Cannabinoid Distribution - Whole Leaf

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Cannabinoid Result (%) Result (mg/g) Reporting Limit (mg/g) Result (mg/mL) Per Unit (mg) CBD - - 0.025 - - CBDa - - 0.025 - - CBDv - - 0.025 - - Δ9-THC 0.177 1.77 0.025 - 12 Δ8-THC - - 0.025 - - THCa - - 0.025 - - THCv - - 0.025 - - CBC - - 0.025 - - CBG 0.0309 0.309 0.025 - 2 CBGa - - 0.025 - - CBN - - 0.025 - - 100 80 60 40 20 CBD CBDa CBDv Δ9-THC Δ8-THC THCa THCv CBG CBGa CBC CBN TOTAL 0.208 2 - 15 TOTAL THC 0.177 1.77 - 12 TOTAL CBD - - - - Cannabinoid Distribution (% of Total Cannabinoids) CERTIFICATE OF ANALYSIS Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None Order ID: OR2019-4162 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None Cultivar (Strain): Orange gummies Lab ID: SA2019-13376 Sample Matrix: Edible Sample Date: 09/30/2019 Date Received: 09/30/2019 Date Completed: Remarks: CANNABINOID (POTENCY) PROFILE Analysis Date/Time: 10/01/2019 1056 Method: HPLC/DAD (Internal Method-001) Moisture Content (%): - Analyst: OL Instrument: Agilent 1100 Water Activity (aw): - This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA. Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616 Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344 Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139 0.0 0.0 0.0 85.1 0.0 0.0 0.0 14.9 0.0 0.0 0.0 UNIT MASS (g): 7 "-" Not detected above RL. Deviations from standard operating procedure: None Recoveries for all analyte standards: 90-110% Replicate Uncertainties: <5% RSD, <20% RPD Sample/Reagent Blanks: <RL for all analytes Values for plant matter are adjusted for moisture content. Total THC = (THCa x 0.877) + Δ9-THC Total CBD = (CBDa x 0.877) + CBD Percentage results are reported by mass. mg/g results are reported as mass component per mass material. Abbreviations: UV - Ultraviolet, HPLC - High Pressure Liquid Chromatography, RL - Reporting Limit, RPD - Relative Percent Difference, RSD - Relative Standard Deviation REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Felling Analytical Services and Technology (F.A.S.T.), LLC www.FASTLaboratories.com 10/02/2019 Page 1 of 1
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Transcript of Cannabinoid Distribution - Whole Leaf

Δ8-THC - - 0.025 - -
THCa - - 0.025 - -
THCv - - 0.025 - -
CBC - - 0.025 - -
CBGa - - 0.025 - -
CBN - - 0.025 - -
100
80
60
40
20
CBD CBDa CBDv Δ9-THC Δ8-THC THCa THCv CBG CBGa CBC CBN
TOTAL 0.208 2 - 15
TOTAL CBD - - - -
CERTIFICATE OF ANALYSIS
Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None
Order ID: OR2019-4162 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None
Cultivar (Strain): Orange gummies Lab ID: SA2019-13376 Sample Matrix: Edible
Sample Date: 09/30/2019 Date Received: 09/30/2019 Date Completed:
Remarks:
Analysis Date/Time: 10/01/2019 1056 Method: HPLC/DAD (Internal Method-001) Moisture Content (%): -
Analyst: OL Instrument: Agilent 1100 Water Activity (aw): -
This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
0.0 0.0 0.0
Deviations from standard operating procedure: None
Recoveries for all analyte standards: 90-110% Replicate Uncertainties: <5% RSD, <20% RPD Sample/Reagent Blanks: <RL for all analytes
Values for plant matter are adjusted for moisture content.
Total THC = (THCa x 0.877) + Δ9-THC Total CBD = (CBDa x 0.877) + CBD
Percentage results are reported by mass. mg/g results are reported as mass component per mass material.
