Laboratory Interfield Laboratories, 13/1208-A, Interprint ... · Sulfamerazin 1.5 to 500 μg/kg...

Laboratory

Interfield Laboratories, 13/1208-A, Interprint House, Karuvelipady, Cochin

Accreditation Standard ISO/IEC 17025: 2005

Discipline Chemical Testing Issue Date 21.10.2013

Certificate Number T-0725 Valid Until 20.10.2015

Last Amended on - of 82

S.No. Product / Material of Test

Specific Test Performed Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

I. FOOD AND AGRICULTURAL PRODUCTS

1. Marine and Farmed

Aquatic Products

Chloramphenicol In-house validated method

IFL/C/QSP SF/007

0.27 to 100 µg/kg

Nitrofuran Metabolites :

a) 3-Amino- 2 Oxazolidilone

(AOZ)

In-house validated method

IFL/C/QSP SF/002

0.9 to 100 µg/kg

b) 3-Amino- 5 -

orpholinomethyl - 2-

oxazolidinone (AMOZ)

0.9 to 100 µg/kg

c) 1-aminohydantoin (AHD)

0.9 to 100 µg/kg

d) Semicarbazide (SEM)

0.9 to 100 µg/kg

Nitrofuran Parent Compounds :

a) Nitrofurazone In-house validated method

IFL/C/QSP SF/003

0.97 to 100 µg/kg

b) Furaltadone

0.97 to 100 µg/kg

c) NitroFurantoin

0.97 to 100 µg/kg

d) Furazolidone

0.97 to 100 µg/kg

Tetracyclines :

a) Tetracycline AOAC 19th

Ed, 995.09 10 to 2000 μg/kg

b) Oxytetracycline 10 to 2000 μg/kg

c) Chlortetracycline 10to 2000 μg/kg

d) Doxycycline

10 to 2000 μg/kg

Laboratory









e) 4-Epitetracycline

IFL C/ QSP SF/ 004 10 to 2000 µg/kg

f) 4-Epichlortetracycline


g) 4-Epioxytetracycline


Trimethoprim In-house Validated Method

IFL/C/QSP SF/007

1.5 to 500 μg/kg

Sulfonamides :

Sulfadiazin In-house Validated Method

IFL/C/QSP SF/007

1.5 to 500 μg/kg

Sulfathiazole 1.5 to 500 μg/kg

Sulfamerazin 1.5 to 500 μg/kg

Sulfamethizole 1.5 to 500 μg/kg

Sulfadimidin/Sulfamethazin 1.5 to 500 μg/kg

Sulfamethoxypyridazin In-house Validated Method

IFL/C/QSP SF/007

1.5 to 500 μg/kg

Sulfachloropyridazin 1.5 to 500 μg/kg

Sulfamethoxazole 1.5 to 500 μg/kg

Sulfadimethoxine 1.5 to 500 μg/kg

Sulfadoxin

1.5 to 500 μg/kg

Oxolinic acid

In-house Validated Method

IFL/C/QSP SF/006

10 to 2000 μg/kg

Nalidixic Acid

10 to 2000 μg/kg

Histamine In-house Validated Method

IFL/C/QSP SF/009

5 to 2000 mg/kg

Laboratory









Indole AOAC 19th

Ed, 981.07

IFL/C/QSP SF/010

10 to 2000 μg/kg

TVBN/ ABVT Annex II 95/149/EC

IFL/C/QSP SF/012

5 to 1000 mg /100g

TMA AOAC 19th

Ed, 971.14

0.5 to 1000 mg /100g

PCBs In-house Validated Method

IFL/C/QSP G/001

0.01 to 1 mg/kg

Quinolones &

Fluoroquinoloes

Oxolinic Acid In-house Validated Method

IFL C/QSP SF/025

10 to 2000 μg/kg

Nalidixic Acid 10 to 2000 μg/kg

Enrofloxacin 10 to 2000 μg/kg

Ciprofloxacin 10 to 2000 μg/kg

Lomefloxacin 10 to 2000 μg/kg

Sarafloxacin 10 to 2000 μg/kg

Flumequin 10 to 2000 μg/kg

Cinoxacin

10 to 2000 μg/kg

Malachite Green and

Leucomalachite Green

In-house Validated Method

IFL C/QSP SF/026

1 to 100 μg/kg

Crystal Violet & Leucocrystal

Violet

1 to 100 μg/kg

Brilliant Green

1 to 100 μg/kg

Laboratory









Sudan I, II, III, IV In-house Validated Method

IFL C/QSP SF/029 by HPLC

0.5 to 1000 mg/kg

Sudan I, II, III, IV In-house Validated Method

IFL C/QSP SF/029 by LCMSMS

0.010 to 100 mg/kg

Pendimethalin In-house Validated Method

IFL C/QSP SF/028

10 to 500 μg/kg

Ethoxyquin AOAC 19th

Ed, 996.13

0.01 to 1000 mg/kg

Mercury AOAC 19th

Ed, 977.15

IFL/C/QSP G/009

0.1 to 100 mg/kg

Arsenic AOAC 19th

Ed, 963.21

IFL/C/QSP G/009

0.1 to 100 mg/kg

Cadmium AOAC 19th

Ed, 972.23

IFL/C/QSP G/009

0.02 to 100mg/kg

Zinc 0.05 to 100 mg/kg

Copper 0.05 to 100 mg/kg

Chromium 0.5 to 100 mg/kg

Nickel 0.5 to 100 mg/kg

Lead 0.06 to 100 mg/kg

Tin 0.1 to 100 mg/kg

Laboratory









Chloride AOAC 19th Ed;

IS 5960 ( 6)-1997

0.1 to 25%

Salt as NaCl AOAC 19th Ed, 937.09

0.1 to 25%

Moisture IS 5960 (Part-5)-2001

AOAC 19th Ed, 950.46

0.1 to 95%

Free Fat IS 5960(Part-4)-1997

0.1 to 50%

Total Fat AOAC 19th

Ed; IS 5960 (3)-1970

0.1 to 50%

Total Ash IS 5960 (Part-2)-2000

0.1 to 25%

Protein AOAC 19th Ed, 928.08

0.1 to 50 %

Residual Sulphite AOAC 19th Ed, 990.28

5 to 1000 mg/kg

Added Phosphate IFL/C/QSP SF/030

100 to 1000 mg/kg

Total Phosphate IFL/C/QSP SF/020

100 to 10000 mg/kg

Sodium AOAC 19th Ed, 969.23

APHA 21st Ed. 3500–Na

and K–B

2 to 5000 mg/kg

Potassium AOAC 19th Ed, 969.23

APHA 21st Ed. 3500 – Na and

K –B IFL/C/QSP SF/021

2 to 5000 mg/kg

Dietary Fibre IS 11062 – 1984

0.2 to 50%

Formaldehyde IFL/C/QSP SF/011

5 to 1000 mg/100 g

Laboratory









2. HONEY AND

HONEY PRODUCTS


IFL/C/QSP HP/001

0.3 to 100 μg/kg


a) 3-Amino- 2

Oxazolidilone(AOZ)


IFL/C/QSP HP/002

1 to 100 μg/kg

b) 3-Amino- 5-

orpholinomethyl – - 2-

oxazolidinone(AMOZ)

1 to 100 μg/kg

c) 1-aminohydantoin(AHD)

1 to 100 μg/kg

d) Semicarbazide(SEM)

1 to 100 μg/kg

Nitrofuran Parent Compounds

:


IFL/C/QSP HP/003

1 to 100 μg/kg

b)Furaltadone 1 to 100 μg/kg

c) NitroFurantoin 1 to 100 μg/kg

d) Furazolidone

1 to 100 μg/kg

Tetracyclines :

a) Tetracycline AOAC 19th Ed, 995.09 10 to 2000 μg/kg


c) Chlortetracycline 10 to 2000 μg/kg

d) Doxycycline

10 to 2000 μg/kg

Streptomycin In-house validated method

IFL/C/QSP HP/004

10 to 500 μg/kg

Laboratory









Trimethoprim In-house validated method

IFL/C/QSP HP/014

1.5 to 500 μg/kg

Sulfonamides :

Sulfadiazin In-house validated method

IFL/C/QSP HP/005

1.5 to 500 μg/kg

Sulfathiazole 1.5 to 500 μg/kg

Sulfamerazin 1.5 to 500 μg/kg

Sulfamethizole 1.5 to 500 μg/kg

Sulfadimidin/Sulfamethazin 1.5 to 500 μg/kg

Sulfamethoxypyridazin 1.5 to 500 μg/kg

Sulfachloropyridazin

1.5 to 500 μg/kg

Sulfamethoxazole In-house validated method

IFL/C/QSP HP/005

1.5 to 500 μg/kg

Sulfadimethoxine 1.5 to 500 μg/kg

Sulfadoxin 1.5 to 500 μg/kg

Sulfanilamide

1.5 to 500 μg/kg

Oxolinic acid In-house validated method

IFL/C/QSP HP/014

10 to 2000 μg/kg

Nalidixic Acid

10 to 2000 μg/kg

Nitroimidazoles:

Metronidazole In-house validated method

IFL C/QSP HP/019

0.5 to 1000 μg/kg

2-Nitroimidazole 0.5 to 1000 μg/kg

Dimetridazole 0.5 to 1000 μg/kg

Ronidazole 0.5 to 1000 μg/kg

Tinidazole 0.5 to 1000 μg/kg

Tylosin

0.5 to 1000 μg/kg

Laboratory









Tin In-house validated method

IFL C/QSP G/009

0.5 to 1000 μg/kg


Arsenic 100 to 1000 µg/kg

Lead 75 to 500 µg/kg

Cadmium 7.5 to 500 µg/kg

Mercury 6.25 to 500 µg/kg

Copper

250 to 2000 µg/kg

Diastase activity

AOAC 19th Ed, 958.09 4 to 90 DN

Maltose

IS 4941 – 1994 (RA 2002) 0.1 to 50%

Fructose-glucose ratio

IS 4941 – 1994 (RA 2002) 0.5 to 2.0

Fructose

IS 4941 – 1994 (RA 2002) 5 to 75 %

Glucose

IS 4941 – 1994 (RA 2002) 5 to 75 %

Colour IFL C/QSP HP/018 1 to 120 mm

Pfund scale

Water insoluble matter IFL C/QSP HP/017

0.005 to 20 %

Foreign material /

Fragments of insects

IS 4941 – 1994 (RA 2002) 0.1 to 5%

Qualitative by visual

Feihe's Test IS 4941-1994 (RA 2002)

Qualitative

Optical density @ 660nm

IS 4941-1994 (RA 2002) 0.01 to 1

Specific gravity

IS 4941-1994 (RA 2002) 0.6 to 2

Laboratory









Moisture

IS 4941-1994 (RA 2002) 0.1 to 75 %

Total Reducing Sugar

IS 4941-1994 (RA 2002) 0.1 to 75%

Ash

IS 4941-1994 (RA 2002) 0.1 to 25 %

Hydroxymethyl furfural

(HMF)

AOAC 19th Ed, 980.23 1.0 to 500 mg/kg

Acidity

IS 4941-1994 (RA 2002) 0.1 to 25 %

Sucrose

IS 4941-1994 (RA 2002) 0.1 to 50 %

Monosodium glutamate DGHS MANUAL 2005,

No.8, 7.2

0.1 to 25%

3. Milk and Milk

Products Including

Milk Powder, Toned

Milk, Skimmed Milk,

Evaporated Milk,

Sweetened Condensed

Milk, Dairy Based

Desserts/ Confections


IFL/C/QSP MLP/008

0.3 to 100 μg/kg


a) 3-Amino- 2-Oxazolidilone

(AOZ)


IFL/C/QSP MLP/001

1 to 100 μg/kg

b) 3-Amino- 5-

morpholinomethyl - 2-

oxazolidinone (AMOZ)

1 to 100 μg/kg

c)1-aminohydantoin (AHD)

1 to 100 μg/kg

d) Semicarbazide (SEM)

