fek 551 fly ash

. 55118 2007

. /. 281/200

.

O Y,

:1. 21

. 1418/1984, .

2. . 4881/19.5.2004 ( 754/2004) , , , .

3. 90 .. 63/2005 ( 98) , :

1. . 32201/11.12.2006 .

2. , :

1. .

2. .

3. , .

4. .

5.

6. , :

1. , , .

2. 6 .

3. , .

, 2 2007

.

10711

10712 ( )

ellenic National Specification

Greek fly ashes

, 2007

-

0. 0.1 0.2 1. 1.1 1.2 2. 2.1 2.2 3. 3.1 3.2 3.2.1 3.2.2 3.2.3 3.3 3.4 3.5 3.6 3.7 3.8 3.9 3.10 3.11 (CR =

customers risk): )3.12 3.13 3.14 k4. /Types

of Greek calcareous fly ashes5. / Specifications5.1 5.2 5.2.1 5.2.2 5.2.3 (Cl)5.2.4 ( SO3)5.2.5 (CaOf)5.2.6 (SiO2),

(AI2O3) (Fe2O3)5.2.7 5.3 5.3.1 5.3.2 5.3.3 Le Chatelier5.3.4 5.3.5 5.3.6 5.3.7 (chemical admixtures)6. 7. 7.1 7.2

7.2.1 7.2.2 7.2.3 7.3

1:

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 1:

1. 2. 2.1 2.2 3. 4. 5. 6. 7. 7.1 7.2

7.3 7.4 7.5 7.5.1 7.5.2 8. 9. 2:

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 3: 3:

1. 2. 3. 4. 5. 6. 7.

( ) 10713

8. 9. 3:

1. 2. 3. 4. 5. 6. 7. 7.1 7.2

7.3 7.4 7.5 8. 4:

(CaO) 1. 2. 3. 4. 5. 6. 7. 8. 9. 4:

Ca(O2)

1. 2. 3. 4. 5. 6. 7. 7.1 7.2 7.3 8. 9. 5:

1. 2. 3. 4. 5. 6. 7. 7.1 7.2 7.3 7.4

7.5 8.

5: Al, Ca, Fe, Mg, K, Na Si

1. 2. 3. 4. 5. 6. 7. 7.1 7.1.1 7.1.2 7.1.3 7.1.4 7.2 7.2.1 7.2.2 7.2.3 7.2.4 7.3 7.3.1 7.3.2 7.3.37.4 7.4.1 7.4.2

7.4.3 7.4.4 7.5 7.5.1 7.5.2

7.5.3 7.5.4 7.6 7.6.1 7.6.2

7.6.3 7.6.4 7.7 7.7.1 7.7.2

7.7.3 8. 9. 6:

1. 2. 3. 4. 5. 6. 7. 8. 9.

10714 ( )

7: 1. 2. 3. 4. 5. 6. 7. 8. 9. 8:

1. 2. 3. 4. 5. 6. 7. 8. 9.

, .

, .

:

.

(RCC), 80% 20% CEM I 42.5.

.

round robin test / (/ ....).

, Portland blended type . 1971, 2002.

/ .

( )

(sustainable development).

0. 01. (mineral

additions)1 ( ) .

2061 (2000) ConcretePart 1 Specification, Performance Production and Conformity. , , , , o , 2061, . 5.2.5. .

, 2061, (European Technical Approval) ( ).

( low calcium fly ash) ( high calcium fly ash calcareous fly ash) / .

.

2061 4501.

, 2061.

( ( 4501) (processing) , , , .

02. ()

. , . IT . IT 11x106 . :1 ( 2061 3.1.23) , . : ( )

( )

( ) 10715

,

.

, , /.

. 45 m 45 60%.

, , 40%, .

1. 1.1

II ( 2061, 2000 3.1.23 5.2.5) ( ), (E 9981), Portland 2061 .

kvalue equivalent performance 2061, 5.2.5.

, , IT .

.

I 2061, 5.1.6 Portland .

1.2

, , o .

, :

.. , , .

.

New Jersey, .

, , , , , .

.

.

.

, .

2.

, (UNE 83420), , ASTM .

4512 .

10716 ( )

( ) 10717

3. / Definitions

. .

3.1 II , (latent)

, (. 2061)

3.2

, , .

