacture. (4 hrs) 1. Petroleum Additives: Octane improver – TEL, MTBE, VI improver, Pour point depressant, Antioxidant, others.

(2 hrs) References 1-Nelson, W. L. "Petroleum Refinery Engineering", Tata McGraw Hill Publishing Company Limited, 1985. 2-Gary J., Handework G., “Petroleum Refining Technology and Economics”,Marcell Dekker Inc. 1984. 3-AddelAal H. A. and Mohamed Aggour "Petroleum and Gas Field Processing" Marcel Dekker Inc. 2003 4- Chang S. Hsu and Paul R. Robinson "Practical Advances in Petroleum Processing Volume 1" Springer Science Business Media, Inc. 2006.

Fourth Year - Petroleum Refinery Eng.

Oil and Gas Refinery Eng .Branch

Units 6 Theoretical 2hr/week Tutorial 1hr/week Practical 3hr/week

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Exp. No. Exp. Name

Exp. No. 1 Properties of Low Temperature

Exp. No. 2 Water Content in Crude Oil

Exp. No. 3 Sediment Content in Crude Oil

Exp. No. 4 Properties of Diesel Fuel

Exp. No. 5 Properties of Crude Oil

Exp. No. 6 Atmospheric Distillation

Fourth Year - Petroleum Refinery Eng Laboratory..

Oil and Gas Refinery Eng .Branch

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Gaseous Fuels Classification of gaseous Fuels; The Importance of Gaseous Fuels. (1 hr) Natural Gas Fundamentals

Natural Gas Origin and Composition; Gas Sources (Nonassociated Gas, Associated Gas, Coal Bed Methane); Natural Gas Phase Behavior; Natural Gas Properties (Physical Properties, GasSpecific Gravity, Ideal and Real Gas Laws, Gas Density, Gas Viscosity). (5 hrs)

Basic Concepts of Natural Gas Processing

Process Modules; Scope of Natural Gas Processing; Processing Objectives; Effect of Gas Type in Field Processing. (4 hrs)

Phase Separation Gravity Separators; Multistage Separation; Centrifugal Separators; Twister Supersonic

Separator ; Slug Catchers; High Efficiency Liquid–Gas Coalescers. (4 hrs)

Condensate Stabilization Stabilization Processes: Flash Vaporization, Stabilization by Fractionation. (4 hrs) Acid Gas Treating

Acid Gas Removal Processes: Amine Processes, Other Processes; Sulfur Recovery Processes. (4 hrs)

Natural Gas Dehydration Water Content Determination; Glycol Dehydration; Solid Desiccant Dehydration. (4 hrs)

Natural Gas Liquids Recovery (2 hrs)

Liquefied Natural Gas (LNG) The LNG Process; LNG Liquefaction. (1 hr)

10-GasToLiquids (GTL) Why GTL? ; GTL Processes. (1 hr) References: 1- Saeid Mokhatab, William A.Poe and James G.Speight. "Hand book of Natural Gas Transmission and Processing" 2006. 2- Arthur J. Kidnay & William R. Parrish “Fundamentals of Natural Gas Processing” 2006. 3- Xiuli Wang XGAS “Advanced Natural Gas Engineering” 2009.

Fourth Year - Gas Technology

Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction Properties of catalyst, determination of surface area, void volume and solid density, pore volume, distribution, classification of catalyst, promotes and inhibitors. (4 hrs)

Rate equations of fluid solid catalytic reactions Rate of adsorption, desorption and surface reaction, rate of limiting step. (4 hrs)

External and internal diffusion effects on the heterogeneous reactions External resistance to mass transfer, mass transfer coefficient, diffusion and reaction in spherical catalyst pellets, internal effectiveness factor, over all effectiveness factor, estimation of diffusion, Thiele type modulus. (6 hrs)

Practical example for catalytic reforming

Analysis of the reaction, active species,, developing the support, catalytic performance, the process, improvement the catalyst, paraffin dehydrocyclization, isomerization composite reaction scheme. (8 hrs)

G\L reactions on solid catalyst trickle beds slurry reactors and three phase fluidized beds

The general rate equation, performance equations, which kind of contactor to use, hydrogenation of ButyNeDoil in a slurry reactor. (4 hrs)

6. Developing industrial catalysts

Properties and characteristics of industrial catalyst, activity, selectivity, stability, morphology, mechanical strength, thermal characteristics, regenerability, reproducibility, originality cost, optimization of a typical catalytic formula, deactivation. (4 hrs)

References 1. Ronald W. Missen et al., (1999), "Introduction to chemical reaction engineering and kinetics",

1P

stP edition, John wiely & Sons, (USA).