1 to 100 μg/kg

Laboratory











IFL/C/QSP MLP/002

1 to 100 μg/kg

b) Furaltadone 1 to 100 μg/kg

c) Furantoin 1 to 100 μg/kg

d) Furazolidone

1 to 100 μg/kg

Tetracyclines :



c) Chlortetracycline

10 to 2000 μg/kg


IFL/C/QSP MLP/004

1.5 to 500 µg/kg

Sulfonamides :


IFL/C/QSP MLP/004

1.5 to 500 µg/kg

Sulfathiazole 1.5 to 500 µg/kg

Sulfapyridin 1.5 to 500 µg/kg

Sulfamerazin 1.5 to 500 µg/kg

Sulfamethizole 1.5 to 500 µg/kg

Sulfadimidin/Sulfamethazin 1.5 to 500 µg/kg

Sulfamethoxypyridazin 1.5 to 500 µg/kg

Sulfachloropyridazin 1.5 to 500 µg/kg

Sulfamethoxazole 1.5 to 500 µg/kg

Sulfadimethoxine 1.5 to 500 µg/kg

Sulfadoxin

1.5 to 500 µg/kg


IFL/C/QSP MLP/007

1.5 to 500 µg/kg

Nalidixic Acid

1.5 to 500 µg/kg

Laboratory









Aflatoxin M1 In-house validated method

IFL/C/QSP MLP/005

Milk : 0.005 to 100 µg/l

Milk powder :

0.05 to 100 µg/kg

Aflatoxins B1, B2, G1, G2 ASTA 4th

Ed, 1997

0.5 to 1000 μg/kg

Ochratoxin A IFL C/QSP S/020

0.25 to 100 μg/kg

Fat IS 11721-1986

0.1 to 50 %

Total Solids IS 12333-1997

0.1 to 50 %

Non-fat solids IS 12333-1997

0.1 to 50 %

Moisture DGHS MANUAL 2005, 2005,

No. 1, 2.1/ IS 11623:1986

(RA 2003)

0.1 to 50 %

Total milk protein DGHS MANUAL 2005,

No.1, 2.1

0.1 to 50 %

Milk fat DGHS MANUAL 2005,

No. 1, 1.7

0.1 to 50 %

Total ash DGHS MANUAL 2005,

No. 1, 9.0

0.1 to 50 %

Ash insoluble in dil HCl DGHS MANUAL 2005,

No. 1, 9.0

0.1 to 50 %

Laboratory









Added colour DGHS MANUAL 2005,

No. 8, 4.2

Qualitative

Milk Solids IS 12333:1997

0.1 to 50 %

Titrable acidity(for milk

powder)

DGHS MANUAL 2005,

No. 1, 9.0

0.01 to 25%

Insolubility Index

(for milk powder)

ISO 8156:2005 0.5 to 25 ml

Wt/Vol (for dairy based

desserts)

DGHS MANUAL 2005,

No. 1, 6.0

0.1 to 5000 g/L

Melamine ISO 15495:2010

0.1 to 100 mg/kg

Mercury In-house validated method

IFL/C/QSP G/009

0.025 to 100 mg/kg

Arsenic AOAC 19th Ed, 986.15

0.025 to 100 mg/kg

Lead AOAC 19th Ed, 972.23

0.2 to 100 mg/kg

Tin AOAC 19th Ed, 980.19

0.05 to 100 mg/kg

Cadmium AOAC 19th Ed, 969.32

0.025 to 100 mg/kg

Zinc AOAC 19th Ed, 969.32

0.05 to 100 mg/kg

Copper AOAC 19th Ed, 969.32 0.05 to 100 mg/kg

Laboratory









4. EGG AND EGG

PRODUCTS

Chloramphenicol

IFL/C/QSP EP/011 0.3 to 100 μg/kg


a) 3-Amino- 2-Oxazolidilone

(AOZ)


IFL/C/QSP EP/012

1 to 100 μg/kg

b) 3-Amino- 5-

morpholinomethyl

- 2- oxazolidinone(AMOZ)

1 to 100 μg/kg

c) 1-aminohydantoin(AHD) In-house validated method

IFL/C/QSP EP/012

1 to 100 μg/kg

d) Semicarbazide(SEM) 1 to 100 μg/kg



IFL/C/QSP EP/015

1 to 100 μg/kg

b) Furaltadone 1 to 100 μg/kg

c) Furantoin 1 to 100 μg/kg

d) Furazolidone

1 to 100 μg/kg

Tetracyclines :



c) Chlortetracycline

10 to 2000 μg/kg


IFL/C/QSP EP/013

1.5 to 500 µg/kg

Sulfonamides :


IFL/C/QSP EP/013

1.5 to 500 µg/kg

Sulfathiazole 1.5 to 500 µg/kg

Sulfamerazin 1.5 to 500 µg/kg

Sulfamethizole 1.5 to 500 µg/kg

Laboratory









Sulfadimidin/Sulfamethazin In-house validated method

IFL/C/QSP EP/013

1.5 to 500 µg/kg

Sulfamethoxypyridazin 1.5 to 500 µg/kg

Sulfachloropyridazin 1.5 to 500 µg/kg

Sulfamethoxazole 1.5 to 500 µg/kg

Sulfadimethoxine 1.5 to 500 µg/kg

Sulfadoxin

1.5 to 500 µg/kg


IFL/C/QSP EP/016

10 to 2000 µg/kg

Nalidixic Acid 10 to 2000 µg/kg

Mercury IFL/C/QSP G/009

0.05 to 1000 mg/kg

5. SUGAR/ REFINED

SUGAR

Extraneous matter DGHS MANUAL 2005,

No.3, 1.1

0.05 to 25 %

Dirt, Filth & Iron fillings DGHS MANUAL 2005,

No.3, 1.1

0.05 to 25%

Colouring matter DGHS MANUAL 2005,

No.8, 4.2

Qualitative

Sulphur dioxide DGHS MANUAL 2005,

No.8, 1.5

5 to 1000 mg/kg

Moisture DGHS MANUAL 2005,

No.4, 7.2

0.1 to 25 %

Acid insoluble ash DGHS MANUAL 2005,

No.4, 8.1

0.1 to 25%

Laboratory









Calcium Oxide DGHS MANUAL 2005,

No.4, 7.7

10 to 25 mg/100g

Total Sugar

(Expressed as Sucrose)

DGHS MANUAL 2005,

No.4, 8.2

1 to 100%

Starch DGHS MANUAL 2005, No.4, 11

1 to 70 %

Conductivity

(of sugar solution)

DGHS MANUAL 2005,

No.4, 7.6

2 to 100 (106 mho/cm)

6. HERBAL

PRODUCTS

INCLUDING

AYURVEDIC

FORMULATIONS

Calcium AOAC 19th Ed, 975.03 100 to 2000mg/kg

Chromium IFL C/QSP G/009 2.5 to 1000 mg/kg

Magnesium AOAC 19th Ed, 963.21 100 to 2000mg/kg

Sodium AOAC 19th Ed, 963.21 100 to 20000 mg/kg

Potassium AOAC 19th Ed, 963.21 100 to 20000mg/kg

Copper AOAC 19th Ed, 963.21 1 to 1000 mg/kg

Lead AOAC 19th Ed, 975.03 2.5 to 100 mg/kg

Cadmium IFL C/QSP G/009 0.25 to 100 mg/kg

Zinc AOAC 19th Ed, 963.21 0.25 to 100 mg/kg

Arsenic AOAC 19th Ed, 963.21 0.1 to 100 mg/kg

Manganese AOAC 19th Ed, 963.21 0.5 to 100 mg/kg

Iron AOAC 19th Ed, 963.21 1 to 100 mg/kg

Nickel AOAC 19th Ed, 963.21 5 to 100 mg/kg

Mercury AOAC 19th Ed, 963.21 0.1 to 500 mg/kg

Laboratory









PESTICIDES RESIDUES

7. MARINE AND

FARMED

AQUATIC

PRODUCTS

Organochlorine Pesticides:

α-HCH IFL/C/QSP G/007 0.01 to 1 mg/kg

β-HCH 0.01 to 1 mg/kg

γ-HCH (Lindane) 0.01 to 1 mg/kg

δ-HCH 0.01 to 1 mg/kg

o,p'- DDT 0.01 to 1 mg/kg

p,p' - DDT 0.01 to 1 mg/kg

o,p'- DDE 0.01 to 1 mg/kg

p,p'- DDE 0.01 to 1 mg/kg

o,p'- DDD 0.01 to 1 mg/kg

p,p' - DDD 0.01 to 1 mg/kg

Endosulfan-α 0.01 to 1 mg/kg

Endosulfan-β 0.01 to 1 mg/kg

Endosulfan sulfate 0.01 to 1 mg/kg

Aldrin 0.01 to 1 mg/kg

Dieldrin 0.01 to 1 mg/kg

Endrin 0.01 to 1 mg/kg

Endrin aldehyde 0.01 to 1 mg/kg

Endrin ketone 0.01 to 1 mg/kg

Cis-Chlordane 0.01 to 1 mg/kg

Trans -Chlordane 0.01 to 1 mg/kg

Heptachlor 0.01 to 1 mg/kg

Heptachlor epoxide 0.01 to 1 mg/kg

Butachlor 0.01 to 1 mg/kg

Alachlor 0.01 to 1 mg/kg

Dicofol 0.01 to 1 mg/kg

Chlorthalonil 0.01 to 1 mg/kg

Dichlofluanid 0.01 to 1 mg/kg

Methoxychlor 0.01 to 1 mg/kg

Vinclozolin 0.01 to 1 mg/kg

Hexachlorobenzene 0.01 to 1 mg/kg

Laboratory









Organophosphorus Pesticides:

Ethion IFL/C/QSP G/007 0.01 to 1 mg/kg

Dichlorvos 0.01 to 1 mg/kg

Chlorpyrifos 0.01 to 1 mg/kg

Chlorpyrifos-Methyl 0.01 to 1 mg/kg

Monocrotophos 0.01 to 1 mg/kg

Malathion 0.01 to 1 mg/kg

Parathion 0.01 to 1 mg/kg

Methyl parathion 0.01 to 1 mg/kg

Azinphos-methyl 0.01 to 1 mg/kg

Quinalphos 0.01 to 1 mg/kg

Triazophos 0.01 to 1 mg/kg

Fenchlorphos 0.01 to 1 mg/kg

Diazinon 0.01 to 1 mg/kg

Dimethoate 0.01 to 1 mg/kg

Ethoprophos 0.01 to 1 mg/kg

Disulfoton 0.01 to 1 mg/kg

Prothiofos 0.01 to 1 mg/kg

Phorate 0.01 to 1 mg/kg

Phorate sulfone 0.01 to 1 mg/kg

Phorate sulfoxide 0.01 to 1 mg/kg

Methylparaoxon 0.01 to 1 mg/kg

Malaoxon 0.01 to 1 mg/kg

Phosalone 0.01 to 1 mg/kg

Triademefon 0.01 to 1 mg/kg

Chlorfenvinphos 0.01 to 1 mg/kg

Profenofos 0.01 to 1 mg/kg

Mevinphos 0.01 to 1 mg/kg

Methamidophos 0.01 to 1 mg/kg

Iprobenfos 0.01 to 1 mg/kg

Laboratory









Acephate IFL/C/QSP G/007 0.01 to 1 mg/kg

Omethoate 0.01 to 1 mg/kg

Fenitrothion 0.01 to 1 mg/kg

Coumaphos 0.01 to 1 mg/kg

Phosphamidon

0.01 to 1 mg/kg

Pyrethroids:

Cypermethrin IFL/C/QSP G/007 0.01 to 1 mg/kg

Deltamethrin 0.01 to 1 mg/kg

Cyfluthrin 0.01 to 1 mg/kg

Cyhalothrin-lambda 0.01 to 1 mg/kg

Permethrin 0.01 to 1 mg/kg

Fenvalerate 0.01 to 1 mg/kg

Esfenvalerate 0.01 to 1 mg/kg

Fenpropathrin 0.01 to 1 mg/kg

Flumethrin 0.01 to 1 mg/kg

Fluvalinate

0.01 to 1 mg/kg

Other Pesticides:

Atrazine IFL/C/QSP G/007 0.01 to 1 mg/kg

Isoproturon 0.01 to 1 mg/kg

Hexaconazole 0.01 to 1 mg/kg

Penconazole 0.01 to 1 mg/kg

Propiconazole 0.01 to 1 mg/kg

Difenoconazol 0.01 to 1 mg/kg

Flusilazole 0.01 to 1 mg/kg

Bitertanol 0.01 to 1 mg/kg

Myclobutanil 0.01 to 1 mg/kg

Fenarimol 0.01 to 1 mg/kg

Captafol 0.01 to 1 mg/kg

Captan 0.01 to 1 mg/kg

Iprodione 0.01 to 1 mg/kg

Laboratory









Benalaxyl IFL/C/QSP G/007 0.01 to 1 mg/kg

Metalaxyl 0.01 to 1 mg/kg

Dimethomorph 0.01 to 1 mg/kg

Fipronil 0.01 to 1 mg/kg

Amitraz 0.01 to 1 mg/kg

Bromopropylate 0.01 to 1 mg/kg

Chlorobenzilate 0.01 to 1 mg/kg

Propargite 0.01 to 1 mg/kg

Trifluralin

0.0001 to 1 mg/kg

Benzo-a-pyrene IFL/C/QSP G/006

0.001 to 1 mg/kg

2-4 D

IFL/C/QSP SF/031 0.01 to 1 mg/kg

8. SPICES, SPICE

PRODUCTS &

CONDIMENTS






o,p'-DDT 0.01 to 1 mg/kg

p,p'-DDT 0.01 to 1 mg/kg

o,p'-DDE 0.01 to 1 mg/kg

p,p'-DDE 0.01 to 1 mg/kg

o,p'-DDD 0.01 to 1 mg/kg

p,p'-DDD 0.01 to 1 mg/kg








Laboratory









Cis-Chlordane IFL/C/QSP G/007 0.01 to 1 mg/kg













4-bromo-2-chlorophenol 0.01 to 1 mg/kg

Hexachlorobenzene 0.01 to 1 mg/kg

4,4'-dichlorobenzophenone

0.01 to 1 mg/kg

Organophosphorus Pesticides :















Laboratory









Ethoprophos IFL/C/QSP G/007 0.01 to 1 mg/kg















Acephate 0.01 to 1 mg/kg


Phosphamidon 0.01 to 1 mg/kg



Etrimfos 0.01 to 1 mg/kg

Oxydematon-methyl 0.01 to 1 mg/kg

Phenthoate 0.01 to 1 mg/kg

Pirimiphos methyl

0.01 to 1 mg/kg

Pyrethroids:




Cyhalothrin 0.01 to 1 mg/kg




Laboratory









Fluvalinate IFL/C/QSP G/007 0.01 to 1 mg/kg



Ethofenprox 0.01 to 1 mg/kg

Bifenthrin

0.01 to 1 mg/kg

Carbamates :

Carbaryl IFL/C/QSP G/007 0.01 to 1 mg/kg

Carbofuran 0.01 to 1 mg/kg

3-Hydroxy Carbofuran 0.01 to 1 mg/kg

Aldicarb 0.01 to 1 mg/kg

Aldicarb sulfone 0.01 to 1 mg/kg

Aldicarb sulfoxide 0.01 to 1 mg/kg

Carbosulfan 0.01 to 1 mg/kg

Propoxur 0.01 to 1 mg/kg

Methomyl 0.01 to 1 mg/kg

Oxamyl 0.01 to 1 mg/kg

Thiodicarb 0.01 to 1 mg/kg

Indoxacarb 0.01 to 1 mg/kg

Methiocarb 0.01 to 1 mg/kg

Ethylene Thiourea

0.01 to 1 mg/kg

Dithiocarbamates:

Maneb IFL C/QSP G/008 0.025 to 1 mg/kg

Mancozeb 0.025 to 1 mg/kg

Propineb 0.025 to 1 mg/kg

Ziram 0.025 to 1 mg/kg

Thiram 0.025 to 1 mg/kg

Metiram

0.025 to 1 mg/kg

Benfuracarb

IFL/C/QSP G/007

0.01 to 1 mg/kg

Laboratory









Other Pesticides & chemicals:





Difenoconazole 0.01 to 1 mg/kg









Benalaxyl 0.01 to 1 mg/kg

Metalaxyl 0.01 to 1 mg/kg






Simazine 0.01 to 1 mg/kg

Imazalil 0.01 to 1 mg/kg

Tebuconazole 0.01 to 1 mg/kg

Triadimenol 0.01 to 1 mg/kg

Acetamiprid 0.01 to 1 mg/kg

Thiacloprid 0.01 to 1 mg/kg

Buprofezin 0.01 to 1 mg/kg

Cartap HCl 0.01 to 1 mg/kg

Abamectin 0.01 to 1 mg/kg

Azoxystrobin 0.01 to 1 mg/kg

Flufenoxuron 0.01 to 1 mg/kg

Laboratory









Oxyfluorfen IFL/C/QSP G/007 0.01 to 1 mg/kg

Fenpyromixate 0.01 to 1 mg/kg

Demeton-S-methyl 0.01 to 1 mg/kg

Ethephon 0.01 to 1 mg/kg

Fenthion 0.01 to 1 mg/kg

Matalaxyl-M/Mefenoxam 0.01 to 1 mg/kg

Tridemorph 0.01 to 1 mg/kg

Carbendazim 0.01 to 1 mg/kg

Benomyl 0.01 to 1 mg/kg

Thiophenate – Methyl 0.01 to 1 mg/kg

Cymoxanil 0.01 to 1 mg/kg

Clothianidin 0.01 to 1 mg/kg

Imidacloprid 0.01 to 1 mg/kg

Thiamethoxam 0.01 to 1 mg/kg

Dinocap 0.01 to 1 mg/kg

Diafenthiuron 0.01 to 1 mg/kg

Emamectin Benzoate 0.01 to 1 mg/kg

Spinosad A 0.01 to 1 mg/kg

Spinosad B 0.01 to 1 mg/kg

Chlorfenapyr 0.01 to 1 mg/kg

Trifluralin 0.01 to 1 mg/kg

Biphenyl 0.01 to 1 mg/kg

Folpet 0.01 to 1 mg/kg

o-Phenylphenol

(Ortofenifenol)

0.01 to 1 mg/kg

Propaquizafop 0.01 to 1 mg/kg

Thenylchlor 0.01 to 1 mg/kg

Tri-allate 0.01 to 1 mg/kg

Chlorantraniliprole 0.01 to 1 mg/kg

Diflubenzuron 0.01 to 1 mg/kg

Ethoxyquin 0.01 to 1 mg/kg

Famoxadone 0.01 to 1 mg/kg

Laboratory









Fenamidone IFL/C/QSP G/007 0.01 to 1 mg/kg

Flubendiamide 0.01 to 1 mg/kg

Kresoxim-methyl 0.01 to 1 mg/kg

Lufenuron 0.01 to 1 mg/kg

Milbemectin 0.01 to 1 mg/kg

Novaluron 0.01 to 1 mg/kg

Pendimethalin 0.01 to 1 mg/kg

Pyraclostrobin 0.01 to 1 mg/kg

Spiromesifen 0.01 to 1 mg/kg

Pyriproxifen 0.01 to 1 mg/kg

Trifloxystrobin 0.01 to 1 mg/kg

Azadirachtin

0.01 to 1 mg/kg

Streptomycin EURL-SRM Method 0.01 to 1 mg/kg

Streptomycin sulphate 0.01 to 1 mg/kg

Kasugamycin

0.01 to 1 mg/kg

Tetracycline AOAC 19TH ED, 995.09

0.01 to 1 mg/kg

Black Sulphur (as S) Manual of Pesticides Residue

Analysis, VCH

10 to 100 mg/kg

9. EGG & EGG

PRODUCTS











Laboratory









p,p' - DDD IFL/C/QSP G/007 0.01 to 1 mg/kg









cis-Chlordane 0.01 to 1 mg/kg

trans-Chlordane 0.01 to 1 mg/kg








Dichlofluanid

0.01 to 1 mg/kg




Chlorpyriphos 0.01 to 1 mg/kg









Laboratory









Dimethoate IFL/C/QSP G/007 0.01 to 1 mg/kg




Pirimiphos-methyl 0.01 to 1 mg/kg


Edifenphos

0.01 to 1 mg/kg

Pyrethroids:




Cyhalothrin-lambda 0.01 to 1 mg/kg



Fenvalarate 0.01 to 1 mg/kg

Esfenvalarate

0.01 to 1 mg/kg

Other Pesticides:





2,4-D

0.01 to 1 mg/kg

10. HONEY & HONEY

PRODUCTS


α-HCH IFL C/QSP G/007 0.003 to 1.0 mg/kg

β-HCH 0.003 to 1.0 mg/kg

γ-HCH (Lindane) 0.003 to 1.0 mg/kg

δ-HCH 0.003 to 1.0 mg/kg


Hexachlorobenzene 0.003 to 1.0 mg/kg

Vinclozolin 0.005 to 1.0 mg/kg

Laboratory









p,p’ – DDT IFL C/QSP G/007 0.003 to 1.0 mg/kg

p,p’ – DDE 0.003 to 1.0 mg/kg

p,p’ – DDD 0.003 to 1.0 mg/kg

o,p’ – DDT 0.003 to 1.0 mg/kg

o,p' – DDE 0.003 to 1.0 mg/kg

o,p' – DDD 0.003 to 1.0 mg/kg

Aldrin 0.003 to 1.0 mg/kg

Dieldrin 0.003 to 1.0 mg/kg

Endosulfan-α 0.003 to 1.0 mg/kg

Endosulfan-β 0.003 to 1.0 mg/kg

Heptachlor 0.003 to 1.0 mg/kg

Heptachlor epoxide 0.003 to 1.0 mg/kg

trans -Chlordane 0.003 to 1.0 mg/kg

cis-Chlordane 0.003 to 1.0 mg/kg

Endrin 0.003 to 1.0 mg/kg

Endosulfan sulfate

0.003 to 1.0 mg/kg


Coumaphos IFL C/QSP G/007 0.01 to 1 mg/kg


Phosalone

0.01 to 1 mg/kg

Pyrethroids :

Cyfluthrin IFL C/QSP G/007 0.005 to 1 mg/kg

Cypermethrin 0.005 to 1 mg/kg




Fluvalinate 0.005 to 1 mg/kg

Cyhalothrin

0.005 to 1 mg/kg

Laboratory









Carbamates :

Carbofuran IFL C/QSP G/007 0.01 to 1 mg/kg


Carbaryl

0.01 to 1 mg/kg

Other Pesticides :

Amitraz IFL C/QSP G/007 0.01 to 1 mg/kg


Chinomethionate 0.01 to 1 mg/kg

Cymiazole

0.01 to 1 mg/kg

11. TEA, COFFEE,

COCOA

PRODUCTS


α-HCH IFL C/QSP G/007 0.01 to 1 mg/kg














cis-Chlordane 0.01 to 1 mg/kg

trans-Chlordane 0.01 to 1 mg/kg


Heptachlor Epoxide

0.01 to 1 mg/kg

Laboratory









Endosulfan sulfate IFL C/QSP G/007 0.01 to 1 mg/kg

Endrin Aldehyde 0.01 to 1 mg/kg

Endrin Ketone 0.01 to 1 mg/kg








4-bromo-2-chlorophenol

0.01 to 1 mg/kg


Ethion IFL C/QSP G/007 0.01 to 1 mg/kg


Chlorpyriphos 0.01 to 1 mg/kg

Monocrotophos

0.01 to 1 mg/kg

Malathion IFL C/QSP G/007 0.01 to 1 mg/kg

Parathion-Methyl 0.01 to 1 mg/kg










Chlorpyriphos-methyl 0.01 to 1 mg/kg



Laboratory









Phorate Sulfone IFL C/QSP G/007 0.01 to 1 mg/kg

Phorate Sulfoxide 0.01 to 1 mg/kg

Methyl Paraoxon 0.01 to 1 mg/kg



Triadimefon 0.01 to 1 mg/kg






Iprobenphos 0.01 to 1 mg/kg




Isocarbophos 0.01 to 1 mg/kg

Glyphosate 0.01 to 1 mg/kg

Glufosinate-ammonium

0.01 to 1 mg/kg

Pyrethroids:

Cypermethrin IFL C/QSP G/007 0.01 to 1 mg/kg



Cyhalothrin 0.01 to 1 mg/kg



Fenvalarate 0.01 to 1 mg/kg

Esfenvalarate 0.01 to 1 mg/kg


Bifenthrin 0.01 to 1 mg/kg

Etofenprox 0.01 to 1 mg/kg

Laboratory









Carbamates:

Carbaryl IFL C/QSP G/007 0.01 to 1 mg/kg





Carbosulfan

0.01 to 1 mg/kg

Dithiocarbamates:

Maneb IFL C/QSP G/008 0.025 to 1mg/kg

Mancozeb 0.025 to 1mg/kg

Propineb 0.025 to 1mg/kg

Ziram 0.025 to 1mg/kg

Isoprocarb

0.025 to 1mg/kg

Other Pesticides:

Atrazine IFL C/QSP G/007 0.01 to 1 mg/kg


Methidathion 0.01 to 1 mg/kg










Chlorfenapyr 0.01 to 1 mg/kg



Laboratory









Ethephon IFL C/QSP G/007 0.01 to 1 mg/kg

Pyridaben 0.01 to 1 mg/kg

Tetradifon 0.01 to 1 mg/kg

S 421 0.01 to 1 mg/kg

Carbendazim, total 0.01 to 1 mg/kg



Fenazaquin 0.01 to 1 mg/kg

Imidacloprid, total 0.01 to 1 mg/kg


Thiametoxam 0.01 to 1 mg/kg


2,4-D, total 0.01 to 1 mg/kg

Diflubenzuron

0.01 to 1 mg/kg

12. FRUITS, FRUIT

PRODUCTS

& VEGETABLES


α-HCH IFL C/QSP G/013 0.01 to 1 mg/kg
















Laboratory









Cis-Chlordane IFL C/QSP G/013 0.01 to 1 mg/kg




o,p'-Dicofol 0.01 to 1 mg/kg

p,p'-Dicofol 0.01 to 1 mg/kg










Hexachlorobenzene

0.01 to 1 mg/kg


4-bromo-2-chlorophenol IFL C/QSP G/013 0.01 to 1 mg/kg








Ethion 0.01 to 1 mg/kg






Laboratory









Methamidophos IFL C/QSP G/013 0.01 to 1 mg/kg





Parathion-ethyl 0.01 to 1 mg/kg




Phosphamidon 0.01 to 1 mg/kg




Oxydematon-methyl 0.01 to 1 mg/kg










Demeton-S-methyl 0.01 to 1 mg/kg

Edifenphos 0.01 to 1 mg/kg

Fenthion Oxon 0.01 to 1 mg/kg

Fenthion Sulfone 0.01 to 1 mg/kg

Fenthion Sulfoxide 0.01 to 1 mg/kg

Glufosinate-ammonium 0.01 to 1 mg/kg

3- (methylphosphinico)

propionic acid

0.01 to 1 mg/kg

Laboratory









Glyphosate IFL C/QSP G/013 0.01 to 1 mg/kg

Aminomethylphosphonic acid

(AMPA)

0.01 to 1 mg/kg

Demeton-S-methylsulfone 0.01 to 1 mg/kg


Phorate-oxon 0.01 to 1 mg/kg


Propetamphos 0.01 to 1 mg/kg

Temephos 0.01 to 1 mg/kg

Thiometon 0.01 to 1 mg/kg

Fosetyl-Al 0.01 to 1 mg/kg

Formothion

0.01 to 1 mg/kg

Pyrethroids:

Cypermethrin IFL C/QSP G/013 0.01 to 1 mg/kg



lambda-Cyhalothrin 0.01 to 1 mg/kg




Fluvalinate 0.01 to 1 mg/kg


Ethofenprox 0.01 to 1 mg/kg


Allethrin 0.01 to 1 mg/kg

Bioallethrin 0.01 to 1 mg/kg

Bifenthrin 0.01 to 1 mg/kg

Transfluthrin

0.01 to 1 mg/kg

Laboratory









Carbamates:

Carbaryl IFL C/QSP G/013 0.01 to 1 mg/kg


3-Hydroxy Carbofuran 0.01 to 1 mg/kg



Carbosulfan 0.01 to 1 mg/kg


Indoxacarb 0.01 to 1 mg/kg


Benomyl

0.01 to 1 mg/kg

Dithiocarbamates:

Maneb IFL C/QSP G/008 0.025 to 1 mg/kg

Mancozeb 0.025 to 1 mg/kg

Propineb 0.025 to 1 mg/kg

Ziram 0.025 to 1 mg/kg

Metiram 0.025 to 1 mg/kg

Thiram 0.025 to 1 mg/kg

Zineb 0.025 to 1 mg/kg


Aldicarb sulfone 0.01 to 1 mg/kg

Aldicarb sulfoxide 0.01 to 1 mg/kg

Methiocarb 0.01 to 1 mg/kg

Oxamyl 0.01 to 1 mg/kg

Ethylene Thiourea 0.01 to 1 mg/kg

Bendiocarb 0.01 to 1 mg/kg

Benfuracarb 0.01 to 1 mg/kg

Dazomet 0.01 to 1 mg/kg

Metam 0.01 to 1 mg/kg

Methylisothiocyanate 0.01 to 1 mg/kg

Fenobucarb 0.01 to 1 mg/kg

Laboratory









Iprovalicarb IFL C/QSP G/008 0.01 to 1 mg/kg

Thiobencarb (Benthiocarb)

0.01 to 1 mg/kg

Other Pesticides:

Atrazine IFL C/QSP G/013 0.01 to 1 mg/kg












Benalaxyl & Benalaxyl-M 0.01 to 1 mg/kg

Metalaxyl & Metalaxyl-M 0.01 to 1 mg/kg






Simazine 0.01 to 1 mg/kg

Tebuconazole 0.005 to 1 mg/kg



Thiacloprid 0.01 to 1 mg/kg


Cartap Hydrochloride 0.01 to 1 mg/kg

Abamectin 0.01 to 1 mg/kg

Azoxystrobin 0.01 to 1 mg/kg

Laboratory









Flufenoxuron IFL C/QSP G/013 0.01 to 1 mg/kg

Oxyfluorfen 0.01 to 1 mg/kg

Fenpyromixate 0.01 to 1 mg/kg

Ethephon 0.01 to 1 mg/kg

Tridemorph 0.01 to 1 mg/kg

Thiophanate – methyl 0.01 to 1 mg/kg

Cymoxanil 0.01 to 1 mg/kg



Thiamethoxam 0.01 to 1 mg/kg

Dinocap 0.01 to 1 mg/kg

Diafenthiuron 0.01 to 1 mg/kg

Emamectin Benzoate 0.01 to 1 mg/kg

Spinosad A 0.01 to 1 mg/kg

Spinosad D 0.01 to 1 mg/kg



Imazalil 0.01 to 1 mg/kg

Flufenzine 0.01 to 1 mg/kg

Oxycarboxin 0.01 to 1 mg/kg

Propanil 0.01 to 1 mg/kg

Paclobutrazol 0.01 to 1 mg/kg

Fenamidone 0.01 to 1 mg/kg

Famoxadone 0.01 to 1 mg/kg

Meptyldinocap 0.01 to 1 mg/kg

Diuron 0.01 to 1 mg/kg

3,4- dichloroaniline 0.01 to 1 mg/kg

Iodosulfuron-methyl 0.01 to 1 mg/kg

Linuron 0.01 to 1 mg/kg

Lufenuron 0.01 to 1 mg/kg

Pencycuron 0.01 to 1 mg/kg

Kresoxim methyl 0.01 to 1 mg/kg

Laboratory









Pyraclostrobin IFL C/QSP G/013 0.01 to 1 mg/kg

Trifloxystrobin 0.01 to 1 mg/kg

Fipronil Sulfone 0.005 to 1 mg/kg



Carboxin 0.01 to 1 mg/kg

Flufenacet 0.01 to 1 mg/kg

Metolachlor 0.01 to 1 mg/kg

S-Metolachlor 0.01 to 1 mg/kg


1-Naphthylacetic acid 0.01 to 1 mg/kg

2,4-D & esters 0.01 to 1 mg/kg

6-Benzyl adenine 0.01 to 1 mg/kg

Azadirachtin 0.01 to 1 mg/kg

Bifenazate 0.01 to 1 mg/kg

Chlormequat 0.01 to 1 mg/kg

Diflubenzuron 0.01 to 1 mg/kg

Homobrassinolide 0.01 to 1 mg/kg

Diquat 0.01 to 1 mg/kg

Dithianon 0.01 to 1 mg/kg

Dodine 0.01 to 1 mg/kg

Fenazaquin 0.01 to 1 mg/kg

Flubendiamide 0.01 to 1 mg/kg

Forchlorfenuron 0.01 to 1 mg/kg

Gibberellic acid 0.01 to 1 mg/kg

Hexythiazox 0.01 to 1 mg/kg

Hydrogen cyanamide 0.01 to 1 mg/kg

Isoprothiolane 0.01 to 1 mg/kg

Mandipropamid 0.01 to 1 mg/kg

Mepiquat 0.01 to 1 mg/kg

Metribuzin 0.01 to 1 mg/kg

Milbemectin 0.01 to 1 mg/kg

Laboratory









Oxadiazon IFL C/QSP G/013 0.01 to 1 mg/kg

Paraquat 0.01 to 1 mg/kg

Pyriproxyfen 0.01 to 1 mg/kg

Spiromesifen 0.01 to 1 mg/kg

Trichlorfon 0.01 to 1 mg/kg

Tricyclazole 0.01 to 1 mg/kg

Uracil 0.01 to 1 mg/kg

Sulphur 0.01 to 1 mg/kg

Chlorantraniliprole 0.01 to 1 mg/kg

Tetraconazole 0.01 to 1 mg/kg

Cyazofamid 0.01 to 1 mg/kg

Dinotefuran 0.01 to 1 mg/kg

Flonicamid 0.01 to 1 mg/kg

Chlorfenapyr

0.01 to 1 mg/kg

Inorganic bromide DGHS MANUAL 2005,

No.8, 10.0

Vogel’s Textbook of Quantitative

Chemical Analysis, 6th

Ed.