, / , . .

3.2.1

/ . CaO, SiO2 Al2O3, Fe2O3 . SiO2, 1971, 25% ..

10718 ( )

3.2.2 ,

, .

3.2.3 , (

) , , .

3.3 CEM ,

42,5 , 1971. 5.3.2 5.3.3 .

, :

(Blaine): 300 m2/kg. (C3A): 6% 12% (Na2O .): 0,5% 1,2%3.4 ,

.

3.5 (%)

75% 25% , , ( 1961).

3.6

, / .

3.7

.

3.8 ,

Pk .

3.9 ,

, , .

3.10 ,

, , , .

3.11 (CR = customers risk: )

, (APA = admissible probability acceptance) , .

3.12 / /

/ , Pk, CR.

3.13 ,

, . ( 1967).

3.14 k k (kvalue),

() ( ) (equivalent performance), ( k=1). , , .

4. /Types of Greek calcareous fly ashes

:) IT CaO (1015%), (.. IT

)

) CaO (>20%), (.. IT ).

, , :

1 () 2 ()

1

R45 SO3 CaOf

1 45% 7%

2 30% 5% 3%

: SO3 5,0 7,0% , IT , CAN/CSAA23.5M86 , , IT .

1, IT ( ) , .

, .. IT .

: , .

2 ( ) IT CEM I . , / . (max or min). H IT .

2061 ( kvalue equivalent performance).

5. / Specifications5.1.

. , 8 4501.

. .

IT , .

5.2. 5.2.1

IT. .

. 18 IT.

5.2.2.

1962, 1 h. ( 1).

. 5% ( 4501).

, , ASTM D6316(2000) ( 1.)

5.2.3 (Cl) Cl

1962 ( 2) 0,10% .

5.2.4 ( SO3) SO3

3, 5,0% .

: SO3 5,0 7,0% , IT , CAN/CSAA23.5M86 , ,, IT .

5.2.5. (CaOf)

2 4 ( 4511) 3% . , CaOf :

CaOf = CaOf ( 4511) CaO ( Ca(OH)2)

To CaO Ca(OH)2 4 [ Ca(OH)2 ].

5.2.6 (SiO2), (Al2O3) (Fe2O3)

5 5. 5 5 Ca, Fe, Mg, K, Na Si .

. 5.2 5.3, 1962 ( 6) 20%. Si2 1971 ( 7) 25% .. 1962 ( 6) 20%.

5.2.7.

5 5 a2. 5% .

5.3. 5.3.1 %

45 m 196.6. 4512 . (IT1, 2) 45 m, 1, 45% 30% , 10% .

5.3.2

1961. 28 . 90 . 75% 85% .

551 ( ) 10719

10720 ( )

2 , , 1961, CEM I, . .

5.3.3 Le Chatelier 30% + 70%

, 1963. 10mm.

: 50% +50% . ( 1963) (ASTM C15105).

5.3.4 1966

150 kg/m3 .

5.3.5.

( ) 10721

a 10 12 1 .

b 196 451, .

c 1967.d .e .f ,

.h (. :

SO3)1

7.2 7.2.1

:)

, 5.2 5.3

) k 10%

) CR (customers risk = ) 5%

, 7.2.2 7.2.3 2.

12 .7.2.2 ,

. (1) (2):

_x kA.s L (1)

_x + kA.s U (2)

:x:

S:

k. (acceptability)L: , 4U: , 4

k k , CR n . kA 3.

10722 ( )

3 kA (Pk = 10%) CR=5%

kA

a

20 21 1,91

21 23 1,89

24 25 1,85

26 27 1,82

28 29 1,80

30 34 1,78

35 39 1,73

40 44 1,70

45 49 1,67

50 59 1,65

60 69 1,61

70 79 1,58

80 89 1,56

90 99 1,54

100 149 1,53

150 199 1,48

200 299 1,45

300 399 1,42

400 1,40

a kA n

7.2.3 cD

cA n k 3.

(3):

cD cA (3) cA k

, cR . cA 4.

4 cA (Pk = 10%) CR=5%

na cA

20 39 0

40 54 1

55 69 2

70 84 3

85 99 4

100 109 5

110 0,075 (n 30)

a n

( ) 10723

1:

1.

, 975 25 C ( ).

2.