2. J.M. Smith (1981), "Chemical engineering kinetics", 3P

rdP edition, McGrowHill, Singapore.

3. J.F. Lepage, J. Cosyns & P. Courty, "Applied heterogeneous Catalysis"

4. James T. Richardson, " Principle of catalyst development"

Fourth Year - Catalysis in Petroleum Refineries

Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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1.Introduction: Definition: Environmental Pollution of Petroleum industry, Historical brief on International concerns with petroleum pollution, Causes effect and control measures of different types of petroleum pollutants of; Air, Water, Soil, Marine, Noise pollution and Nuclear Hazards. Petroleum pollution allowable limits in the environment. (2 hrs)

2.The Impact of Production Operations: Measuring Toxicity, Hydrocarbons, Salt, Heavy metals, Production chemicals, Produced water, Air pollution. (2 hrs)

3.Treatment of Wastewater from Petroleum Industry: Removal of suspended Hydrocarbons, Removal of Dissolved Hydrocarbons (Adsorption, Volatilization, Biological processes, Precipitation, Ultraviolet Irradiation and Oxidation), Removal suspended solids (Gravity separation, Filtration, Coagulation and Flocculation), Removal of Dissolved Solids (Precipitation, Reverse Osmosis or Membrane Technology, Evaporation or Distillation), Neutralization. (10 hrs) 4.Treatment of Air Emissions: Air pollutants ( Hydrocarbons, Particulates, Gases), Characterization, Meteorological factor influencing, Characteristics of Stack Plume. Control of Particulates: Cyclone, Packed bed, Spray tower, Electrostatic Precipitator. Control of Gases ( CO, SOX,NOX): (Adsorption, Combustion, Control of SO2 and NO2). Chimney Design. (8 hrs) 5.Treatment of Solids: Removal water, Removal Hydrocarbons, Solidification. (2 hrs)

6.Safety in Petroleum Refinery: Fire Prevention and Control: Need, Accidents and causes of fire, Prevention and action taken in a case of fire, Dow fire and explosion index. Materials handling and storage, Noise Hazardous, Radiation Hazardous, Common Hazardous Materials in Refinery. (6 hrs) References: (1)Gulf Publishing Company, "Environmental Engineering Control in Petroleum Engineering" 1996. (2)M.L. Davis & D.A. Cornwell. "Introduction to Environmental Engineering" Tata McGraw & Hills, 2007. (3) L.K. Wang, "Air Pollution Control Engineering" Humana Press Inc., 2Rev Ed. Edition, 2004

(4) R. Weiner & R. Matthews, "Environmental Engineering" ButterwothHeinemann, 2003.

(5) N.W. Jern, "Industrial Wastewater Treatment" Imperial College Press, 2006.

(6) S.D. Lin & C.C. Lee, "Water and wastewater Calculation Manual" Mc-GrawHill, 2001.

(7) M.J. Hammer,"Water & Wastewater Technology" John wiley & Sons, End Edition.

(8) P.A. Vesilind & J. Jeffrey, "Environmental Engineering" Ann Afbar Sc., 2003.

(9) Ray Asfahl, "Industrial Safety and Health Management" Prentice Hall.

Fourth Year - Environmental Pollution &Safety in Petroleum Refineries

Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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Introduction Definitions, Corrosive environment, Consequences of corrosion , Cost of corrosion, Why metals corrode ,Basic concepts in corrosion, Anodic and Cathodic reactions, Type of cells. (2 hrs)

Classification of corrosion

Wet corrosion , Dry corrosion, Forms of corrosion. (4 hrs)

Kinetics of Aqueous corrosion Faraday's laws of electrolysis and its application in determining the corrosion rate, reversibility and exchange current density polarization, activation polarization, Concentration polarization, combined polarization. (4 hrs)

Thermodynamics

Free energy, Cell potential, Reversible electrode potential, Nernst equation. (2 hrs)

Determining the corrosion rate Corrosion rate measurement units, methods determining corrosion rate; 1-immersion test 2-electrochemical technique a) Tafel extrapolation b) Linear polarization (4 hrs)

Passivity Active Passive metals and conditions for passivity, Kinetics of passivity table passivity, Unstable Passivity. (2 hrs)

Reference electrodes Hydrogen electrode, AgAgCl electrode, ZnZnClR2R electrode, PbPbClR2R electrode . (2

hrs)