1 to 1.0 mg/kg

13. MILK & MILK

PRODUCTS


Lindane (γ-HCH) IFL/C/QSP G/007 0.01 to 1 mg/kg





Cis-Chlordane 0.01 to 1 mg/kg





Laboratory









β-HCH IFL/C/QSP G/007 0.01 to 1 mg/kg



α-HCH 0.01 to 1 mg/kg



p,p' - DDD

0.01 to 1 mg/kg













Edifenphos 0.01 to 1 mg/kg




Trichlorfon

0.01 to 1 mg/kg

Other Pesticides :


Fenvalerate

0.01 to 1 mg/kg

Laboratory









Carbofuran IFL/C/QSP G/007 0.01 to 1 mg/kg



2,4-D 0.01 to 1 mg/kg

Paraquat dichloride 0.01 to 1 mg/kg

14. FOOD GRAINS,

CEREALS, PULSES

& CEREAL BASED

FOOD

PRODUCTS


Monocrotophos IFL/C/QSP G/007 0.01 to 1 mg/kg





Thiometon 0.01 to 1 mg/kg

Oxydemeton methyl

0.01 to 1 mg/kg

Carbamates :

Carbaryl IFL/C/QSP G/007 0.01 to 1 mg/kg

Carbofuran

0.01 to 1 mg/kg

Dithiocarbamates

IFL/C/QSP G/008 0.025 to 1.0 mg/kg

Other Pesticides :

Carbendazim IFL/C/QSP G/007 0.01 to 1 mg/kg


2,4-D 0.01 to 1 mg/kg

Paraquat Dichloride

0.01 to 1 mg/kg

15. EDIBLE OIL &

EDIBLE FAT



Phenthoate IFL/C/QSP G/007 0.01 to 1 mg/kg


Laboratory









Carbamates :

Carbofuran IFL/C/QSP G/007 0.01 to 1 mg/kg

Thiodicarb

0.01 to 1 mg/kg

Other Pesticides:

Indoxacarb IFL/C/QSP G/007 0.01 to 1 mg/kg



Oxyfluorfen 0.01 to 1 mg/kg


Metribuzin 0.01 to 1 mg/kg

Metolachlor 0.01 to 1 mg/kg

Spinosad 0.01 to 1 mg/kg

Thiochlorprid 0.01 to 1 mg/kg


Paraquat Dichloride

0.01 to 1 mg/kg

16. SPICES, SPICE

PRODUCTS &

CONDIMENTS

(Black pepper, Chilly,

Cumin white, Cumin

black, Fennel,

Fenugreek, Ginger

dried, Nutmeg,

Saffron, Turmeric,

Curry powders, Dried

mango ) in whole and

powdered form

Capsaicin ASTA 4th Ed: Method 21.3

1000 SHU to 10m SHU

Mycotoxins

Aflatoxins B1, B2, G1, G2

ASTA 4th Ed, 1997 0.5 to 1000 μg/kg

Ochratoxin A

IFL C/QSP S/020 0.25 to 1000 μg/kg

Sudan I ASTA 4th

Ed: Method 28.0 HPLC: 1 to 100 mg/kg

LCMS : 0.01 to 10 mg/kg

Sudan II HPLC : 1 to 100 mg/kg


Sudan III HPLC : 1 to 100 mg/kg


Sudan IV HPLC : 1 to 100 mg/kg


Laboratory









Rhodamine B IFLC/QSP/S/ 006

J. Mass Spec. 2005,40,866 – 875

0.01 to 1 mg/kg

Sudan Red 7B ASTA 4th

Ed: Method 28.0

0.5 to 100 mg/kg

Sudan Orange G ASTA 4th

Ed: Method 28.0

1 to 100 mg/kg

Butter Yellow ASTA 4th

Ed: Method 28.0

1 to 100 mg/kg

Para Red ASTA 4th

Ed: Method 28.0

0.5 to 100 mg/kg

Total Ash ASTA 4th

Ed: Method 3.0

0.1 to 20%

Acid insoluble Ash ASTA 4th

Ed: Method 4.0

0.1 to 20 %

Crude Fibre ASTA 4th

Ed: Method 7.0

0.1 to 50 %


0.2 to 50 %

Piperine ASTA 4th

Ed: Method 12.1

0.1 to 50 %

Non volatile Methylene

Chloride Extract

ASTA 4th

Ed: Method 11.0 0.1 to 10 %

Volatile oil ASTA 4th

Ed: Method 5.0

0.1 to 25%

Curcumin

ASTA 4th

Ed Method 18.0

0.1 to 95 %

Laboratory









Cadmium AOAC 19th Ed,

977.15/971.20/975.03

IFL C/QSP G/009

0.25 to 100 mg/kg

Mercury 0.1 to 100 mg/kg

Arsenic 0.1 to 100 mg/kg

Lead 0.75 to 100 mg/kg

Copper 0.5 to 100 mg/kg

Chromium 2.5 to 100 mg/kg


Tin 0.5 to 100 mg/kg

Iron

1 to 250 mg/kg

Extraneous Matter ASTA 4th Ed. 14.0 1 to 25 %

Insect Damaged matter ASTA 4th Ed. 14.0 1 to 100 %

Light Berries ASTA 4th Ed. 14.0 1 to 50 %

Moisture ASTA 4th

Ed. 2.0 0.1 to 25 %

Lead Chromate Test in

Turmeric

IS : 3576, 1994 Qualitative

Added colour DGHS No.8, 4.2 Qualitative

Cold water soluble extract IS 1797 - 1985 1 to 80 %

Water soluble ash IS : 1797- 1985,RA 2001 0.1 to 60 %

Calcium as CaO IS 1797 - 1985 0.01 to 25 %

Alcohol soluble extract IS 1797 - 1985 1.0 to 50%

Total Nitrogen IFLC/QSP SF/ 018 0.1 to 50 %

Laboratory









Non-volatile ether extract ASTA 4th

Ed: Method 11.0 0.1 to 50 %

Common salt IS 1797 - 1985 0.1 to 50 %

Starch ASTA 4th

Ed: Method 8.0 1 to 70%

Sulphur Dioxide AOAC 19th Ed, 962.16 2 to 1000 mg/kg

Insect DGHS MANUAL 2005,

No.10, 2.0

Qualitative

Rodent contamination DGHS MANUAL 2005,

No.10, 2.0

Qualitative

Live or Dead Insect /

Fragments

DGHS MANUAL 2005,

No.10, 2.0

Qualitative

Damaged/discoloured

material

DGHS MANUAL 2005,

No.10, 2.0

Qualitative

Mould AOAC 19th Ed, 968.33

Visual

Peroxidase Test DGHS MANUAL 2005,

No.5, 17.5

Qualitative

Edible seeds other than the

said product

DGHS MANUAL 2005,

No.10, 2.0

0.1 to 100 %

Empty or malformed capsules

in cardamom

DGHS MANUAL 2005,

No.10, 2.0

0.1 to 100 %

Light seeds in cardamom ASTA 4th

Ed: Method 14.0

0.1 to 50 %

Laboratory









Premature and shriveled

capsules in cardamom

DGHS MANUAL 2005,

No.10, 2.0

0.1 to 50 %

Unripe & marked chilly DGHS MANUAL 2005,

No.10, 2.0

0.1 to 100 %

Broken fruits/ Seeds/

Fragments of chilly

DGHS MANUAL 2005,

No.10, 2.0

0.1 to 100 %

Tendrils, Mother Cloves DGHS MANUAL 2005,

No.10, 2.0

0.1 to 100 %

Headless cloves DGHS MANUAL 2005,

No.10, 2.0

0.1 to 50 %

Khokar Cloves DGHS MANUAL 2005, No.10, 2

0.1 to 50 %

Split fruits of coriander

DGHS MANUAL 2005, No.10, 2 0.1 to 50 %

Nutmeg in mace %w/w

DGHS MANUAL 2005, No.10, 2 0.1 to 50 %

Allyl iso-thiocyanate in

mustard

DGHS MANUAL 2005,

No.10, 12.0

0.1 to 50 %

p-hydroxybenzyl iso-

thiocyanate in mustard

DGHS MANUAL 2005,

No.10, 12A

0.1 to 50 %

Argemone seeds in mustard DGHS MANUAL 2005,

No.10, 18.0

0.1 to 50 %

Laboratory









Pin heads or broken berries of

pepper

DGHS MANUAL 2005,

No.10, 2.0

0.1 to 100 %

Bulk density - pepper ASTA 4th

Ed. Method 25.0

100 to 1200 g/l

Other foreign edible seeds -

pepper

DGHS MANUAL 2005,

No.10, 2.0

0.1 to 50 %

Black berries in pepper DGHS MANUAL 2005,

No.10, 2.0

0.1 to 50%

Defective Rhizomes of

turmeric

IS - 3576: 1994

0.1 to 100 %

Dyes:

Auramine IFL C/QSP S/003 10 to 500 µg/kg

Fast Garnet GBC 10 to 500 µg/kg

Metanil Yellow 10 to 500 µg/kg

Orange II 10 to 500 µg/kg

Orange OT 10 to 500 µg/kg

p-Nitroaniline 10 to 500 µg/kg

Rhodamine B 10 to 500 µg/kg

Sudan Black B 10 to 500 µg/kg

Sudan Red B 10 to 500 µg/kg

Sudan Red G 10 to 500 µg/kg

Toluidine Red

10 to 500 µg/kg

17. EDIBLE SALT Moisture ASTA 4th

Ed. Method 2.0

0.1 to 25 %

Sodium Chloride IS : 797 -1982

0.1 to 100%

Iodine content IS : 7224 -1985

5 to 70 mg/kg

Laboratory









Water insoluble matter AOAC 19th Ed, 925.55

0.1 to 20 %

Matter insoluble in dil acid AOAC 19th Ed, 925.55

0.1 to 20 %

Matter soluble in water other

than NaCl

IS : 253 : 1985 0.1 to 20%

18. STIMULANT

FOODS COFFEE,

CHICORY, TEA &

COCOA POWDER

Moisture IS : 2791- 1992, DGHS 4,1.2

0.1 to 25 %

Crude fibre IS 10226 (Part 1 ) - 1982

(RA 2005)

0.1 to 25 %


0.2 to 50 %

Total fat AOAC 19th

Ed , 922.06

0.1 to 25%

Total ash IS 2791 - 1992 (RA 1998)

0.1 to 25 %

Water soluble ash IS 13855-1993 (RA 1998)

0.1 to 60 %

Water insoluble ash IS 13857- 1993 (RA 1998)

0.1 to 60 %

Acid insoluble ash IS 13857-1993 (RA 1998)

0.1 to 60 %

Mycotoxins

Aflatoxins B1, B2, G1, G2

ASTA 4th

Ed, 1997 0.5 to 1000 μg/kg


0.25 to 1000 μg/kg

Sugars AOAC 19th

Ed, 925.15

SP:18 (Part 9)- 1984

0.1 to 75 %

Laboratory









Caffeine IS 2791-1992,

ISO 10727:20029 (E)

0.01 to 50 %

Alkalinity of water soluble

ash

IS 13856-1993 (RA 1998) 3.5 to 5.5ml of

0.1 N HCl

0.01 to 5% (as K2O)

Lead

IFLC/QSP G/ 009

AOAC 19th

Ed, 975.15

1 to 100 mg/kg

Copper

0.5 to 100 mg/kg

Petroleum ether extract IS 18(Part 9 )-1984

IS 3077-1992 (RA 1998)

0.1 to 30 %

Water soluble matter/ extract IS 3633-1972, Appendix B,

IS 13857-1993

0.1 to 80%

Total Catechins IS 15344-2003

0.05 to 50%

Solubility in Water IS 2791-1992

(RA 1998)

Qualitative

Iron Filing IS 3633 : 2003

100 to 5000 mg/kg

Test of Chicory DGHS MANUAL 2005,

No.4, 1.9.1

Qualitative

Insects fragments DGHS MANUAL 2005,

No.10, 2.0

Qualitative

Rodent hair & excreta DGHS MANUAL 2005,

No.3, 1.2

Qualitative

Laboratory









Added colouring matter DGHS MANUAL 2005,

No.8, 4.2

Qualitative

Arsenic

AOAC 19th Ed, 18th Ed., 986.15 0.1 to 100 mg/kg

Mercury

AOAC 19th Ed, 18th Ed., 977.15 0.1 to 100 mg/kg

Nickel

AOAC 19th Ed, 18th Ed. 971.20 2.5 to 250 mg/kg

Cadmium


Zinc


Microscopic examination DGHS MANUAL 2005,

No.4, 1.9

--

19. ALCOHOLIC

BEVERAGE (WINE)

Alcoholic Strength AOAC 19th Ed, 920.57

OIV-MA-AS312-01B

1 to 80 %

Volatile acidity OIV-MA-AS313-02

1 to 50 g acetic acid/L

SO2 Free OIV- MA AS323-04

5 to 200 mg/l

SO2 Total OIV-MA-AS323-04

5 to 500 mg/l

pH AOAC 19th Ed, 960.19

OIV-MA-AS313-15

1 to 14

Total acidity OIV-MA-AS313-01 1.0 to 50 mEq/l or

1 g/L (as tartaric acid)