Abbreviations: UV - Ultraviolet, HPLC - High Pressure Liquid Chromatography, RL - Reporting Limit, RPD - Relative Percent Difference, RSD - Relative Standard Deviation
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
10/02/2019
Δ8-THC - - 0.0251 - -
THCa - - 0.0251 - -
THCv - - 0.0251 - -
CBC - - 0.0251 - -
CBG - - 0.0251 - -
CBGa - - 0.0251 - -
CBN - - 0.0251 - -
100
80
60
40
20
CBD CBDa CBDv Δ9-THC Δ8-THC THCa THCv CBG CBGa CBC CBN
TOTAL 0.153 1.53 - 10.7
TOTAL CBD - - - -
CERTIFICATE OF ANALYSIS
Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None
Order ID: OR2019-4684 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None
Cultivar (Strain): Smokies / Jamberry Lab ID: SA2019-14896 Sample Matrix: Edible
Sample Date: 10/18/2019 Date Received: 10/18/2019 Date Completed: 10/25/2019
Remarks:
Analyst: OL Instrument: Agilent 1100 Water Activity (aw): -
This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
0.0 0.0 0.0
UNIT MASS (g): 7
"-" Not detected above RL.
Deviations from standard operating procedure: None
Recoveries for all analyte standards: 90-110% Replicate Uncertainties: <5% RSD, <20% RPD Sample/Reagent Blanks: <RL for all analytes
Values for plant matter are adjusted for moisture content.
Total THC = (THCa x 0.877) + Δ9-THC Total CBD = (CBDa x 0.877) + CBD
Percentage results are reported by mass. mg/g results are reported as mass component per mass material.
Abbreviations: UV - Ultraviolet, HPLC - High Pressure Liquid Chromatography, RL - Reporting Limit, RPD - Relative Percent Difference, RSD - Relative Standard Deviation
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
10/25/2019
Xylenes* (1330-20-7) - 430
"-" not detected above reporting limit
"*" - o,m,p-Xylene and Ethylbenzene
1,2-Dimethoxyethane Monoglyme
2,3-Dimethylbutane Neohexane
2,3-Dimethylbutane Diisopropyl
N,N-Dimethylformamide DMF
Dimethysufoxide DMSO
Solvent Synonym(s)
Ethyl acetate EtOAc
Ethyl benzene Phenylethane
Ethylene glycol 1,2-Ethanediol
Ethylene oxide Oxirane
Solvent Synonym(s)
CERTIFICATE OF ANALYSIS
Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None
Order ID: OR2019-4684 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None
Cultivar (Strain): Smokies / Jamberry Lab ID: SA2019-14896 Sample Matrix: Edible
Sample Date: 10/18/2019 Date Received: 10/18/2019 Date Completed: 10/25/2019
Remarks:
Analysis Date/Time: 10/22/2019 0258 Method: USP <467> Deviations from SOP:
Analyst: OL Instrument: Agilent 6890 None
Disclaimer: This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
10/25/2019
"-" not detected above reporting limit
"*" analyzed by GC/MS (all others analyzed
by LC/MS/MS)
the cis- and trans- permethrin isomers.