975 25 C .

3. 196 2 7 (

) EN 4501, 5.2.2 (

)4.

.

5.

0,1 mg. ,

1000 C.

, (Mg(ClO4)2), .

, 20 25 mL, .

6. 975

25 C, (*) ( g). ,

. 1g + 0,05 g (B g)

( ).

, 975 25 C.

20 , 40 .

, ( ).

( ( g).

( 15 min 975 25 C), , (*).

8. , %

. . , :

[% ] = 100 [( )/] x 100:: , g,: ,

g : +

, g. : 0.04% : 0.08%9. &

, ( ) :

S2 + 2O2 SO42 ,

7 , (% S2), :

4 x 15,999 / 32,06 x (%S2) = 1,996 x (%S2)

7 1,996 x (% S2):

= [% ] + 1,996 x (% S2)

:

(SO4

2), .

% . . SO3 (% SO3)

; ( 975 25 ) (SO4

2), .

% . . SO3 (% SO3)

(SO42),

, :

() = (% SO3) ] (% SO3) ] % . . SO3

(% S2), :

(% S2) = () x 32,06/80,0622 = 0,4 x ().: =[% ] + 1,996 x 0,4 x () = [%

] + 0,8 x ()

.10. (*) :

10724 ( )

, , , 0,0005 g.

, , .

11. EN 4501/2001, (

), 5.2.2, 196 2 & 7 ( ), 1 .

1 h , 196 2 (12).

1:

1.

, , (CO2) (IR).

2. 2.1

( ), .

, , .

( ).

, .

. , , . .

. .

.

2.2

.

, , 2.1

3. ASTM D 631600 (ASTM D 501600)4.

.

5.

, .

, , , .

, .

(CRMs), .

: .

( IR, ).

6.

:

, .

99,5 % min. , 10%.7. 7.1

.7.2

.

, , . ( ), . .

, .

( ) 10725

7.3

(CRMs) .

, , , , .

7.4 .

, . , , .

.

7.5 7.5.1

.

.

( ), .

, .

, , .

7.5.2 100 500 mg

, 0,1 mg.

10%, , , .

.

, , (< 150C) , .

, , 7.5.1

8.

, :

% C ( ) = ( ) ( )

9.

, , , EDTA ( C: 1,07 %), CaCO3 ( C: 12,00 %), (NIST 1632b) ( C: 6,86 % 0,26 %).

.

(CaO) , , .

.

, , .

2:

1.

.

2.

, , , , 25C, ,

3. 1962 44.

5.

0,1 mg 10 mL 0,1 mL

(Mg(ClO4)2)

( , 0,45 m)

5 mL 250 mL 500 mL

10726 ( )

6.

:

(HNO3) 1+2 1 + 100 (AgNO3)

150C 0,05 mol/ L 8,494 g

1000 mL .

(NH4SCN) 0,05 mol /L 3,8 g

1000 mL .

(III) (NH4Fe(SO4)2.12H2O 100 mL

, 10 mL 1+2.

7. 5g 0,05 g

250 mL

50 mL 1+2 (

) 1

, 5 mL 0,05 mol / L 1

1 + 100 500 mL , 1 + 100. 200 mL

5mL .

, .

V1

, V2

8.

% . :

Cl = 1,773/1000 x (V2 V1) x 100/ m1 = 0,1773 x (V2 V1)/ m1:m1: V1:

V2: .

: 0,005%. :

0,010%.9. &

.

10.

0,01%.

3: .

. ,

, SO3.

, , .

3:

1.

, .

2.

. , pH 1 1,5, . .

3. 1962, 8. (

)4.

, , .

5.

0,1 mg. ,

1000 C.

(Mg(ClO4)2) ( ).

, 20 25 mL, .

6.

.

*02005511804070032*

(HCl), 1,19 g/cm3.

(HCl) (1+11). 10 mL

110 mL . (1+16). 10 mL

( 0,90 g/cm3) 160 mL

. 12 g

(BaCl2.2H2O) 100 mL.

(AgNO3). 0,5 g

(AgNO3) , 10 mL 100 mL.

7. 1 g 0,05 g (B g)

.

250 mL 90 ml .

, 10 mL

, 15 .

, ( 0,45 m).

, (*).

, 250 ml ( ).

pH , 1 1,5, (1+11) (1+16).