Laboratory









Chlorides IFL C/QSP G/025

1 to 250 mg/L

Fluorides IFL C/QSP G/025

1 to 250 mg/L

Density


OIV-MA-AS2-01

0.1 to 10 g/ml

Specific gravity

0.9 to 1.2

Glucose + Fructose AOAC 19th Ed, 985.09

OIV-MA-AS311-02

10 to 250 g/L

Total sugars AOAC 19th Ed, 920.65

10 to 100 g/L

Total dry matter

OIV-MA-AS2-03A 10 to 100 g/L

Color Intensity

OIV-MA-AS2-07B 0.1 to 50 mg/L

Iron

AOAC 19th Ed, 970.19 0.1 to 100 mg/L

Copper

AOAC 19th Ed, 970.18 0.1 to 100 mg/L

Potassium

AOAC 19th Ed, 963.13 1 to 1000 mg/L

Sodium

AOAC19th Ed, 963.13 1 to 1000 mg/L

Ash

AOAC 19th Ed, 920.67 0.1 to 25 %

Alkalinity of ash

AOAC 19th Ed, 920.68 1 ml to 200

H2SO4/100ml

Lead

AOAC 19th Ed, 967.08 0.1 to 100 mg/L

Laboratory









Cadmium AOAC 19th Ed, 967.08

0.025 to 100 mg/L

Mercury AOAC 19th Ed, 970.12

0.005 to 100 mg/L

Arsenic

AOAC 19th Ed, 967.08 0.005 to 100 mg/L

20. EDIBLE OIL,

EDIBLE FAT

(Ground nut oil, Palm

oil, Sunflower oil,

Rape seed oil, Cotton

seed oil, Mustard oil,

Corn oil, coconut oil,

Rice bran oil,

Palmolein, Gingelly

oil, Soyabean oil)

Melting point IS : 548 (Part I) – 1964

0 to 100o C

Refractive Index IS : 548 (Part I) – 1964

1.3 to 1.7

Specific gravity IS : 548 (Part I) – 1964

0.6 to 2

Saponification value IS : 548 (Part I) – 1964

10 to 300

lodine value IS : 548 (Part I) – 1964

2 to 200

Peroxide value IS : 548 (Part I) – 1964

0.5 to 10 mEq/kg

Polenske value IS : 548 (Part I) – 1964

1.0 to 50.0

Acid value IS : 548 (Part I) – 1964

0.25 to 10 mgKOH/g

Free fatty acids IS : 548 (Part I) – 1964

0.05 to 20%

Unsaponifiable matter IS : 548 (Part I) – 1964

0.1 to 20%

Test for Argemone oil IS : 548 (Part II) – 1976

Qualitative

Bellier Test IS : 548 (Part II) – 1976

Qualitative

Laboratory









Hydrocyanic acid IS : 548 (Part II) – 1976

Qualitative

Phosphorus In-house method

IFL C/QSP G/016

10 to 500 mg/kg

Flash Point DGHS, 2005 Lab Manual – 2

25 to 350o C

Test for castor oil IS : 548 (Part II) – 1976

Qualitative

Added Colouring matter DGHS MANUAL 2005,

No.8, 4.2

Qualitative

Added flavouring matter DGHS MANUAL 2005,

No.4, 7.0

Qualitative

Test for Sesame oil DGHS MANUAL 2005,

No. 2,15.0 IS548(II),1976

Qualitative

Test for Cotton Seed Oil DGHS MANUAL 2005,

No.2, 16.0 IS548(II),1976

Qualitative

Total fatty acid AOAC 19th Ed, 969.33

0.1 to 50 %

Moisture

AOAC 19th Ed, 984.20 0.1 to 25 %

Butylated Hydroxy Anisole

(BHA)

AOAC 19th Ed, 983.15 10 to 250 mg/kg

TBHQ

AOAC 19th Ed, 983.15 20 to 250 mg/kg

Laboratory









Aflatoxin B1,B2,G1,G2

IFL C/ QSP G/ 002 0.5 to 1000 µg/kg

Nickel

IFL C/QSP G/009 0.75 to 100 mg/kg

Zinc


Lead


Copper IFL C/QSP G/009

0.25to 100 mg/kg

Mercury IFL C/QSP G/009

0.1 to 100 mg/kg

Arsenic IFL C/QSP G/009

0.1 to 100 mg/kg

Cadmium IFL C/QSP G/009

0.25 to 100 mg/kg

Chromium IFL C/QSP G/009

1.25 to 100 mg/kg

21. PALMOLEIN Cloud Point DGHS MANUAL 2005,

No. 2, 17.0

0 to 100

o C

BHA DGHS MANUAL 2005,

No.8, 5.0

2 to 20mg/kg

22. OLIVE OIL Tea seed oil test DGHS MANUAL 2005,

No. 2, 24.0

Qualitative

Laboratory









FRUITS AND VEGETABLES

23. FRESH FRUITS AND

VEGETABLE

Rotting Visual Examination

Qualitative


No. 3, 1.2

Qualitative

Added colouring matter DGHS MANU AL 2005,

No.8, 4.0

Qualitative

Added wax coating IFL C/ QSP G/031

Qualitative


Qualitative

PROCESSED FRUITS AND VEGETABLES

24. ALL FRUITS AND

VEGETABLES AND

THEIR PRODUCTS

Zinc AOAC 19th Ed, 975.03

0.25 to 100 mg/kg

Tin AOAC 19th Ed, 975.03

0.05 to 100 mg/kg

Nickel AOAC 19th Ed, 975.03

0.5 to 100 mg/kg

Chromium AOAC 19th Ed, 975.03

0.25 to 100 mg/kg

Cadmium AOAC 19th Ed

0.05 to 100 mg/kg

Copper 977.15/971.20/975.03

0.25 to 100 mg/kg

Lead IFL C/QSP G/009

0.15 to 100 mg/kg

Mercury IFL C/QSP G/009

0.1 to 100 mg/kg

Arsenic

IFL C/QSP G/009

0.1 to 100 mg/kg

Laboratory









25. FRUIT AND

VEGETABLE

SAUCES/ KETCHUP/

PUREE/

PULP/CULINARY

PASTE/

FRUIT DRINKS/

SQUASHES/ FRUIT

SYRUPS/FRUIT &

VEG. JUICES/FRUIT

NECTARS/FRUIT

BEVERAGES/

SHARBAT

Water content DGHS MANUAL 2005,

No. 5, 4.1

1 to 90 %

Colour DGHS MANUAL 2005,

No. 8, 4.2

Qualitative

Fumaric acid AOAC 19th Ed, 986.13

50 mg/kg

Total soluble solids DGHS MANUAL 2005,

No. 5, 1.6

0.1 to 80 %

Acidity

as citric acid/ malic acid/

Oxalic acid/ Tartaric acid/

Lactic acid/ Acetic acid/ Oleic

acid

AOAC 19th Ed, 942.15 0.1 to 50 %

Ascorbic acid

AOAC 19th Ed, 986.13 50 to 2000 mg/kg

Sugar, Dextrose, Invert sugar AOAC 19th Ed, 925.35


0.1 to 70 %

Salt DGHS MANUAL 2005,

No. 3, 16.2

0.1 to 25 %

Sulphur Dioxide AOAC 19th Ed, 990.28

5 to 500 mg/kg

Benzoic acid AOAC 19th Ed, 994.11

1 to 1000 mg/kg

Sorbic acid AOAC 19th Ed, 974.08/974.10

10 to 1000 mg/kg

Laboratory









Drained weight of fruit in

pack (liquid pack)

DGHS MANUAL 2005,

No. 5, 1.4

10 to 100 %

Drained weight of fruit in

pack (solid pack)

DGHS MANUAL 2005,

No. 5, 1.4

10 to 100 %

Container fill DGHS MANUAL 2005,

No. 5, 1.3

1 to 100%

Total soluble solid salt free

basis (m/m)

DGHS MANUAL 2005,

No. 5, 1.6,1.7

1 to 50%

Extraneous matter AOAC 19th Ed, 945.75

0.1 to 10%

Insects AOAC 19th Ed, 970.72/950.89

Qualitative

Alkalinity test AOAC 19th Ed, 920.68 1 to 50ml of

0.05 M H2SO4

26. PICKLES Drained weight DGHS MANUAL 2005,

No. 5, 1.4

1 to 80 %

NaCl content (package in

brine)

DGHS MANUAL 2005,

No. 5, 1.7

0.1 to 80%

Acidity as citric acid DGHS MANUAL 2005,

No. 5, 2.4

0.05 to 25 %

Acidity as acetic acid

(package in vinegar)

DGHS MANUAL 2005,

No. 14.5

0.1 to 25%

Laboratory









Synthetic colour DGHS MANUAL 2005,

No. 8, 4.2

Qualitative

Sulphur dioxide AOAC 19th Ed, 990.28

20 to 2000 mg/kg

Sodium and Potassium

benzoate as benzoic acid

DGHS MANUAL 2005,

No.8, 1.2

20 to 2000 mg/kg

27. NUTS-

GROUNDNUT,

CASHEW NUT,

PISTACHIO, BEAN /

RAISINS/DATES

Moisture AOAC 19th Ed, 925.40

0.1 25 %

Aflatoxins B1, B2, G1, G2 ASTA 4th Ed, 1997

0.5 to 1000 μg/kg


0.25 to 1000 μg/kg

Damaged Kernel DGHS MANUAL 2005,

No.10, 2.0

1 to 100%

Extraneous matter DGHS MANUAL 2005,

No.10, 2.0

1 to 25%

Blemished units DGHS MANUAL 2005,

No.10, 2.0

1 to 100%

Empty shells DGHS MANUAL 2005,

No.10, 2.0

1 to 50%

Sugared raisin DGHS MANUAL 2005,

No.10, 2.0

1 to 100%

Acidity of extracted fat as

oleic acid

IS 4884 :1975 0.1 to 25%

Laboratory









Living/Dead insects /

fragments


Present /Absent


Present /Absent


No.10, 2.0

Present /Absent

Acid insoluble ash DGHS MANUAL 2005,

No.5, 5.3

0.05 to 25 %

Hydrocyanic acid AOAC 19th Ed, 915.03

5 to 200 mg/kg

28. VINEGAR Acidity as acetic acid DGHS MANUAL 2005,

No.5, 14.5

0.1 to 20%

Total solids DGHS MANUAL 2005,

No.5, 14.3

0.1 to 25%

Total Ash content DGHS MANUAL 2005,

No.5, 14.4

0.1 to 25%

Foreign substance DGHS MANUAL 2005, No.5, 14

0.1 to 10%

29. CEREALS, PULSES -

WHOLE AND IN

POWDERED (Wheat,

Rice, Atta, Maida, All

Dals, Oats, Barley)

Moisture AOAC 19th Ed, 925.10

0.1 to 25%

Aflatoxins B1, B2, G1, G2 ASTA 4th Ed, 1997

0.5 to 1000 μg/kg


0.25 to 1000 μg/kg

Total Ash AOAC 19th Ed, 923.03

0.1 to 25 %

Laboratory









Acid insoluble Ash IS : 1155, 1968 (RA 2000)

0.1 to 25 %

Crude Fibre

IS : 1155, 1968 (RA 2000) 0.1 to 50 %

Gluten

IS : 1155, 1968 (RA 2000) 1 to 50 %

Alcoholic acidity IS : 1155, 1968 (RA 2000)