Corrosion prevention in Oil Industry Materials selection , Alteration of Environment, Design , Coating , Anodic protection, Inhibitors

(4 hrs) Cathodic Protection

Sacrificial anode corrosion protection, impressed current anode corrosion protection, Major impressed current anodes, Galvanic systems anodes, Design parameters in cathodic protection, Stray current corrosion. (4 hrs)

Corrosion in Oil Industry Case Study

Fourth Year - Corrosion Eng,

Oil and Gas Refinery Eng .Branch

Units 2 Theoretical 2hr/week Tutorial 1hr/week Practical -hr/week

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المرحلة االولى فرع هندسة العمليات الكيمياوية

المرحلة االولى فرع هندسة تكريرالنفط و الغاز

المواد

ساعة /اسبوع

الفصل الثاني الفصل االول الوحدات

تمارين عملي نظري تمارين عملي نظري

4 - - 2 - - 2 اللغة االنكليزية 2 - 1 2 - 1 4 (Ι) الرياضيات

المبادئ األساسية للهندسة I (2 - 1 2 - 1 4الكيمياوية(

6 1 2 2 1 2 2 كيمياء ال 4 - 2 1 - 2 1 الرسم الهندسي

هندسة الميكانيك ومقاومة المواد

2 - 1 2 - 1 4

2 1 - 1 1 - 1 تكنولوجيا الكهرباء 1 2 1 1 2 1 4 (Ι)برمجة الحاسبات

4 - 6 - - 6 -المعامل 36 6 12 13 6 12 13 المجموع

31 31ساعة /أسبوع

المواد

ساعة /اسبوع

الفصل الثاني الفصل االول الوحدات

تمارين عملي نظري تمارين عملي نظري

4 - - 2 - - 2 اللغة االنكليزية Ι 2 - 1 2 - 1 4)الرياضيات (

المبادئ األساسية للهندسة (Ι) الكيمياوية

2 - 1 2 - 1 4

6 1 2 2 1 2 2كيمياء النفط 4 - 2 1 - 2 1الرسم الهندسي

هندسة الميكانيك ومقاومة 4 1 - 2 1 - 2المواد

2 1 - 1 1 - 1تكنولوجيا الكهرباء 1 2 1 1 2 1 4 (Ι)برمجة الحاسبات

4 - 6 - - 6 -المعامل 36 6 12 13 6 12 13المجموع

31 31ساعة /اسبوع

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الثانية المرحلة فرع هندسة العمليات الكيمياوية

الثانية المرحلة فرع هندسة تكريرالنفط و الغاز

المواد ساعة /اسبوع

الوحدات الفصل الثاني الفصل االول تمارين عملي نظري تمارين عملي نظري

1 - - - 1 - 1حقوق اإلنسان 1 1 - 1 - - - الديمقراطية II (2 - 1 2 - 1 4الرياضيات (

المبادئ األساسية للهندسة ) IIالكيماوية (

2 - 1 2 - 1 4

6 1 2 2 1 2 2جريان الموائع 5 1 - 2 1 2 2الكيمياء الفيزياوية II (1 2 1 1 2 1 4برمجة الحاسبات ( 5 1 2 2 1 - 2هندسة علم المواد 3 1 - 1 1 2 1تكنولوجيا الوقود

3 1 2 1 1 - 1اإلحصاء والقياسات 36 9 8 14 9 8 14المجموع

31 31ساعة /اسبوع

المواد ساعة /اسبوع

الوحدات الفصل الثاني الفصل االول تمارين عملي نظري تمارين عملي نظري

1 - - - 1 - 1حقوق اإلنسان 1 1 - 1 - - -الديمقراطية

2 - 1 2 - 1 4 (II)الرياضياتالمبادئ األساسية للهندسة

2 - 1 2 - 1 4 (II)الكيمياوية

6 1 2 2 1 2 2جريان الموائع 5 1 - 2 1 2 2الكيمياء الفيزياوية

1 2 1 1 2 1 4 (II)برمجة الحاسبات 5 1 2 2 1 - 2 علم المواد هندسة

3 1 - 1 1 2 1 خصائص المنتجات النفطية 3 1 2 1 1 - 1 اإلحصاء والقياسات

36 9 8 14 9 8 14المجموع 5B31 31 ساعة /اسبوع

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المرحلة الثالثة فرع هندسة العمليات الكيمياوية