5 .

.

10 mL . (BaSO4).

15 ( ).

12 24 , 60C .

, .

, (*).

( g) , (**).

.

, .

975 25 C, (**).

, ( ).

(BaSO4). ( g).

: 15 min .

8. (BaSO4),

: (BaSO4) =

:: , g, :

, g.

(SO3) ( ), % . . SO3 , :

% SO3 = [() x 0,343 / ] x 100T : 0,07%.T : 0,08%.9. (*)

: , . (AgNO3).

, (AgCl), .

, (AgNO3), .

(**) : , , 0,0005 g.

3:

1.

, , (S2) (IR).

2.

( ), .

551 ( ) 10727

10728 ( )

, , 1350 C .

( ).

, .

. , , .

.

. .

. , .

3. ASTMD 5016984.

.

5.

, .

, , 1350C . .

(CRMs), .

6.

:

, .

99,5 % min.7. 7.1

.7.2

(CRMs) , .

( ), (CRMs) . .

(CRMs) .

7.3

(CRMs) .

, , .

7.4

, . (CRMs), , .

.

7.5 1350C

, .

5% SO3 300 mg , 0,1 mg.

5% SO3 140 mg , 0,1 mg.

.

( ), .

, .

, , SO3.

8.

S SO3.

4: (CaO)

1.

(CaO) .

( ) 10729

2.

2, , .

, (CaO), (HCl) .

3. 45114.

.

5.

0,1 mg . , 0,063 mm

( ISO 565). ,

silica gel ( ).

. , 250 mL.

(NaOH) , (CO2) .

(.. ), ( 0,007 mm)

0,05 mL.6.

.

, 3 (Butanoic acid, 3 oxoethyl ester (= ethyl acetoacetate)

2 (Butane2ol) 2 (Propane2ol) (bromophenol blue). (

0,1 g 100 mL ).

(HCl), 0,100 .

7.

, 100 g ( 0,063 mm). , , .

1,0 1,5 g (m g) 250 mL.

, 12 mL , 3 80 mL 2.

(NaOH).

1 . ,

.

2, 50 mL.

: .

(HCl) (C: 0,100 mol/L), ( ).

(HCl) (V mL).

CaO.

, .

.

8.

, % . . , :

%CaO] = [(28,04xCxV)/(mx1000)]x100

C: (HCl), mol/1

V: (HCl), , ml

m: , g.

.

: 0,02%. : 0,04%.9.

, (CaO) (Ca(OH)2).

4: Ca(OH)2 .

1.

. ,

Ca(OH)2 > CaO + 22.

( 2, , ) , ( 380450C)

10730 ( )

3. ASTM E 186897ASTM 195398ASTM E 113198ASTM E 47300, 1142974.

.

Ca(OH)2 CaO 4

5. ,

:

: mg m

:

25C 1000C 5C/min,

: ( 2 Ar) 50 100 mL/min 5mL/min

0.1 C 251000C

: 0,1 min

: .

N26.

:

Ca(OH)2. 99,5 %.7. 7.1

: : 20C / min :

: 600C

: 2 : 50 mL/min : .

7.2

Ca(OH)2 .

7.3

Ca(OH)2, , Ca(OH)2, % (380450C).

CaO% = 3.11 [1 + 2]:1: %

2: % Ca(OH)2

8.

1 (1) (2) (differential thermogravimetry DTG ) .

Ca(OH)2 :

1.

2. 0 (1) (2)

= 1 2

:. DTG

.

.

.

.

(1) . Ca(OH)2 CaO :

CaO = 3.11 1 M1 g

.

( ) 10731

9. TG,

, , , . , , 2 Ar, (10C / min).

. , , . % %min. . ASTM 1582 1C/min .

1.

5:

1.

/ .

2.

(Li2B4O7). To

(HCl).

/ .

3. ASTM E 886 94, 1 10.ASTM D 3682 96, 8.3.4.

.

5.

0,1 mg.

1000C 1200C.

, 35 85 mL. ,

200C. .6.

() .

(Li2B4O7), ( ).

(HCl), 1,19 g/cm3.

(HCl), (5+95). 50mL

1000 mL .7. 7.1 (

), 200 (74m).

7.2. 0,1 g 0,0001 g ,

, .