0.1 to 50 %

Calcium Carbonate DGHS MANUAL 2005,

No.3, 8.7

0.01 to 10 %

Added colour DGHS MANUAL 2005,

No.8, 4.2

Qualitative

Extraneous matter

IS 4333 (Part 1) - 1996 0.1 to 25 %

Damaged grains

IS 4333 (Part 1) - 1996 0.1 to 25 %

Weevilled grains

IS 4333 (Part 1) - 1996 0.1 to 25 %

Other edible grains

IS 4333 (Part 1) - 1996 0.1 to 25 %

Uric acid

AOAC 19th Ed, 969.46 2 to 1000 mg/kg

Iron AOAC 19th Ed,

977.15/971.20/975.03

IFL C/QSP G/009

1.0 to 50 mg/kg

Thiamine Inhouse validated method

IFL C/QSP G/015

0.01 to 100 mg/100g

Laboratory









Riboflavin Inhouse validated method

IFL C/QSP G/015

0.01 to 100 mg/100g

Niacin Inhouse validated method

IFL C/QSP G/015

0.01 to 100 mg/100g

Vitamin D Inhouse validated method

IFL C/QSP G/014

2.5 to 500 µg/100g

Argemone seeds DGHS MANUAL 2005, No.3, 1

0.1 to 25%

Khesari dal DGHS MANUAL 2005,

No.3, 11.0

Qualitative

Foreign matter DGHS MANUAL 2005,

No.3, 1.1.2.1

0.1 to 25%

1)Mineral matter DGHS MANUAL 2005,

No.3, 1.1.2.1

0.1 to 25%

2) Organic matter DGHS MANUAL 2005,

No.3, 1.1.2.1

0.05 to 25%

Insect DGHS MANUAL 2005,

No.3, 1.2

Qualitative

Microscopic Examination DGHS MANUAL 2005,

No.3, 1.3

-

Rodent hair & Excreta DGHS MANUAL 2005,

No.3, 1.2

Qualitative

Laboratory









Presence of mould DGHS MANUAL 2005,

No.3, 1.1

Qualitative

Test for mineral oil AOAC 19th Ed, 966.01

Qualitative

Total protein DGHS MANUAL 2005,

No. 3, 8.8

0.1 to 50%

Sulphur dioxide AOAC 19th Ed, 990.28

10 to 500 mg/kg

Ascorbic acid IFL C/QSP G/024

5 to 500 mg/kg

Benzoyl peroxide AOAC 19th Ed, 935.34

5 to 500 mg/kg

Potassium bromate AOAC 19th Ed, 956.03

5 to 500 mg/kg

Deoxynivalenol in wheat DGHS MANUAL 2005,

No.3, 7.0

0.3 to 10 mg/kg

30. BISCUITS, BREAD Acid insoluble Ash in Dil HCl

(on dry wt basis)

DGHS MANUAL 2005,

No.3, 14.4

0.1 to 25%

Acidity of extracted fat (as

Oleic acid)

DGHS MANUAL 2005,

No.3, 14.4

0.01 to 25%

Added colouring matter DGHS MANUAL 2005,

No.8, 4.3

Qualitative

Salt (as Sodium chloride) DGHS MANUAL 2005,

No.3, 16.2

0.1 to 25 %

Laboratory









Synthetic colour :

Ponceau 4 R

DGHS MANUAL 2005,

No.8, 4.2

Qualitative

Trans fat IFL C/QSP G/021

0.1 to 30%

31. NUTRITIONAL

FACTORS OF FOOD

PRODUCTS

Total Fat IS 5960 (Part III) 1970

IFL C/QSP SF/015

0.1 to 50g/100g

Saturated Fat IFL C/QSP SF/015 A

0.1 to 50g/100g

Unsaturated Fat

IFL C/QSP SF/015 B 0.1 to 50g/100g

Trans fat

IFL C/QSP G/021 0.1 to 25g/ 100 g

Monounsaturated Fatty acid

(MUFA)

AOAC 19th Ed, 19th

Ed 996.06 0.1 to 25g/ 100 g

Polyunsaturated Fatty acid

(PUFA)

AOAC 19th Ed, 19th

Ed 996.06 0.1 to 25g/ 100 g

Dietary Fibre

IS 11062 - 1984 0.2 to 50 g/100g

Protein AOAC 19th Ed, 920.87, 928.08,

981.10

0.1 to 75 g/100g

Cholesterol IFL C/ QSP G/ 019

5 to 500 mg/100 g

Vitamin C IFL C/QSP G/024

0.5 to 500 mg/100g

Vitamin A

IFL C/ QSP G/028

100 to 1000µg/100g

Laboratory









Vitamin D In-house validated method

IFL C/QSP G/014

2.5 to 1000µg/100g

Thiamine IFL C/QSP G/015

0.01 to 100 mg/100g

Riboflavin IFL C/QSP G/015

0.01 to 100 mg/100g

Niacin IFL C/QSP G/015

0.01 to 100 mg/100g

Sugar IFL C/QSP G/026

0.25 to 20g/100g

Total Carbohydrate AOAC 19th Ed, 986.25

(by difference)

--

Calcium AOAC 19th Ed, 923.03/ 938.08

IS 3025 (Part 40) 1991

1 to 5000 mg/100g

Sodium AOAC 19th Ed, 19th Ed.

IFL C/QSP G/009

7.5 to 1000 mg/100g

Iron AOAC 19th Ed, 19th Ed.

IFL C/QSP G/009

0.025 to 1000 mg/

100 g

Total Calories / Energy IFL C/ QSP G/027

(by calculation)

--

Folic acid In-house validated method

IFL C/QSP G/015

0.01mg/100g

Laboratory









32. SWEETS AND CON-

FECTIONARY

SUGAR BOILED

CON-FECTIONARY/

LOZENGES/

CHEWING GUM/

BUBBLE GUM/

CHOCOLATE/

JELLY / CANDY

DROPS

Ash sulphated (on salt free

basis)

DGHS MANUAL 2005,

No.4, 13.2

0.1 to 25 %

Ash sulphated DGHS MANUAL 2005,

No.4, 13.2

0.1 to 25 %

Ash insoluble (in dil. HCl) DGHS MANUAL 2005,

No.4, 13.3

0.1 to 25 %

Total Protein (dry basis) DGHS MANUAL 2005,

No.4, 13.4

0.1 to 50 %

Fat content DGHS MANUAL 2005,

No.4, 13.5

0.1 to 50 %

Sucrose content DGHS MANUAL 2005,

No.4, 13.6

0.1 to 25 %

Gum DGHS MANUAL 2005,

No.4, 14.6

0.1 to 50 %

Moisture DGHS MANUAL 2005,

No.4, 1.2

0.1 to 25 %

Reducing Sugar

(calculated as Dextrose)

DGHS MANUAL 2005,

No.4, 6.4

0.1 to 90 %

Sodium, Potassium Benzoate/

Benzoic Acid

DGHS MANUAL 2005,

No.8, 1.2

5 to 500 mg/kg

Laboratory









Sulphur Dioxide DGHS MANUAL 2005,

No.4, 7.5

20 to 500 mg/kg

Sorbic Acid & its Calcium,

Sodium & salts

DGHS MANUAL 2005,

No.4, 1.3

5 to 500 mg/kg

L- Tartaric Acid IFL C/ QSP G/028

0.05 to 25 %

Talc DGHS MANUAL 2005,

No.3, 28.0

0.01 to 10 %

Lead

AAS/AOAC 19th Ed, 975.03 0.25 to 100 mg/kg

Copper


Arsenic


Tin


Zinc


Cadmium


Mercury


Antimony


Iron


Milk fat (on dry basis) DGHS MANUAL 2005, No.4,

15.6

0.1 to 50 %

Laboratory









Cocoa solids

(on moisture free & fat free

basis)

DGHS MANUAL 2005,

No.4, 15.7

0.1 to 50%

Milk solids

(on moisture free & fat free

basis)

DGHS MANUAL 2005,

No.4, 15.4

0.1 to 70 %

II. PLASTICS & PLASTIC PRODUCTS

1. PACKAGING

MATERIALS

(Plastic containers,

sealable single/ multi-

layered flexible films,

sealing gaskets, liners

and like materials)

Migration of constituents

IS 9845 : 1998 5 to 1000 mg/l

Colour Migration IS 9845 : 1999 Qualitative

III. DRUGS & PHARMACEUTICALS

1. AMOXYCILLIN

CAPSULES

250 mg, 500 mg

Identification

IP 2010, Page No. 813 Qualitative

Dissolution

IP 2010, Page No. 813 40 to 120%

Assay

IP 2010, Page No. 814 90 to 110%

2. AMOXYCILLIN

DISPERSIBLE

TABLETS

Identification


Assay

IP 2010, Page No. 817 90 to 120%

Laboratory









3. AMOXYCILLIN

ORAL SUSPENSION

Identification


pH

IP 2010, Page No. 815 5 to 7.5

Assay

IP 2010, Page No. 815 90 to 120%

4. AMPICILLIN

CAPSULES

Identification


Dissolution

IP 2010, Page No. 823 30 to 120%

Assay

IP 2010, Page No. 824 92.5 to 107.5%

5. ASPIRIN TABLETS Dissolution IP 2010 Addendum 2012,

Page No. 2882

30 to 120%

Assay IP 2010, Page No. 843

95 to 105%

Identification IP 2010, Page No. 843

Qualitative

Salicylic acid


6. ALBENDAZOLE TABLETS

Identification IP 2010, Page No. 781 Qualitative

Assay

IP 2010, Page No. 781 92.5 to 107.5%

7. IBUPROFEN

TABLETS

Dissolution IP 2010, Page No. 1482 30 to 110%

Identification,


Assay

IP 2010, Page No. 1483 95 to 105%

Laboratory









8. NORFLOXACIN

TABLETS

Identification A,B IP 2010, Page No. 1794 Qualitative

Assay

IP 2010, Page No. 1795 90 to 110%

Dissolution

IP 2010, Page No. 1795 30 to 120%

9. OFLOXACIN

TABLETS


Dissolution

IP 2010, Page No. 1810 30 to 120%

Assay

IP 2010, Page No. 1810 90 to 110%

Related substance


10. PARACETAMOL

SYRUP

Identification A,B IP 2010 Addendum 2012,

Page No. 2940

Qualitative

Related substances IP 2010Addendum 2012,

Page No. 2940

Qualitative

Assay

IP 2010Addendum 2012,

Page No. 2941

90 to 110%

11. PARACETAMOL

TABLETS


Related substances IP 2010, Page No. 1861

Qualitative

Dissolution

IP 2010, Page No. 1861 30 to 120%

Assay

IP 2010, Page No. 1861 95 to 105%

Laboratory









12. POVIDONE IODINE

OINTMENT

Identification A,B,C

USP NF 2009, Page No. 1421 Qualitative

pH

USP NF 2009, Page No. 1421 1.5 to 6.5

Ethanol

USP NF 2009, Page No. 1421 Qualitative

Assay

USP NF 2009, Page No. 1421 85 to 120

13. POVIDONE IODINE

SOLUTION

Identification IP 2010, Page No. 1943

Qualitative

pH IP 2010, Page No. 1943

3 to 6.5

Ethanol IP 2010, Page No. 1943

Qualitative

Assay IP 2010, Page No. 1943

85 to 120%

14. SALBUTAMOL

SULPHATE

TABLETS

Identification A,B,C


Related substances


Assay

IP 2010, Page No. 2089 90 to 110%

Uniformity of content

IP 2010, Page No. 2089 85 to 115%

15. SALBUTAMOL

SYRUP

Identification A,B IP 2010, Page No. 2088 Qualitative

pH

IP 2010, Page No. 2088 3.4 to 4.5

Assay

BP 2007, Vol. 3 90 to 110%

Laboratory









16. CAPSULES Content of active ingredients

IP 2010, Page No. 721 80 to 120%

Uniformity of weight

IP 2010, Page No. 722 5 to 10%

Disintegration

IP 2010, Page No. 722 1 to 50 min

Dissolution

IP 2010, Page No. 1861 10 to 120 %

17. TABLETS

(Coated Tablets,

Uncoated tablets,

Dispersible tablets,

Film coated Tablets)

Content of active ingredients

IP 2010, Page No. 751 80 to 120%

Uniformity of weight

IP 2010, Page No. 752 5 to 10%

Uniformity of content

IP 2010, Page No. 751 70 to 130%

Disintegration

IP 2010, Page No. 752 10 sec to 60 min

Dissolution

IP 2010, Page No. 752 10 to 120%

18. DISPERSIBLE

TABLETS

Uniformity of dispersion IP 2010, Page No. 753 Qualitative

19. LACTOSE IP Identification A,B,C


Appearance of solution


Acidity or Alkalinity


Sp. Optical rotation

IP 2010, Page No. 1554 54.4° to 55.9°

Laboratory









Light Absorption


Arsenic


Heavy metals


Sulphated Ash

IP 2010, Page No. 1554 0.05 to 5%

Water

IP 2010, Page No. 1554 4.5 to 5%

20. STARCH Identification


Acidity


Iron IP 2010, Page No. 2544

Qualitative

Fluorescence IP 2010, Page No. 2544

Qualitative

Oxidising substance IP 2010, Page No. 2544

Qualitative

Sulphated ash IP 2010, Page No. 2544

0.05 to 5%

Loss on drying

IP 2010, Page No. 2544 1 to 35%

Laboratory









IV. WATER

1. Drinking Water as per

IS 10500-2012;

Packaged Drinking

Water other than

natural mineral water

IS 14543-2004;

Packaged natural

mineral water IS 13428

-1998; Drinking Water

as per W.H.O.; Water

for Processed Food

Industry - IS 4251;

Feed/Boiler water IS

10496-1983; Water as

per 98/83/EC; Effluent

water; Water for

mixing Concrete IS

456:2000

Colour, True Colour Units IS 3025 (Part - 4) 1983

2120 B , APHA 22nd Ed.

1 to 50

Odour IS 3025 (5) 1983

2150, APHA 22nd Ed.