Abbreviations: LC - Liquid Chromatography, GC - Gas Chromatography, MS - Mass Spectrometry, RL - Reporting Limit, AL - Action Level, CAS - Chemical Abstract Services
Pesticide Synonym(s)
Cyfluthrin Baythroid
DDVP Dichlorvos
Ethoprophos Prophos
Pesticide Synonym(s)
Myclobutanil Systhane
Naled Dibrom
Phosmet Imidan
Pesticide Synonym(s)
Propiconazole Tilt
Propoxur Baygon
Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None
Order ID: OR2019-4684 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None
Cultivar (Strain): Smokies / Jamberry Lab ID: SA2019-14896 Sample Matrix: Edible
Sample Date: 10/18/2019 Date Received: 10/18/2019 Date Completed: 10/25/2019
Remarks:
Analysis Date/Time: 10/22/2019 0258 Method: LC/MS/MS and GC/MS Deviations from SOP:
Analyst: OL Instrument: Waters Acquity/TQD None
Disclaimer: This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
10/25/2019
Abbreviations: EC - Escherichia Coli, CFU - Colony-Forming Unit, RL - Reporting Limit, AL - Action Level
Color Key
CERTIFICATE OF ANALYSIS
Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None
Order ID: OR2019-4684 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None
Cultivar (Strain): Smokies / Jamberry Lab ID: SA2019-14896 Sample Matrix: Edible
Sample Date: 10/18/2019 Date Received: 10/18/2019 Date Completed: 10/25/2019
Remarks:
Analyst: OL Instrument: Waters Acquity/TQD None
Disclaimer: This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
10/25/2019
Color Key
CERTIFICATE OF ANALYSIS
Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None
Order ID: OR2019-4684 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None
Cultivar (Strain): Smokies / Jamberry Lab ID: SA2019-14896 Sample Matrix: Edible
Sample Date: 10/18/2019 Date Received: 10/18/2019 Date Completed: 10/25/2019
Remarks:
Analyst: OL Instrument: PerkinElmer Elan 9000 None
Disclaimer: This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
10/25/2019
Escherichia Coli (E. Coli) Absent 1
Mold Absent 104
Yeast Absent 104
Abbreviations: EC - Escherichia Coli, CFU - Colony-Forming Unit, RL - Reporting Limit, AL - Action Level, NT - Not Tested
Color Key
CERTIFICATE OF ANALYSIS
Order Type: Medical Cannabis Customer ID: 403 Harvest/Extract Lot: None
Order ID: OR2019-4684 Customer Name: Doverbrothers LLC Harvest/Extract Batch: None
Cultivar (Strain): Smokies / Jamberry Lab ID: SA2019-14896 Sample Matrix: Edible
Sample Date: 10/18/2019 Date Received: 10/18/2019 Date Completed: 10/25/2019
Remarks:
Analyst: OL Instrument: Thermo Incubator None
Disclaimer: This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
10/25/2019
Δ8-THC - - 0.0254 - -
THCa - - 0.0254 - -
THCv - - 0.0254 - -
CBC - - 0.0254 - -
CBG - - 0.0254 - -
CBGa - - 0.0254 - -
CBN - - 0.0254 - -
100
80
60
40
20
CBD CBDa CBDv Δ9-THC Δ8-THC THCa THCv CBG CBGa CBC CBN
TOTAL 0.171 1.71 - 11
TOTAL CBD - - - -
CERTIFICATE OF ANALYSIS
Order ID: OR2019-5128 Customer Name: Doverbrothers LLC Harvest/Extract Batch: 12
Cultivar (Strain): Gummy Lab ID: SA2019-16373 Sample Matrix: Edible
Sample Date: 11/04/2019 Date Received: 11/05/2019 Date Completed: 11/12/2019
Remarks:
Analyst: OL Instrument: Agilent 1100 Water Activity (aw): -
This information is provided as a service and makes no claims of efficacy and/or safety of this product. Results are applicable only for the sample(s) analyzed and for the specific analysis conducted. This report is for informational purposes only and should not be used to diagnose, treat, or prevent any medical-related symptoms. The statements and results herein have not been approved and/or endorsed by the FDA.
Arkansas Location 232 S Broadview St Greenbrier, AR 72058 (501) 679-2616
Oklahoma City Location 3680 E I-240 Service Rd Oklahoma City, OK 73135 (405) 595-0344
Tulsa Location 14720 E Admiral Pl, Ste H Tulsa, OK 74108 (918) 340-7139
0.0 0.0 0.0
UNIT MASS (g): 6.5
"-" Not detected above RL.
Deviations from standard operating procedure: None
Recoveries for all analyte standards: 90-110% Replicate Uncertainties: <5% RSD, <20% RPD Sample/Reagent Blanks: <RL for all analytes
Values for plant matter are adjusted for moisture content.
Total THC = (THCa x 0.877) + Δ9-THC Total CBD = (CBDa x 0.877) + CBD
Percentage results are reported by mass. mg/g results are reported as mass component per mass material.
Abbreviations: UV - Ultraviolet, HPLC - High Pressure Liquid Chromatography, RL - Reporting Limit, RPD - Relative Percent Difference, RSD - Relative Standard Deviation
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of
Felling Analytical Services and Technology (F.A.S.T.), LLC
www.FASTLaboratories.com
11/12/2019