0,5 g (Li2B4O7).

(Li2B4O7). 0,5 g Li2B4O7,

.

, 1000C.

15 min 1000C .

( ).

7.3.

, .

, 250 400 mL.

10732 ( )

( ), , .

150 mL (5+95) .

30 min .

.

: , . .

.

200 mL.

(5+95). ( 200 mL), (5+95).

7.4

1 g (Li2B4O7) .

, 1000 C.

, 7.2 7.3.

7.5

( ) (, ) .

. : (Si), (Al), (Fe), (Ca),

(Mg), (K), (Na), (Ti) (Mn).

II. : (Ba), (Cr), (Cu), (Ni)

(Co), (Zn), (Mo) (V).

: (.. , , ., ).

8.

(200 mL).

, (5+95).

5: AI, Ca, Fe, Mg, , Na Si

1.

(), (Ca), (Fe), (Mg), (). (Na) (Si) , (AAS) (AAS ):

2.

(AAS) , . , , , . , . , .

, 5

3. ASTM 88588 (reapproved 1996)ASTM D 368296ASTM D 1193

2 Annual book of ASTM standards Vol.11.014.

(AAS). H , , , . ( 5)

5. :

, , , , 190800 nm .

: . .

: , . , .

( ) 10733

:

, . , .

: 250 mL .

: , , Teflon , , 1:1 HNO3 , 1: l HCl .

6.

. American Chemical Society, .

: , II D 1193.

: .

, .

(): , 1 .

1: , .

(1:1): 1:1 .

(1:1): HCl 1:1,

: .

: .

: . , . > 99.5%

7.

. :

15 min ( ).

, , .

, , % , .

. , . .

. , . , , 0 80%. . :

= log (100%) = 2 log (%T),: % = 100 % ,

, .

5

1 g (Li2B4O7)

.

, 1000C.

, 7.2 7.3 5.

. , , , , .

, , . .

.

10734 ( )

, . , . 1.

:

.

.

7.1 7.1.1 : 5 50 mg/L

309,3 nm (. 2 3).

: : : : 1 mg/L : 0,1 mg/L 2:

308,2 nm 1 396,2 nm 2 394,4 nm 2,5 3:

0,3 mg/L .

7.1.2 : 1,000 g

( ) . 15 mL HCl , . , 1L . 1 mL = 1 mg AI (1000mg/L)

KCI: 95 g (KCl) 1L.

7.1.3

. . 100 mL , , 2,0 mL KCl.

7.1.4 .

. (, 1000 g/mL) , .

7.2 7.2.1 : 0,2 7 mg/L

422,7nm (. 4 )

: : : 0,08 mg/L 0,01 mg/L 4: 239,9nm

120.7.2.2 : 1,250 g

CaCO3 ( ) 180C 1h, . 1000 mL . 1 mL = 0,5 mg Ca (500 mg/L)

: 29 g La2O3 , 250 mL HCl ( ). 500 mL .

7.2.3

. .

10 mL 1,0 mL , . 20 mL + 2mL LaCl3 = 22 mL.

7.2.4 , ,

. (La) . Ca pH >7, . Mg>1000 mg/L Ca. 500 mg/L Na, K NO3 .

2 5 .

7.3 7.3.1 : 0,3 5 mg/L

248,3nm (. 5 6)

0,12 mg/L 0,03 mg/L: : : 5:

: 248,8 nm 2 271,9 nm 4 302,1 nm 5 252,7 nm 6 372,0 nm 10 6:

0,05 mg/L .

7.3.2 : 1,000 g

( ) 5 mL HNO3 , . , 1 L . ImL = 1mg Fe (1000 mg/L).

7.3.3.

. .

7.4 7.4.1 : 0,02 0,5 mg/L

285,2 nm (. 7) 0,007 mg/L 0,001 mg/L: : : 7:

202,5 nm 25.7.4.2

: 0,829 g MgO (

) 10 mL HNO3 1 L . 1 mL = 0,50 mg MgO (500 mg/L).

: 29 g La2O3 , 250mL HCl ( ). 500 mL .

7.4.3

. , .

10 mL 1,0 mL , . 20 mL + 2 mL LaCl3 = 22 mL.

7.4.4

2mg/L La. Na, K Ca 400mg/L.