المرحلة الثالثة فرع هندسة تكريرالنفط و الغاز

المواد ساعة /اسبوع

الوحدات الفصل الثاني الفصل االول تمارين عملي نظري تمارين عملي نظري

5 1 2 2 1 - 2ديناميك الحرارة 4 1 - 2 1 - 2الرياضيات التطبيقية

5 1 - 2 1 3 2انتقال كتلة 4 1 - 2 1 - 2تصميم المفاعل

5 1 3 2 1 - 2انتقال حرارة 5 1 - 2 1 2 2تصميم المعدات

3 1 2 2 - - -التحليالت العددية الهندسة الكيميائية

اإلحيائية 2 - 1 - - - 2

2 - - - 1 - 2الدقائق وتكنولوجيا النانو 2 1 - 2 - - - الصناعات البتروكيمياوية

37 8 7 16 8 5 16المجموع 31 29 أسبوعساعة /

المواد ساعة /اسبوع

الوحدات الفصل الثاني الفصل االول تمارين عملي نظري تمارين عملي نظري

5 1 2 2 1 - 2 ديناميك الحرارة 4 1 - 2 1 - 2 الرياضيات التطبيقية

5 1 - 2 1 3 2 انتقال كتلة 4 1 - 2 1 - 2 تصميم المفاعل

5 1 3 2 1 - 2 انتقال حرارة 5 1 - 2 1 2 2 تصميم المعدات

3 1 2 2 - - - التحليالت العددية 2 - - - 1 - 2المواد الكيمياوية من النفط

2 - - - 1 - 2 هندسة االحتراق 2 1 - 2 - - - خزن ونقل النفط ومشتقاته

37 8 7 16 8 5 16 المجموع6B 31 29ساعة /اسبوع

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المرحلة الرابعة فرع هندسة العمليات الكيمياوية

المواد ساعة /اسبوع

الوحدات الفصل الثاني الفصل االول تمارين عملي نظري تمارين عملي نظري

4 - 2 1 - 2 1المشروع 5 1 - 2 1 3 2الوحدات الصناعية

5 1 - 2 1 3 2السيطرة على العمليات 4 1 3 1 1 3 1الصناعات الكيمياوية

2 - - - 1 - 2 هندسة تكرير النفط 2 - - - 1 - 2هندسة العوامل المساعدة

2 1 - 2 - - - اإلدارة الصناعية 2 - - - 1 - 2 هندسة البيئة والسالمة الصناعية

2 1 - 2 - - - هندسة التآكل 2 1 - 2 - - - اختيار األفضل

30 6 5 12 6 11 12المجموع 23 29ساعة /اسبوع

المرحلة الرابعة فرع هندسة تكريرالنفط و الغاز

المواد ساعة /أسبوع

الوحدات الفصل الثاني الفصل االول تمارين عملي نظري تمارين عملي نظري

4 - 2 1 - 2 1 المشروع 5 1 - 2 1 3 2 الوحدات الصناعية

5 1 - 2 1 3 2 السيطرة على العمليات 6 1 3 2 1 3 2 هندسة تكرير النفط

2 - - - 1 - 2 تكنولوجيا الغازالعوامل المساعدة في مصافي

النفط - - - 2 - 1 2

2 - - - 1 - 2 اإلدارة الصناعيةالتلوث البيئي والسالمة في

مصافي النفط- - - 2 - 1 2

2 - - - 1 - 2 هندسة التآكل 2 1 - 2 - - - اختيار األفضل

32 6 5 13 6 11 13 المجموع7B 24 30ساعة/أسبوع

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ت االختصاص الدقيق االختصاص العام اللقب العلمي الشهادة االسم الثالثي واللقب

ظواهر أنتقال هـ.كيمياوية استاذ دكتوراه نيران خليل ابراهيم خلف 1 بوليمرات علوم كيمياء استاذ دكتوراه نجاة جمعة صالح معلة 2 عوامل مساعدة هـ.كيمياوية استاذ مساعد دكتوراه شهرزاد رفعت رؤوف قاسم 3 اجتماع سياسي كليةاالداب استاذ مساعد دكتوراه بشرى عبد هللا مجيت سعيد 4 تاكل المعادن هـ.كيمياوية استاذ مساعد دكتوراه عصام كامل صالح عبدالغني 5 سيطرة على العمليات هـ.كيمياوية استاذ مساعد دكتوراه غانم مقبول علوان يعقوب 6 فيزياء/مواد متراكبة العلوم التطبيقية استاذ مساعد دكتوراه محمد أبراهيم محمد نصيف 7 تكنولوجيا مواد مركبة هـ.كيمياوية استاذ مساعد دكتوراه عدنان عبدالجبار عبدالرزاق عثمان 8 سيطرة على العمليات هـ.كيمياوية استاذ مساعد دكتوراه زيدون محسن شكور ولي 9