Qualitative

Turbidity, NTU IS 3025 (Part - 10) 1984,

2130B, APHA 22nd Ed.

1 to 500 NTU

Total Dissolved Solids IS 3025(Part - 16) 1984,

2540C, APHA 22nd Ed.

10 to 1000 mg/l

Conductivity 2510 B, APHA 22nd Ed.

2μS/cm to 200 mS/cm

pH IS 3025( Part -11) 1983

1 to 14

Barium as Ba Annexure F IS 13428/1998,

IS 15302-2003,

3500, APHA 22nd Ed.

0.03 to 50 mg/l

Copper as Cu IS 3025(Part 42) 1992,

3500, APHA 22nd Ed.

0.025 to 100 mg/l

Iron as Fe IS 3025(Part 53)2003,

IS 15303-2003

3500Fe-B , APHA 22nd Ed.

0.075 to 100 mg/l

Manganese as Mn Clause 35 of IS 3025 2003

0.025 to 100 mg/l

Laboratory









Nitrate IS 3025(Part -34) 1998

4500 NO.3-B, APHA 22nd Ed.

1 to 100 mg/l

Nitrite IS 3025(Part -34) 1998

4500 NO2- B, APHA 22nd Ed.

0.01 to 1 mg/l

Fluoride 23 of IS 3025/1964,

4500F-D, APHA 22nd Ed.

0.3 to 3 mg/l

Zinc IS 3025(49) 1994;

3500, APHA 22nd Ed.

0.05 to 10 mg/l

Silver Annex-J of IS 13428/1998;

3500, APHA 22nd Ed.

7.5 to 100 µg/L

2.0 to 100 µg/L

Aluminium IS 3025(Part-55) /IS 15302:2003

3500, APHA 22nd Ed

0.02 to 300 mg/l

Chloride IS 3025 (32) 1988;

4500 Clˉ - B, APHA 22nd Ed

5 to 500 mg/l

Selenium IS 3025 (56)/ IS :15303 -2003;

3500 APHA 22nd Ed

0.0025 to 1 mg/l

Sulphate IS 3025 (24) 1986

4500 SO42-

E APHA 22nd Ed

5 to 500 mg/l

Alkalinity IS 3025(Part-23) 1986 5 to 500 mg/l

0.1 ml H2SO4/100ml

Laboratory









Cyanide IS 3025(27) 1986:

4500 CNˉ- F APHA 22nd Ed

0.01 to 1 mg/l

Lead IS 3025(Part -47) 1994;

3500 APHA 22nd Ed

7.5 to 100 µg/L

3.0 to 100 µg/L

Chromium Annex - J of IS 13428 /1998

3500 APHA 22nd Ed

5.0 to 100 µg/L

Nickel Annex-L of IS 13428/1998

3500 APHA 22nd Ed

15.0 to 100 µg/L

7.5 to 100 µg/L

Calcium Hardness IS 3025(Part -21) 1998

2340C APHA 22nd Ed

5 to 500 mg/l

Magnesium Hardness IS 3025(Part -21) 1998

2340C APHA 22nd Ed

2 to 500 mg/l

Sulphide IS 3025(Part -29) 1986

4500S-2 APHA 22nd Ed

0.02 to 500 mg/l

Borate (Boron) Annex-H of IS 13428/1989

4500-B APHA 22nd Ed

0.2 to 100 mg/l

Antimony Annex-G of IS 13428/1998,

IS 15303: 2003 AAS - HVG

(GBC Instrument Manual)

0.0025 to 10 mg/l

Laboratory









Polychlorinated Biphenyls

(PCB)

a) 2,6 - Dichlorobiphenyl

Annex-M of IS 13428 0.05 to 1000 µg/l

b) 2,4,4’ – Trichlorobiphenyl

EPA 525.2/APHA 22nd Ed 0.05 to 1000 µg/l

c) 2,2’,5,5’ –

Tetrachlorobiphenyl

0.05 to 1000 µg/l

d) 2,2’3,4,4’,5’ –

Hexachlorobiphenyl

EPA 525.2/APHA 22nd Ed 0.05 to 1000 µg/l

e) 2,2’,4,4’,5,5’ –

Hexachlorobiphenyl

0.05 to 1000 µg/l

f) 2,2’,3,4,4’,5,5’-

Heptachlorobiphenyl

0.05 to 1000 µg/l

Benzo (a) pyrene

USEPA / APHA 22nd Ed. 0.01 to 100 µg/l

Polynuclear Aromatic

Hydrocarbons

a) Benzo[b] fluoranthene

APHA 6440, EPA 525.2 0.01 to 100 µg/l

b) Benzo[k] fluoranthene

0.01 to 100 µg/l

c) Indenol [1,2,3-c d] pyrene

APHA 6440, EPA 525.2 0.01 to 100 µg/l

d) Benzo[ghi]perylene

0.01 to 100 µg/l

Laboratory









Total hardness as CaCO3 IS 3025(Part -21) 1998

2340C APHA 22nd Ed

5 to 500 mg/l

Dissolved Oxygen APHA 22nd Ed 4500 – O-C

1 to 500 mg/l

Phosphorus APHA 22nd Ed 4500 Р-C

1 to 1000 mg/l

Suspended Solids APHA 22nd Ed 2540 D

IS 3025(17)1984 RA 1996

10 to 1000 mg/l

BOD APHA 22nd Ed 5210 – B

1 to 1000 mg/l

COD APHA 22nd Ed 5220 – B

2 to 1000 mg/l

Oil & Grease IS 2488 Part I

2 to 1000 mg/l

Calcium as Ca IS 3025(46) 1994;

3500 APHA 22nd Ed

2 to 1000 mg/l

Magnesium as Mg IS 3025(Part -46) 1994;

3500 APHA 22nd Ed

0.5 to 500 mg/l

Sodium IS 3025(Part -45) 1993

3500Na-B APHA 22nd Ed

10 to 500 mg/l

Total solids APHA 22nd Ed 2540 10 to 1000 mg/l

Total Organic Carbon APHA 22nd Ed 5310 5 to 1000 mg/l

Residual free chlorine IS 3025 (Part-26) 1986 0.01 to 100 mg/l

Phenolic compounds as

C6H5OH

IS 3025 (Part 43) 1992 0.001 to 1 mg/l

Mineral Oil IS 3025 (Part-39) 1989 0.01 to 10 mg/l

Laboratory









Anionic surface active agents

as MBAS

Annex-K of IS 13428/1998 0.1 to 50 mg/l

Mercury IS 3025 (Part-48) 1992;

3500 APHA 22nd Ed

0.75 to 1000 µg/l

Cadmium IS 3025 (Part-41) 1992;

3500 APHA 22nd Ed

1.5 to 100 µg/l

0.05 to 100 mg/l

Arsenic IS 3025 (Part-37-1988);

3500 APHA 22nd Ed

0.0025 to 10 mg/l

Boron IS 13428 H

0.2 to 100 mg/l

Ammonium/ammonia 4500 NH3-F APHA 22nd Ed

0.1 to 100 mg/l

Potassium 3500 K-B- APHA 22nd Ed

0.1 to 1000 mg/l

Silica IS 3550 1965 RA 1998,

ASTM D 859-94

0.01 to 100 mg/l

Molybdenum 3500, APHA 22nd Ed.

0.01 to 100 mg/L

Chloramines 4500-Cl G, APHA 22nd Ed.

0.1 to 100 mg/L

Acidity IS 3025 (22) 1986

RA 2003

5 to 100 mg/L

0.1 ml NaOH/100ml

Volatile / Organic residue IS 3025 (18) 1984 RA 2002

APHA 22nd Ed 5560.C

10 to 100 mg/L

Laboratory









Fixed / Inorganic residue IS 3025 (18) 1984, RA 2002

10 to 100 mg/L

Acrylamide IFL C/QSPW/032

0.1 to 1000 µg/l

Bromate IFL C/QSP W/031

5 to 1000 µg/l

Benzene

USEPA 524.2/ APHA 6200 0.5 to 1000 µg/l

1,2 Dichloro ethane

0.5 to 1000 µg/l

Epichlorohydrin

0.1 to 1000 µg/l

Tetrachloroethene &

Trichloroethene

0.5 to 1000 µg/l

Trihalomethanes

Chloroform USEPA 524.2/ APHA 6200 0.5 to 1000 µg/l

Bromodichloromethane 0.5 to 1000 µg/l

Dibromochloromethane 0.5 to 1000 µg/l

Bromoform 0.5 to 1000 µg/l

Vinyl chloride

0.5 to 1000 µg/l

Pesticide Residues

α-HCH USEPA 525.2/ APHA 22nd Ed 0.01 to 1000 µg/L

β-HCH 0.01 to 1000 µg/L

γ-HCH(Lindane) 0.01 to 1000 µg/L

δ-HCH 0.01 to 1000 µg/L

o,p'- DDT 0.5 to 1000 µg/l

p,p' - DDT 0.5 to 1000 µg/l

o,p'- DDE 0.5 to 1000 µg/l

p,p'- DDE 0.5 to 1000 µg/l

o,p'- DDD 0.5 to 1000 µg/l

p,p' - DDD 0.5 to 1000 µg/l

Endosulfan-α 0.5 to 1000 µg/l

Endosulfan-β 0.5 to 1000 µg/l

Laboratory









Endosulfan sulphate USEPA 525.2/ APHA 22nd Ed 0.5 to 1000 µg/l

Endrin 0.5 to 1000 µg/l

Endrin Aldehyde 0.5 to 1000 µg/l

Endrin ketone 0.5 to 1000 µg/l

Heptachlor 0.5 to 1000 µg/l

Heptachlor epoxide 0.5 to 1000 µg/l

Cis-Chlordane 0.5 to 1000 µg/l

Trans -Chlordane 0.5 to 1000 µg/l

Methoxychlor 0.5 to 1000 µg/l

Malaoxon 0.5 to 1000 µg/l

Monocrotophos 0.5 to 1000 µg/l

Ethion 0.5 to 1000 µg/l

Chlorpyrifos 0.5 to 1000 µg/l

Phorate 0.5 to 1000 µg/l

Phorate sulfoxide 0.5 to 1000 µg/l

Phorate sulfone 0.5 to 1000 µg/l

Atrazine 0.5 to 1000 µg/l

Aldrin 0.01 to 1000 µg/L

Dieldrin 0.01 to 1000 µg/L

Methyl Parathion 0.5 to 1000 µg/l

Methyl Paraoxon 0.5 to 1000 µg/l

Malathion 0.5 to 1000 µg/l

Butachlor 0.5 to 1000 µg/l

Alachlor 0.5 to 1000 µg/l

Isoproturon 0.5 to 1000 µg/l

2,4-D 0.1 to 1000 µg/L

-X-X-X-X-X-X-X-X-X-X-X-X-X-X-

*NOTE: The Laboratory has demonstrated competence for the stated scope for WATER. This however does not fully

cover the specification requirements of BIS for the Packaged Drinking Water as per IS 14543 and the Packaged

Natural Drinking Water IS 13428.

Laboratory Interfield Laboratories, 13/1208-A, Interprint ... · Sulfamerazin 1.5 to 500 μg/kg...

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Transcript of Laboratory Interfield Laboratories, 13/1208-A, Interprint ... · Sulfamerazin 1.5 to 500 μg/kg...