7.5 7.5.1 : 0,1 2 mg/L

766,5nm (. 8)

: 0.04mg/L : 0.01 mg/L

: : : 8:

404,4. 500.

7.5.2

: 0,1907g KCl ( ), 110C, 1L. 1mL=0,10 mg K (100 mg/L).

7.5.3

. .

7.5.4

(>2800C), .

. Na Na / 10. Na Na (1000g/mL) . , (Cs).

.

7.6 7.6.1 : 0,03 1 mg/L,

589,6 nm (. 9)

0,015 mg/L 0,002 mg/L: : : 9: 330,2 nm

, 185, Na.

7.6.2

: 2,542 g NaCl ( ), 140C, 1L. 1 mL = 1mg (1000 mg/L).

7.6.3

.

551 ( ) 10735

10736 ( )

.

7.6.4

. (1000 mg/L) , .

7.7 7.7.1 : 5 50 mg/L

251,6 nm.: : : 7.7.2

:

, . 0.1070 g SiO2 1g , HCl HNO3 250 mL . 200 ppm.

.

: 50 mL HCl (. . 1.19 g/mL) 50 mL HNO3 (. 1.42 g/mL) 1000 mL.

7.7.3 .

Si, 1 mL AI (1000 ppm) 100 mL

Si mL ppmSi % SiO2 25 50 53.5 20 40 42.8 15 30 32.1 10 20 21.4

: 2g / Li2B4O7 .

: .

% :%SiO2 = [(CB) / (B) x x 1.07

=

C = C =

= ppm Si 8. mg/L

. :

mg/L = A [(C+B)/C]:= mg/L

= mL

C = mL :

mg /kg = A x V/D: = mg/L

V= mLD = IT g

%

E = [(CB)/(AB)]x(N/M)xFx100:= = C= = ppm = ppm F = %

: %

( ) 10737

9. . ,

, , .

. : , , .

. :

. , , . .

Scientific Apparatus Makers Association (SAMA) : , , .

, . .

mg L

1%.. ,

AAS .

, , , Mg, , , , .

Mg, Ca Ba. , Si n Ca.

, , , . .

, , , . , . .

, , . , , , , .

, , , , . , , . , . , .

. ASTM D 368292, AI, Fe, Ca, Mg, Na, HCl. .

10738 ( )

6:

1.

.

2.

.

. , , .

3. 196 2, 10.4.

.

5.

0,1 mg. ,

1000 C.

(Mg(ClO4)2 ).

, 20 25 ml, .

. , 250 ml. (.. ),

( 0,007 mm)

6.

.

(HC1), 1,19 g/cm3.

(HCl) (1+3). 10 mL

30 mL . (HCl) (1+9). 10 mL

90 mL . . 250 g

1000 mL.

(AgNO3). 0,5 g

(AgNO3) , 10 mL 100 mL.

7. 1 g 0,05 g (B g)

.

200 mL.

25 mL .

, 40 mL HCl ,

. .

20 mL .

100 mL 1+3 .

, ( 0,45 m).

, , (*).

250 mL 100 mL .

16 .

4 . ,

.

, 100 mL 1+9 (*).

( g) , (**).

.

, .

975 25 C, (**).

, ( ).

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.8. ,

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( ) 10739

. (AgNO3).

, (AgCl), .

, (AgNO3), .

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7: 1.

. 197.1 3.2 , (HCl) ().

, SiO2 , 5 , SiO2 , 6.

2.

HCl (Li2B4O7).

(HCl).

/ .

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.

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56, 5 6 Si 66 () .

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) :

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( 6)(Si2)AY= % Si2

( )9.

HCl (200 mL).

, (5+95).

8:

1.

, 105 110C.

2.

105 110C, .3. ASTM C 31198b, 11,12 EN 4501/2001, 7.4.

.

5.

0,1 mg. ,

110 5C 6. 7. 105 110C, ,

(*)

10740 ( )

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. ( g)

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105 110C. 105 110C. ,

( ).

( g). ,

, (*).

8. , % . .

, :% =100 [( )/] x 100 :

: , g,:

, g : +

, g.9. (*) :

, 0,0005 g.

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10742 ( )

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2007-04-23T12:15:48+0200Athens, Ethniko TypografioTheodoros MoumourisSigned PDF (embedded)

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