جريان متعدد االطوار هـ.كيمياوية استاذ مساعد دكتوراه رياض صادق محمدصالح محمد 10 انتقال كتلة هـ.كيمياوية استاذ مساعد دكتوراه طالب محمد نايف حسن 11 كيمياء النفط هـ.كيمياوية استاذ مساعد دكتوراه عادل شريف حمادي رهيف 12 عوامل مساعدة هـ.كيمياوية مدرس دكتوراه ايمان جواد طه محمد 13 امتزاز هـ.كيمياوية مدرس دكتوراه انتصار حسين خلف هادي 14 انتقال كتلة هـ.كيمياوية مدرس دكتوراه صالح سلمان ابراهيم عباس 15 تكنولوجيا البوليمرات هـ.كيمياوية مدرس دكتوراه نبيلة عادل محمد صالح 16 انتقال حرارة هـ.كيمياوية مدرس دكتوراه خالد حامد رشيد عبد الخالق 17 تحليلية علوم كيمياء مدرس ماجستير أمل ثجيل جبر بجاي 18 تاكل المعادن هـ.كيمياوية مدرس ماجستير خالد تركي راشد كيطان 19 هندسة احيائية هـ.كيمياوية مدرس ماجستير نغم اديب عبد الكريم حسون 20 هندسة احيائية هـ.كيمياوية مدرس ماجستير تغريد لطفي عبد الرحمن علي 21 أقتصاد االدارة واالقتصاد مدرس ماجستير ماهر عزيز عبد الرحمن حبيب 22 أنتقال كتلة هـ.كيمياوية مدرس ماجستير علي رعد محمد جواد كاظم 23 كيمياء فيزياوية علوم كيمياء مدرس ماجستير احالم سعيد معروف محمد 24 معالجة المستحلبات هـ.كيمياوية مدرس ماجستير لمى حسين محمود خلف 25 العضوية علوم كيمياء مدرس ماجستير علياء عصام مهدي عبد هللا 26 تآكل معادن هـ.كيمياوية مدرس ماجستير بشير أحمد عبد الحسين عزيز 27 كيمياء صناعية علوم كيمياء مدرس مساعد ماجستير منال افهم توما نعمان 30 انتقال حرارة هـ.كيمياوية مدرس مساعد ماجستير حيدرعبد علي عبد الكريم محمد 28 برامجيات علوم الحاسوب مدرس مساعد ماجستير عمار محمد علي محمد 29 تكنولوجيا النانو هـ.كيمياوية مدرس مساعد ماجستير أياد داري جعفررمضان 31 تلوث البيئة هـ.كيمياوية مدرس مساعد ماجستير زينب عدنان ناصر راضي 32 امتزاز/تكنولوجيا النانو هـ.كيمياوية مدرس مساعد ماجستير ضياء عبد الرسول حسين 33 تآكل معادن هـ.كيمياوية مدرس مساعد ماجستير نضال احمد شاكر 34

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االختصاص الدقيق االختصاص العام اللقب العلمي الشهادة االسم الثالثي واللقب ت

سيطرة على العمليات هـ.كيمياوية استاذ دكتوراه صفاء الدين عبد هللا علي عبدالقادر 1 جريان متعدد االطوار هـ.كيمياوية استاذ دكتوراه ثامر جاسم محمد شالل 2 انتقال المادة هـ.كيمياوية استاذ دكتوراه قصي فاضل عبد الحميد ولي 3 تاكل المعادن هـ.كيمياوية استاذ مساعد دكتوراه شذى احمد سامح عبد هللا 4 ديناميك الحرارة هـ.كيمياوية استاذ مساعد دكتوراه ناهض وديع ميخائيل دانيال 5 تصميم المفاعالت هـ.كيمياوية استاذ مساعد دكتوراه محمد فاضل عبد علي 6 أنتقال كتلة هـ.كيمياوية استاذ مساعد دكتوراه انعام اكرم صبري طاهر 7 انتقال حرارة هـ.كيمياوية استاذ مساعد دكتوراه جمال مانع علي حسوني 8 انتقال كتلة هـ.كيمياوية استاذ مساعد دكتوراه عروبة نافع عبد هللا محمد 9

أنتقال كتلة/تقطير هـ.كيمياوية استاذ مساعد دكتوراه نضال محمود عبد الرزاق محمد 10 جريان متعدد االطوار هـ.كيمياوية مدرس دكتوراه عامر عزيز عبد الرحمن حبيب 11 جريان موائع هـ.كيمياوية مدرس دكتوراه سحر عبد الهادي داود 12 هندسة مفاعالت هـ.كيمياوية مدرس دكتوراه فرح طالب جاسم محمد 13 ديناميك الحرارة-تبريد هـ.كيمياوية مدرس دكتوراه شروق طالب رمضان باقر 14 ظواهر أنتقال هـ.كيمياوية مدرس دكتوراه والء عبد الهادي نوري محمد علي 15 أنتقال كتلة هـ.كيمياوية مدرس دكتوراه جنان عبد الكريم عبد الرزاق حسن 16 هـ.تكرير البترول هـ.كيمياوية مدرس دكتوراه بشير يوسف شرهان خليفة 17 نمذجة وحركية مفاعالت البلمرة هـ.كيمياوية مدرس دكتوراه سعد رحيم سلطان عربيد 18 ديناميك المفاعالت هـ.كيمياوية مدرس ماجستير ابتسام حسين مهدي حسن 19 مواد متراكبة هـ.كيمياوية مدرس ماجستير زينب يوسف شنين عنبر 20 عوامل مساعدة هـ.كيمياوية مدرس ماجستير هيام محمد عبد الرحيم عليان 21 تقطير هـ.كيمياوية مدرس ماجستير فضل هاشم فرج حسن 22 أنتقال كتلة هـ.كيمياوية مدرس ماجستير علياء خضيرمجيد راضي 23 أمنية البيانات علوم الحاسوب مدرس ماجستير غيداء سعيد مهدي صالح 24 هندسة التآكل هـ.كيمياوية مدرس ماجستير كمال محمد احمد محمد 25 امتزاز هـ.كيمياوية مدرس ماجستير ليث سالم صبري محمد حسن 26 سيطرة عمليات هـ.كيمياوية مدرس ماجستير فاروق أحمد مهدي علي 27 سيطرة عمليات هـ.كيمياوية مدرس ماجستير زهراء فاضل زحوار محمد 30 أنتقال كتلة هـ.كيمياوية مدرس ماجستير حيدر عبد الكريم محسن كريم 28 بوليمرات هـ.كيمياوية مدرس ماجستير مي علي مسلم رشيد 29 تكنولوجيا المساحيق هـ.كيمياوية مدرس ماجستير فاضل عباس حمادي نفاوة 31 أنتقال كتلة هـ.كيمياوية مدرس مساعد ماجستير علي عبد الرحمن نصيف 32 تلوث هـ.كيمياوية مدرس مساعد ماجستير سميرة نجم عبد هللا خلف 33 السيطرةعلى العمليات هـ.كيمياوية مدرس مساعد ماجستير علي محمد حميد مجيد 34 تاكل المعادن هـ.كيمياوية مدرس مساعد ماجستير عالء مشجل علي سعد 35 أنتقال حرارة هـ.كيمياوية مدرس مساعد ماجستير عباس جواد سلطان عبود 36 حركية تفاعالت هـ.كيمياوية مدرس مساعد ماجستير اريج دلف عباس بارود 37 أنتقال موائع هـ.كيمياوية مدرس مساعد ماجستير هبة محمود عبد هللا سلمان 38 فيزياء الليزر العلوم التطبيقية مدرس مساعد ماجستير خولة عبد الكاظم علي حسين 39 سيطرة عمليات هـ.كيمياوية مدرس مساعد ماجستير عفراء هالل كامل عزيز 40 تكنولوجيا البوليمرات هـ.كيمياوية مدرس مساعد ماجستير بشار جواد كاظم حسين 41 تكنولوجيا المعلومات علوم الحاسوب مدرس مساعد ماجستير صفا أمين أحمد صبار 42 تطبيقات الحاسوب علوم الحاسوب مدرس مساعد ماجستير نهلة فاضل علوان حسين 43 تكنولوجيا االغشية هـ.كيمياوية مدرس مساعد ماجستير عمر صباح مهدي صالح 44 تكنولوجيا االغشية هـ.كيمياوية مدرس مساعد ماجستير حيدر عالء صالح عبد الكريم 45